模拟白酒样品中三聚氰胺的紫外分光光度法分析过程初探 |
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引用本文: | 王小艳,薛亚丽,谢建平. 模拟白酒样品中三聚氰胺的紫外分光光度法分析过程初探[J]. 安徽农业科学, 2010, 38(11): 5542-5543 |
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作者姓名: | 王小艳 薛亚丽 谢建平 |
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作者单位: | 周口师范学院,河南周口,466000;周口师范学院,河南周口,466000;周口师范学院,河南周口,466000 |
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摘 要: | 依据三聚氰胺在紫外区220~240nm有灵敏的吸收峰,对建立简便、快速、灵敏的测定模拟白酒样品中三聚氰胺的紫外分光光度法分析过程进行了探索。研究表明,在较低浓度时,相对标准偏差为1.0%,回收率为102%;在高浓度时,可能由于溶液中物质间的相互作用,误差较大。
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关 键 词: | 食品安全 三聚氰胺 紫外分光光度法 模拟白酒样品 |
A Preparatory Study on Melamine in Artificial White Spirit Sample by Ultraviolet Spectrophotometry |
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Affiliation: | WANG Xiao-yan et al (Zhoukou Normal University, Zhoukou, Henan 466000) |
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Abstract: | A preparatory method was investigated for the determination of melamine by ultraviolet spectrophotometry.Melamine has a sensitive absorption peak between 220 nm and 240 nm.The method was used to determine melamine in white spirit with the standard deviation 1.0%,and the average recovery was 102% in low concentration.But the deviation was bigger in high concentration.The influence of interactions among materials existed in the solution was a possible reason. |
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Keywords: | Food security Melamine Ultraviolet spectrophotometry Artificial white spirit sample |
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