| 新型水产诱食剂氯化羧甲基二甲基锍的合成 |
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| 引用本文： | 陆豫,李伟杰,邸维龙,吴世林. 新型水产诱食剂氯化羧甲基二甲基锍的合成[J]. 饲料工业, 2006, 27(12): 54-55 |
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| 作者姓名： | 陆豫 李伟杰 邸维龙 吴世林 |
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| 作者单位： | 南昌大学中德联合研究院,330047,江西南昌;汕头大学多学科研究中心;广州市智特奇饲料科技有限公司 |
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| 摘 要： | 运用无溶剂合成方法,利用较低成本的氯乙酸为原料与二甲硫醚反应,合成新型水产动物诱食剂——氯化羧甲基二甲基锍。该化合物通过1HNMR、13CNMR、MS和元素分析证实了其结构。通过正交实验法,获得较佳反应条件:反应温度为75℃,反应时间12h,n氯乙酸:n二甲基硫醚=1:1.18,收率达到72.2%。
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| 关 键 词： | 诱食剂 氯化羧甲基二甲基锍 合成 |
| 收稿时间： | 2006-03-21 |
| 修稿时间： | 2006-03-21 |
Synthesis of carboxymethyl dimethyl sulfonium chloride as a novel aquatic feed attractant |
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| Lu Yu,Li Weijie,Di Weilong,Wu Shilin. Synthesis of carboxymethyl dimethyl sulfonium chloride as a novel aquatic feed attractant[J]. Feed Industry, 2006, 27(12): 54-55 |
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| Authors: | Lu Yu Li Weijie Di Weilong Wu Shilin |
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| Abstract: | Carboxymethyl dimethyl sulfonium chloride as a novel aquatic feed attractant was synthesized with chloroacetic acid, methyl sulfide and in solvent free system. Its chemical structure was determined by 1HNMR, 13CNMR, MS spectra and elemental analysis. Optimum reaction condition was obtained by orthogonal test, which reaction temperature was 75℃, reaction time 12h and n(chloroacetic acid):n(metyl sulfide)=1:1.18, Yield of the product was 72.2%. |
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| Keywords: | feed attractant carboxymethyl dimethyl sulfonium chloride synthesis |
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