| 大豆中戊唑醇的气相色谱分析方法研究 |
| |
| 引用本文： | 孙慧,侯志广,钱永盛,刘晓旭,逯忠斌. 大豆中戊唑醇的气相色谱分析方法研究[J]. 安徽农业科学, 2011, 39(15): 9029-9030 |
| |
| 作者姓名： | 孙慧 侯志广 钱永盛 刘晓旭 逯忠斌 |
| |
| 作者单位： | 吉林农业大学资源与环境学院; |
| |
| 基金项目： | 农业部残留课题资助项目(2009F01) |
| |
| 摘 要： | [目的]建立气相色谱测定大豆和植株中戊唑醇残留的分析方法。[方法]样品经丙酮提取、液-液分配、弗罗里硅土层析柱净化后,采用气相色谱氮磷检测器进行测定。[结果]在添加量为0.02～1.00 mg/kg范围内,戊唑醇在大豆和植株中的平均回收率分别为90.7%～105.3%和93.2%～100.6%,相对标准偏差分别为2.1%～8.9%和1.7%～4.6%;方法的最低检出量为1×10-10 g,最低检测浓度为0.01 mg/kg。[结论]该方法简单、快速,结果准确,灵敏度、精密度和检测限均符合农药残留分析的要求。
|
| 关 键 词： | 大豆 戊唑醇 气相色谱 |
Studies on Residue Analysis Method of Tebuconazole in Soybean by Gas Chromatography |
| |
| SUN Hui et al. Studies on Residue Analysis Method of Tebuconazole in Soybean by Gas Chromatography[J]. Journal of Anhui Agricultural Sciences, 2011, 39(15): 9029-9030 |
| |
| Authors: | SUN Hui et al |
| |
| Affiliation: | SUN Hui et al(College of Resources and Environment,Jilin Agricultural University,Changchun,Jilin 130118) |
| |
| Abstract: | [Objective] The aim was to establish a residue analysis method of tebuconazole in soybean by gas chromatography.[Method] After samples went extracted by acetone,cleaned up with petroleum ether by liquid-liquid partition and Florisil siliceous earth chromatography column,they were determined by gas chromatography with nitrogen-phosphorus detection(NPD).[Result] Average recoveries of tebuconazole in soybean and plant were 90.7%-105.3% and 93.2%-100.6% respectively under the spiking level of 0.02-1.00 mg/kg,an... |
| |
| Keywords: | Soybean Tebuconazole Gas chromatography |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
