用微波加热法测定油料作物种子的水分含量

报道了采用微波加热技术测定大豆等油料作物种子水分含量的新方法。该方法的最适测定条件为：微波功率700W、升温时间8min，标准偏差在0．028％-0．040%之间。本方法具有操作简便、准确快速、节能省时的优点。     

魔芋葡甘聚糖衍生物在烟草保润中的应用研究

为开发新型烟草保润剂,以魔芋葡甘聚糖(KGM)、丙二醇和甘油作对照,进行了魔芋葡甘聚糖改性产物(KSAP)在烟丝中的应用效果对比试验。试验结果显示,在T为22+1℃,RH为(40+2)%时,KSAP溶液的重量减少量最小,为1.119 g,添加KSAP保润剂的样品烟丝最终含水率最高,为10.05%,说明KSAP的保湿性能和在卷烟中的保润效果优于丙二醇和甘油;在T为22+1℃、RH为(90+2)%时,KSAP吸湿率比丙二醇和甘油分别低2.39%和7.54%,说明KSAP兼具防潮的功效。同时红外光谱和扫描电镜的结构分析表明,KSAP为富含—OH和—COO—亲水基团的多网格物理结构的高分子材料。     

MX化合物的红外吸收谱的计算

对MX化合物的红外吸收谱进行了理论计算,由此得出在MX化合物的红外吸收谱中具有红外活性的定域模。     

盐酸浸提法和消煮法测定牧草中钾钙含量的比较研究

以豆科牧草苜蓿为样品,采用盐酸浸提法和消煮法测定牧草中钾、钙含量.结果表明:2种方法绘制的钾标准曲线较为接近,R2分别高达0.990 9、0.992 3.采用盐酸浸提法测得的钾、钙含量平均值(0.55%、2.39%)小于消煮法测得的钾钙含量平均值(0.57%,2.43%);采用盐酸浸提法测得的钾、钙含量标准差(0.02,0.27)大于消煮法测得的标准差(0.01,0.24).经t检验2种方法测得的结果差异不显著.但与消煮法相比,盐酸浸提法具有简便、快速、节约以及环保的特点.     

Mathematic Models for Analysis of Quality Components in Sugarcane Juice with Fourier Transform Near Infrared Spectroscopy

With the technique of Fourier transform near infrared (FT-NIR) spectroscopy, the calibration models for quantitative analysis of sucrose and polarization in sugarcane juice were developed by using transmission mode and calibrating with partial least square (PIS) algorithm. The determination coefficients (R2)of the predicted models for sucrose and polarization in juice were 0. 9980 and 0. 9979 respectively; the root mean square errors of cross validation (RMSECV) were 0. 143 and 0. 155% for sucrose and polarization in juice respectively. The predictive errors measured by FT-NIR were close to those by routine laboratory methods. The results demonstrated that the FT-NIR methods had high accuracy and they were able to replace the routine laboratory analysis. It was also demonstrated that as a rapid and accurate measurement, the FT-NIR technique had potential applications in quality control of mill sugarcane, establishment of payment system based on sugarcane quality, and selection of clones in sugarcane breeding.     

基于GSM及单片机的汽车防盗报警系统设计

介绍了一种基于GSM网络和单片机的远距离汽车防盗报警系统.系统以单片机为控制中心,采用红外传感器实时检测防盗报警信号,然后通过GSM网络以短消息方式将汽车安全情况传送到车主的手机上,车主接收到紧急程度较高的报警信息时,可通过GSM网络发送汽车点火控制信号.     

直膨式太阳能热泵供暖系统运行控制策略

针对直膨式太阳能热泵用于建筑供暖时稳定性差、效率低等问题,该研究基于构建的直膨式太阳能热泵地板辐射供暖试验平台,提出了一种基于环境参数的系统运行控制策略。热泵采用环保工质丙烷,集热/蒸发器和冷凝器均采用微通道结构,通过蓄热水箱与水循环管路相连,将热量输送到地板辐射供暖系统。基于大量试验数据与分析,拟合得到满足室内热舒适前提下不同环境温度下的供水温度下限,根据实际的太阳辐射强度将水箱内部水温提升至相应设定值以满足蓄热需求。试验结果表明：基于所提出的控制策略,系统能够及时响应环境工况变化,在多种工况都能保证较优的性能并满足舒适供暖需求,系统平均性能系数在2.02～3.58之间,压缩机入口工质过热度稳定保持在7～11 ℃,压缩机排气温度保持在90 ℃以内。所提出的运行控制策略有助于直膨式太阳能热泵供暖系统安全稳定高效运行。     

木材对5.43μm红外线的吸收及其穿透规律的研究

根据福建 2 2个主要树种的红外光谱特性 ,选择波长为 5 .43μm远红外辐射作实验 ,获得了反映木材对远红外吸收的实验规律的一个普遍公式 .根据该公式得到了透过率分别为 1 /1 0 0、1 /1 0、 1 /e的穿透深度 ,发现穿透率为 1 /e的穿透深度与细胞腔的尺度同一数量级 ,阐明细胞是吸收远红外辐射的基元的观点     

Chemical composition and microstructure of uroliths associated with the feeding of high-level cottonseed meal diet to sheep

The chemical composition and microstructure of five urolith samples (4 bladder stones and one kidney stone) associated with the feeding of high level of cottonseed meal (CSM) diet to Chinese merino fine wool sheep (Junken breed, Xinjiang) were examined by optical microscope, X-ray diffraction, X-ray energy dispersive spectrometry (EDS), scanning electron microscopy (SEM), and infrared spectroscopy analysis. The bladder stone samples appeared yellow or white, small powder and loose mass, and as finely granular under the optical microscope. However, the kidney stone samples from a experimental sheep were found as small brown mass, higher hardness, and as a cracklike structure. Oxygen, phosphorus, potassium and magnesium were found as four major elements in these uroliths by X-ray energy dispersive spectrometry (EDS). Potassium magnesium phosphate (MgKPO₄) and potassium magnesium phosphate hexahydrate (MgKPO₄·6H₂O) were major components in the bladder stones, while less magnesium ammonium phosphate hexahydrate (MgNH₄PO₄·6H₂O) examined by X-ray diffraction and infrared spectroscopy analysis. However, the newly found prismatic crystals, which were rich in magnesium and pyrophosphate, were identified as magnesium pyrophosphate (Mg₂P₂O₇) in the kidney stone. The bladder stone samples appeared irregular mass and balls, cracked under SEM with low magnification, while appeared cracked, irregular layer-like, honeycomb-like or tiny balls under high magnification. The kidney stone samples were observed as cone, irregular block or layered crystal structures.     

贮木场木材剩余物阴燃过程研究

以木材剩余物构成阴燃床的燃烧材料,在阴燃实验装置中进行阴燃传播实验,利用热电偶测量阴燃传播速度,采用气相色谱仪检测阴燃特征气体组份.并分析了阴燃方式、空气流速和加热功率对阴燃传播过程的影响.研究结果表明:阴燃的传播速度随着氧气浓度、空气流速、加热功率的增加而提高,阴燃初期主要特征气体为CO<,2>和CO,氧气浓度是控制阴燃向有焰燃烧的关键参数,逆向阴燃在向有焰燃烧转变时需要的氧气浓度高于同向阴燃.