| 大孔吸附树脂纯化蒺藜总皂苷的工艺研究 |
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| 引用本文： | 杨帆,朱才庭,程丹,周斌.大孔吸附树脂纯化蒺藜总皂苷的工艺研究[J].安徽农业科学,2011,39(26):15939-15940. |
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| 作者姓名： | 杨帆 朱才庭 程丹 周斌 |
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| 作者单位： | 江西科技师范学院药学院,江西南昌,330013;广东省罗浮山白鹤制药厂,广东惠州,516133 |
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| 基金项目： | 江西科技师范学院本科生创业科研基金资助项目; 江西省自然基金资助项目(编号:2010GZY0058) |
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| 摘 要： | 目的]通过对10种大孔吸附树脂筛选,寻求适用于纯化蒺藜总皂苷类成分的大孔吸附树脂。方法]比较不同种大孔吸附树脂对蒺藜总皂苷的静态吸附率和解吸率;用不同浓度的乙醇进行洗脱并计算总皂苷回收率和纯度。结果]HPD-300大孔吸附树脂的回收率为87%,纯度可以达到68%。结论]HPD-300树脂综合性能最好,适宜于蒺藜总皂苷的分离纯化。
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| 关 键 词： | 蒺藜(Tribulus terrestris L.) 大孔吸附树脂:纯化 总皂苷 |
Purification of Total Saponin in FRUCTUS TRIBULI by Macroporous Adsorption Resins |
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| YANG Fan et al.Purification of Total Saponin in FRUCTUS TRIBULI by Macroporous Adsorption Resins[J].Journal of Anhui Agricultural Sciences,2011,39(26):15939-15940. |
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| Authors: | YANG Fan |
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| Institution: | YANG Fan et al(School of Pharmacy,Jiangxi Science and Technology Normal University,Nanchang,Jiangxi 330013) |
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| Abstract: | Objective]To select 10 types of macroporous adsorption resin so as to find out the resin which was applicable to purifying the total saponin in FRUCTUS TRIBULI.Method]The static absorption ratios and desorption ratios of total saponin in FRUCTUS TRIBULI by different types of macroporous adsorption resin were compared,the HPD-300 was eluted by different concentrations of ethanol to calculate the purity and yield of total saponin.Results]]The yield and purity of HPD-300 resin was 87% and 68%.Conclusion]HP... |
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| Keywords: | FRUCTUS TRIBULI Macroporous adsorption resin Purification Total saponin |
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