| N-(7-氟-3-氧-3,4-二氢-苯并噁嗪-6-基-)乙酰胺类化合物的合成及除草活性 |
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| 引用本文： | 黄明智,闵忠诚,任叶果,胡礼,黄路,杨光富. N-(7-氟-3-氧-3,4-二氢-苯并噁嗪-6-基-)乙酰胺类化合物的合成及除草活性[J]. 农药学学报, 2006, 8(2): 172-175 |
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| 作者姓名： | 黄明智 闵忠诚 任叶果 胡礼 黄路 杨光富 |
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| 作者单位： | 1.华中师范大学 化学学院 湖北 武汉 430079 |
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| 基金项目： | 国家高技术研究发展计划(863计划) |
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| 摘 要： | 为了寻找高效、安全的具有除草活性的新化合物,利用2-取代乙酰氯和2H苯并噁嗪-3-酮反应合成了9个N-(7-氟-3-氧-3,4-二氢苯并噁嗪-6-基-)乙酰胺类化合物,其结构经元素分析、IR、1H NMR确证。初步除草活性测试表明:在有效剂量75 g/hm2下,化合物 5d 芽后茎叶处理对刺苋Amaranthus spinosus等4种杂草显示出90%以上的抑制率。
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| 关 键 词： | N-苯并噁嗪乙酰胺 合成 除草活性 |
| 文章编号： | 1008-7303(2006)02-0172-04 |
| 收稿时间： | 2006-01-10 |
| 修稿时间： | 2006-04-24 |
Synthsis and Herbicidal Activity of N-(7-Fluoro-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl) Acetamide |
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| HUANG Ming-zhi,MIN Zhong-cheng,REN Ye-guo,HU Li,HUANG Lu and YANG Guang-fu. Synthsis and Herbicidal Activity of N-(7-Fluoro-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl) Acetamide[J]. Chinese Journal of Pesticide Science, 2006, 8(2): 172-175 |
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| Authors: | HUANG Ming-zhi MIN Zhong-cheng REN Ye-guo HU Li HUANG Lu YANG Guang-fu |
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| Affiliation: | 1.College of Chemistry,Central China Normorl University, Wuhan 430079,China2.National Engineering Research Center for Agrochemicals,Hunan Research Institute of Chemical Industry,Changsha 410007, China |
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| Abstract: | In search of safe and more efficacious herbicidal compounds,nine novel derivatives of N-(7-fluoro-3-oxo-3,4-dihydro-2H-benzo oxazin-6-yl) acetamide were prepared from the reaction of 2-substitued acetyl chloride with the corresponding 2H benzo oxazine-3-one. Their chemical structures were confirmed by elemental analysis, IR and 1H NMR. The primary bioassay results showed that 5d exhibited control efficacy of more than 90% against Amaranthus spinosus at 75 g a.i./hm2. |
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| Keywords: | N-benzo [ b ] [ 1,4 ] oxazin acetamide synthesis herbicidal activity |
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