超声波辅助提取千斤拔中总黄酮的工艺研究 |
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引用本文: | 陈帅,王慧竹. 超声波辅助提取千斤拔中总黄酮的工艺研究[J]. 安徽农业科学, 2011, 39(36): 22311-22312,22316 |
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作者姓名: | 陈帅 王慧竹 |
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作者单位: | 吉林化工学院化学与制药工程学院,吉林吉林,132022 |
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摘 要: | [目的]优选超声波法提取千斤拔中总黄酮的最佳工艺条件。[方法]以总黄酮提取率为评价指标,采用单因素和正交试验确定超声波辅助提取千斤拔总黄酮的工艺条件。[结果]最佳的超声提取条件为乙醇浓度为80%,提取时间为25min,料液比为.1:20(g/ml),提取次数为2次;在此条件下,千斤拔总黄酮的得率为3.00%。[结论]确定了超声波辅助提取千斤拔总黄酮的最佳工艺条件,为千斤拔资源的合理开发利用提供了理论依据。
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关 键 词: | 千斤拔(Philippine Flemingia Root) 总黄酮 正交试验 超声波 |
Study on Extraction Process of General Flavone from Radix Flemingia Philippinensis with Ultrasonic Wave Method |
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Affiliation: | CHEN Shuai et al (College of Chemistry and Pharmaceutical Engineering,Jilin Institute of Chemical Technology,Jilin,Jilin 132022) |
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Abstract: | [Objective] The aim was to study the optimum extraction process of general flavone from Radix Flemingia Philippinensis with ultrasonic wave method.[Methods]With the extraction rate of flavonoids as the evaluation index,the extraction process was optimized with single factor and orthogonal test.[Results] The optimum extraction process of general flavone from Radix Flemingia Philippinensis with ultrasonic wave method was as follows: ethanol concentration of 80%,ultrasonic time of 25 min,solid-liquid ratio of 1∶20(g/ml),extraction times for 2 times.Under the condition,the yield of general flavone from Radix Flemingia Philippinensis was 3.00%.[Conclusion] The optimum ultrasonic wave extraction process of general flavone from Radix Flemingia Philippinensis was obtained,which would provide theoretical basis for the development and utilization of Radix Flemingia Philippinensis. |
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Keywords: | Philippine Flemingia Root General flavone Orthogonal test Ultrasonic wave method |
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