衡平新闻自由与司法独立间的关系

1.总结我国在此方面的漏洞,寻求切实可行的法制理念近代中国在对司法独立进行价值追求的过程中,逐渐抽空其内在的生命,转而崇拜其外在的空壳,并将这个空壳视为真实的存在,以便于使其依归于中国的现实,实现其一种本土化的选择目标——从理想到现实的转换、从价值理念到工具理念的嬗变。从司法权的三大原则中,凸显司法独立与新闻自由间的冲突,微见这对矛盾的在现实中的漏洞。1.1司法权的专属性司法独立原则下司法权必须专属于合格的法院[1]。因此,确定司法     

Establishment and Application of Reversed-phase High Performance Liquid Chromatography Method for Detection of Related Substances of Rifaximin Uterine Infusion in Dairy Cows

The study was aimed to establish a method for detection of rifaximin related substances by reversed-phase high-performance liquid chromatography with UV detector. The instrument methods was WondaSil C18-WR 250 mm×4.6 mm 5 μm column, mobile phase was methanol∶acetonitrile∶3.16 g/L ammonium formate (concentrated aqueous ammonia adjusted to pH 7.2)=31.5∶31.5∶37, with detection wavelength 276 nm. Area normalization method was used to calculate the limit of detection, limit of quantification and concentration of rifaximin uterine injectant; The precision of the method, linear correlation and related substances specificity were explored. And the degradation degree of the peak area of the principal components was compared by the destruction of the extreme conditions, the content of the related substances and the separation degree. 40 to 150 μg/mL concentration of rifaximin, peak area and concentration showed a good linear relationship (R²=0.9998), the related substances concentration on peak area linear regression equation was y=23 510x+7 182, within a certain period of time after preparation of acids, alkalis, oxidation, high temperature degradation damage in varying degrees, in the main ingredient content in the sample before the damage was 100.00%, after oxidative damage and heat damage the main component was 13%, acids, alkalis destruction of the main component degradation was about 18%, the main component peak retention time was consistency before and after the destruction. The retention time and resolution of rifaximin and related-substance were good. (The separation between the main component peak and the impurity peaks were greater than 1.5, the degree of separation between the impurity peak and impurity peaks greater than 1.2). The substance detection methods of rifaximin uterine injectants was simple and had specificity and good repeatability, selective and sensitive, which could be used to analyze the related substance of rifaximin uterine injectants.     

HPLC测定真菌及其制品中麦角甾醇含量

本研究旨在找出真菌及其制品的特征指标,用于其质量评价、掺伪鉴别等.建立了真菌及其制品中麦角甾醇含量测定的高效液相色谱法(HPLC),并利用建立的HPLC法对冬虫夏草、破壁灵芝孢子粉等真菌及其制品以及螺旋藻、大豆油等6种植物油样品进行麦角甾醇含量的测定.结果显示,麦角甾醇在5～160μg/mL范围内具有较好的线性,线性相...     

E-1-碘-3-苯基-3-三甲硅氧基-1-辛烯的合成

以己酸为原料,经六步合成出标题化合物。对于中间体——3-苯基-3-羟基-1-辛炔(Ⅳ)。设计了两条不同的合成路线,即由乙炔基锂或乙炔基溴化镁与酮反应高产率地合成出(Ⅳ)。研究了二氢吡喃和三甲基氯硅烷保护(Ⅳ)的反应条件。最后,利用三正丁基锡烷为氢化剂,碘为卤化剂,由3-苯基-3-三甲硅氧基-1-辛炔以93.2％的产率立体专属性地合成出标题化合物。     

论配偶权的立法完善及保护

配偶权是指法律赋予的夫妻互为权利义务主体的身份权,其他任何人均不得侵犯。我国现行《婚姻法》对配偶权的规定过于简单、笼统,尤其是漠视夫妻关系的自然属性,并对配偶权缺乏有效的保护机制,因而有待完善。完善配偶权,主要应充实配偶权的具体内容,并设计相应的救济方法。     

高效液相色谱法测定兽用复方酮康唑乳膏中酮康唑的含量

笔者建立了高效液相色谱法测定兽用复方酮康唑乳膏中酮康唑含量。样品经80℃水浴用乙醇提取等前处理,采用Agilent ZORBAX Eclipse(4.6 mm×150 mm,5μm)色谱柱;流动相为甲醇-水（74∶26）;流速为1.0 mL/min;柱温为30℃;检测波长为239 nm。结果酮康唑在0.4015～1.2016 mg/mL范围内呈良好线性,r2=1.000。样品平均回收率为99.52%,RSD为0.70%。该法简便可靠,可测定兽用复方酮康唑乳膏中酮康唑含量。     

奶牛用利福昔明子宫注入剂有关物质反相高效液相色谱检测方法的建立及应用

本试验旨在建立利福昔明有关物质的检测方法。采用反相高效液相色谱法,紫外检测器进行检测,采用WondaSil C18-WR 250 mm×4.6 mm 5 μm色谱柱,柱温:40 ℃,流动相及其比例为:V（甲醇） ∶V（乙腈）∶V（3.16 g/L甲酸铵,浓氨水调pH至7.2）=31.5∶31.5∶37,检测波长276 nm。采用面积归一化法计算利福昔明子宫注入剂的检测限、定量限及其浓度;考察了方法精密度、线性相关性及有关物质专属性,并通过极端条件的破坏、有关物质的含量、分离度等对主成分峰面积降解程度进行了比较。利福昔明子宫注入剂主成分峰在浓度为40~150 μg/mL的范围内,峰面积与浓度呈现良好的线性关系（R²=0.9998）,其有关物质浓度对峰面积线性回归方程为y=23 510x+7 182,其进样精密度RSD为0.13%,方法精密度RSD为0.46%,制剂一定时间内经过强酸、强碱、氧化、高温条件破坏后均有不同程度降解,以破坏前的样品主成分含量为100.00%,氧化破坏和高温破坏主成分降解达13%,酸、碱破坏主成分降解在18%左右,主成分峰保留时间在以上4种条件破坏前后一致,且主成分峰与杂质峰之间及杂质峰与杂质峰之间分离度良好（主成分峰与杂质峰之间分离度均大于1.5,杂质峰与杂质峰之间分离度均大于1.2）。本试验建立的利福昔明子宫注入剂有关物质检测方法操作简便,专属性和重复性好,可适用于利福昔明子宫注入剂有关物质的测定。     

明代文徵明诗画中的茶事空间研究及启示*

以明代文徵明诗画中的茶事空间为议题，研究其特征及动力机制，采取图文互证的方法，总结归纳文徵明茶事空间的特征和其中体现的个人特征。首先，受时代影响，茶事空间在选址上具有“避居山水”的特点，尤其是喜爱临近惠山泉。其次，外部自然环境常被引入室内茶事空间，形成室内外空间一体化。此外，茶事空间受文徵明个人生活品味影响，追求专属性，注重周遭自然环境，且注重园林前导空间以及多空间、多视线的景观叙事空间营造。