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烟用聚丙烯丝束滤棒成型胶粘剂中苯系物含量的测定
引用本文:黎洪利,白晓虹,文鹏,蔡利.烟用聚丙烯丝束滤棒成型胶粘剂中苯系物含量的测定[J].安徽农业科学,2011,39(6):3657-3658,3680.
作者姓名:黎洪利  白晓虹  文鹏  蔡利
作者单位:1. 重庆烟草工业有限责任公司,重庆,400060
2. 重庆医药工业研究院有限责任公司,重庆,400061
摘    要:目的]测定烟用聚丙烯滤棒成型胶粘剂中的苯系物含量。方法]采用顶空-气相色谱法对丙纤胶进行检测,并用外标曲线法进行定量。结果]以5 m l饱和NaC l溶液作为样品基质,样品瓶在80℃下平衡30.0 m in,各苯系物的平均回收率为93%~105%,相对标准偏均差〈5%。结论]该方法可以用来测定烟用丙纤胶中微量苯系物。

关 键 词:聚丙烯丝束  胶粘剂  苯系物  顶空-气相色谱法

Determination of Benzene Homologues in Adhesive Applied on Polypropylene Tow for Making Cigarette Filter Rod
LI Hong-li et al.Determination of Benzene Homologues in Adhesive Applied on Polypropylene Tow for Making Cigarette Filter Rod[J].Journal of Anhui Agricultural Sciences,2011,39(6):3657-3658,3680.
Authors:LI Hong-li
Institution:LI Hong-li et al(Chongqing Tobacco Industrial Co.Ltd,Chongqing 400060)
Abstract:Objective] To determine the benzene homologues in adhesive applied on polypropylene tow for making cigarette filter rod.Method] Headspace gas chromatography with area-external standard method was applied to quantitative analyze the benzene homologues in adhesive.Result] The sample was mixed with 5 ml saturated sodium chloride solution,then sample vial was balanced 30.0 min under 80 ℃.Under such conditions,the recovery was 93%-105%,and RSD was below 5%.Conclusion] The method was suitable for the determination of the benzene homologues in adhesive applied on polypropylene tow for making cigarette filter rod.
Keywords:Polypropylene fiber tow  Adhesive  Benzene homologues  Headspace gas chromatography  
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