交换性阳离子对磷灰石中磷和钙释放的影响

研究了以Ｌｉ~＋、Ｎａ~＋、Ｋ~＋、ＮＨ~＋_４等一价阳离子取代磷灰石表面交换性二价阳离子对磷灰石中磷和钙释放的影响，并就可能涉及的机理进行了探讨．     

电机护环钢在硝酸盐溶液中应力腐蚀开裂的控制过程研究

本文在文献［１］基础上，运用金相，电化学方法研究了５０Ｍｎ１８Ｃｒ４电机护环钢依照ＱＨＪ－７９试验标准在硝酸盐介质中应力腐蚀开裂（即ＳＣＣ）的性质，结果指出，此体系中ＳＣＣ的控制过程为阳极溶解。     

Energy metabolism and apoptotic effect of microwave radiation on rat myocardial cells

AIM: To investigate the effect of microwave radiation at different intensities on the rat myocardium and its possible mechanism.METHODS: The rats were radiated by the intensity of 500, 1 000, 1 500 and 2 000 W/m² with 2 450 MHz microwave for 6 min. The heart tissue was collected 6 h after microwave radiation. ATP and mitochondria complex Ⅳ and Ⅴ were measured. The changes of the tissue structures were observed under transmission electron microscope. The apoptosis of the myocardial cells was detected by a cell analyzer. The protein level of cleaved caspase-3 was determined by Western blotting.RESULTS: The concentration of ATP and activity of mitochondria complex Ⅳand Ⅴ signi-ficantly decreased compared with control group in the cardiac tissues. The decreased number, morphological abnormalities such as dissolved cavitation, matrix and obvious tumefaction of mitochondria were observed under transmission electron microscope. The microwave radiation induced the apoptosis of myocardial cells in the rats. The cell apoptotic rate and the protein level of cleaved caspase-3 increased with increasing intensity of microwave radiation(P<0.05).CONCLUSION: Microwave radiation has obvious injury effect on the rat heart, which can cause cardiac energy metabolism dysregulation and cardiac myocyte apoptosis.     

稻谷热风、微波干燥品质与玻璃化转变研究

以函数拟合、近红外检测及发芽率测定,研究稻谷热风、微波干燥的去水性能及其蛋白质、直链淀粉含量与出芽品质;结合TG/DSC测试,探讨2种热源干燥稻谷的玻璃化转变对其干燥后品质的影响。结果表明:以对数函数拟合稻谷热风、微波干燥去水性能的准确度高;经2种热源干燥稻谷的蛋白质、淀粉含量过程差异不显著;但热风干燥稻谷初期蛋白质含量差异明显。鲜稻谷发芽率显著低于其经热风、微波干燥后的发芽率,三者分别为0.65±0.19、0.93±0.03、0.77±0.02。随含水率降低,经热风、微波干燥稻谷的热重损失与热流则呈不同趋势变化,二者中点温度均减小,综合影响干谷品质。     

微波流态化干燥姜片复水能力和物性分析

针对微波干燥对脱水蔬菜复水能力和应用品质的影响,研究了在单位质量微波功率为0.6、0.9、1.2 W/g的微波流态化干燥(MFD),及在75℃电热鼓风干燥(AD)条件下干燥姜片的复水特性。试验发现,微波干燥姜片的复水能力要弱于热风干燥。随着水浴温度的升高,各组产品的复水能力增加,复水比之间的差距缩小。经动力机械分析仪(DMA)测定复水姜片的蠕变特性,微波流态化干燥所得姜片在复水后的硬度大,在不同微波功率间的差异不明显。通过扫描电子显微镜(SEM)发现,微波流态化干燥姜片的微观结构变化远大于热风干燥。结合干制品的复水和蠕变过程,分析认为姜片组织结构的变化会影响水分的渗透与吸收。复水能力是脱水蔬菜品质的重要指标,改进后的微波-电热鼓风干燥能在保证工作效率的基础上,改善微波干燥产品的复水能力。     

微波磷酸法中密度纤维板厂废料制备活性炭

以中密度纤维板(MDF)厂废料为原料,采用微波辐射磷酸法制备活性炭。探讨了在微波功率900W条件下磷料比、水料比、辐照时间对产品活性炭各项主要指标的影响。得到了试验条件下微波辐射磷酸法制备活性炭的最佳工艺: 磷料比3．5:1,水料比1:1,辐照时间9min。用此工艺制备活性炭产品的得率39．44％,碘吸附值949．08mg／g,亚甲基蓝脱色力10．76mL／0．1g,苯酚吸附值350．25mg／g。本工艺方法为中密度纤维板厂废料的综合利用找到了新的途径。     

灌溉农田土壤湿度的时空变化特征

为了探讨现代土壤墒情监测手段在业务监测实践中的应用方法,利用中国气象科学研究院固城生态与农业气象试验基地的业务和试验资料,对灌溉农田土壤湿度的时间变化特征和空间关系进行了分析。结果表明,灌溉农田的土壤湿度呈一年的周期性变化;浅层(0-50cm)土壤湿度时空波动显著,且各层的变化存在不一致性,60cm以下土层湿度时空变化很小,0-50cm土层的平均土壤湿度能较好地反映0-200cm土层的土壤水分状况,对土壤湿度的监测应集中在浅层50cm内,并需要逐层测量;浅层土壤湿度变异明显,大田中两点各层土壤湿度的相关性一般随两点距离增加而减小,单个测点的土壤湿度测值的代表性差,因此在自动土壤水分仪器布点时,要获得地段的平均土壤湿度信息,必须设置多个观测重复;表层5cm的土壤湿度变化剧烈而迅速,不能正确反映作物根系主要分布层的土壤水分状况,而表层10cm的土壤湿度与作物根系主要分布层的土壤湿度具有很好的联动性,可以较好地反映作物生长的环境土壤水分状况,因此,在应用微波遥感监测土壤墒情时,其对地表的探测深度需要达到10cm以上才能获得关于作物根系主要分布层的土壤水分状况信息,相应地,在土壤墒情微波遥感监测中,需要采用5GHz以下的频率。     

Possible influence of termites (Macrotermes bellicosus) on forms and composition of free sesquioxides in tropical soils

There has been less concern about soil mineralogical alteration than about soil physical, chemical and biological changes induced by termite nest-building activity. Furthermore, much less attention has been paid to free sesquioxides than to phyllosilicate minerals. In the present study, we conducted field morphological observations and selective dissolution analysis to characterize free sesquioxides in termite (Macrotermes bellicosus) mounds as compared with surrounding pedons in different toposequence positions, i.e., seasonally flooded valley bottom, hydromorphic fringe and well-drained upland sites. Distinctive redoximorphic features, such as surface yellowish layers on mound structures from the fringe site, indicate possible alteration of iron sesquioxide forms in the mounds due to the transportation of soil from reductive (aquic subsoil) to oxidative (epigeal mound) environments by the nest-building activity of M. bellicosus. On the other hand, the iron-soluble content in the dithionite-citrate-bicarbonate (DCB) system (Fe_d) was generally higher in the mound structures than at the adjacent sub-surface (Ap2) horizon at each toposequence position, while there was less difference in the content of acid ammonium oxalate (AAO) extractable iron (Fe_o) as compared to Fe_d. As a consequence, the iron activity index (Fe_d/Fe_o ratio) was found for the most part to be lower in the mound structures than in the neighboring Ap2 horizon. In addition, the content of Fe_d, AAO-soluble Al (Al_o) and DCB-extractable Al (Al_d) was significantly correlated with clay content in these soils. These findings suggest that M. bellicosus preferentially collects clay particles, probably from the clay-rich subsoils, such as the argillic horizon, which has been formed by the co-migration of phyllosilicate minerals and relatively crystalline sesquioxides. The species then likely incorporates them into the mounds, which induces an increase in the Fe_d content relative to that of Fe_o, resulting in a decreased iron activity index in the mound structures.     

月季干燥花护形护色的研究

以广州当地红色切花月季为试材,分别采用细沙、硅胶、硅胶+细沙这3种包埋剂,结合高火、中高火、中火这3种微波火力和5个不同干燥时间的试验处理组合,通过分析月季花朵在干燥过程中花色、花瓣质感、花瓣牢固性等指标的变化规律,研究了鲜花干制过程中的保色保形问题.结果表明:包埋剂结合微波处理能有效的降低干燥花花瓣的皱缩程度,提高干花的综合外观品质;其中硅胶+细沙包埋结合微波中高火4min处理的保色保形效果最佳.     

响应面优化黑豆总黄酮微波辅助提取工艺及其抗氧化性能评价

为优化微波提取黑豆总黄酮化合物的工艺,并对其抗氧化性进行初步研究,在单因素试验的基础上,选取液料比、乙醇体积分数和微波功率为自变量,总黄酮得率为响应值的三因素三水平的响应曲面分析法,模拟得到二次多项式回归方程的预测模型。结果表明:提取工艺的最佳条件为功率600 W、液料比40∶1、乙醇体积分数60%,在此条件下,总黄酮得率达到22.1 mg·g~(-1)。抑制油脂过氧化作用的研究结果表明黑豆黄酮是一种天然的抗氧化剂。