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101.
102.
David E. Barnekow Stephen M. Brown Sandra L. Byrne Arlene W. Hamburg Mike A. Huskin Andrea M. Leisure 《Pest management science》1995,43(3):211-219
The metabolism of cis- and trans-1,3-dichloropropene (1,3-D) was studied in soybean plants grown in soil treated 24 days prior to planting with [U-14C]E- and Z-1,3-dichloropropene at 380 liters ha?1. Isolation and identification of the 14C residue from soybean plants at 84 days (forage) and 176 days (mature) after application showed that no 1,3-dichloropropene or its putative metabolites, 3-chloroallyl alcohol and 3-chloroacrylic acid, could be detected in any of the tissues. The components of the 14C residue included major plant constituents (i.e. fatty acids, protein, pigments, organic acids, sucrose and other carbohydrates, and lignin). 相似文献
103.
A series of isothiocyanates (R-NCS, R, 1–6 carbon atoms) was applied in the vapour phase to wheat in sealed containers. The speed of sorption, as measured by the rate of loss from the intergranular air space, was inversely proportional to molecular weight; e.g. the time for 50% sorption of hexyl isothiocyanate was over 100 times longer than for the methyl analogue. Despite extensive sorption, most of the applied chemicals was recovered from the fumigated wheat seven days after dosing, indicating that sorption did not lead to extensive degradation. Purge and trap techniques proved suitable for recovery of low-boiling, but not high-boiling chemicals. 相似文献
104.
Although it is well known that judicious use of adjuvants can increase the performance of foliage-applied sprays of many agrochemicals, little information is available in the public domain about their ultimate effects on pesticide residues in treated crops. In the present work, the influence of Agral (polyoxyethylene nonylphenols), Toil (methyl esters of rapeseed fatty acids) and Bond (styrene-butadiene copolymers) on surface and crop residues of diclofop-methyl/diclofop and propiconazole in wheat and field beans was investigated using a model system simulating field practice. Pesticides were applied as commercial formulations, diclofop-methyl 378 g litre(-1) EC (Hoegrass) and propiconazole 250 g litre(-1) EC (Tilt), at their maximum approved rates, 1135 g AI ha(-1) and 125 g AI ha(-1), respectively, both in the presence or absence of the maximum rate recommended for each candidate adjuvant. No detectable residues of diclofop-methyl or propiconazole were found in wheat 35 days after any of the four applications. However, residues of diclofop were present in this crop, and those from applications containing Agral (0.07 mg kg(-1) fresh weight (FW)) or Bond (0.08 mg kg(-1) FW) were significantly lower than those with no adjuvant (0.14 mg kg(-1) FW) or Toil (0.16 mg kg(-1) FW). Unlike wheat, residues of both diclofop and propiconazole were detected in field beans after harvest. Significantly higher residues of the former were recorded from the applications with Agral or Bond (ca 0.32 mg kg(-1) FW) than with those with no adjuvant or Toil (ca 0.15mg kg(-1) FW). All the propiconazole applications containing adjuvants showed a similar significant increase in residues (0.10-0.16 mg AI kg(-1) FW) over the no-adjuvant treatment (0.05 mg kg(-1) FW) in this crop. There appeared to be little agreement between the apparent amounts of uptake, as indicated by the rates of decline of surface residues up to 5 days after application, and final residues in either target species. On wheat, surface residues of diclofop-methyl decreased from initially ca 20 to as little as 0.02 mg kg(-1) FW using adjuvants; the corresponding values for propiconazole were ca 2 to ca 0.03 mg kg(-1) FW. Recoveries of diclofop-methyl from the surfaces of field beans were much higher than those from wheat, declining from ca 30 to only ca 6 mg kg(-1) FW during the course of 5 days; the corresponding residues for propiconazole were ca 2 mg to 0.15 mg kg(-1) FW. These findings are discussed in relation to uptake results obtained with radiolabelled pesticides and adjuvants in the laboratory, and to the mandatory requirements for pesticide residue data for the authorised use of adjuvants in the UK. 相似文献
105.
Antonious GF 《Pest management science》2002,58(1):85-91
The efficacy of esfenvalerate (84 g litre-1 EC; Asana XL) at 7.0 g AI ha-1 on broccoli was tested against the flea beetle, Phyllotreta cruciferae Goeze (Chrysomelidae: Coleoptera) and the imported cabbage worm, Pieris rapae L (Pieridae: Lepidoptera) under field conditions. Insect populations were monitored before and after treatment. Periodic sweep-net collections and examination of the leaves in treated and untreated broccoli plots revealed mean reductions of P cruciferae levels of nearly 98% 1 week post-application compared with untreated plots. The residual toxicity of esfenvalerate was also effective for 2 weeks in reducing population density of P rapae by 69% on broccoli leaves. The impact of esfenvalerate on feeding damage to broccoli leaves was established by counting the number of feeding holes made by P cruciferae on spring broccoli and P rapae on fall broccoli. As the leaf area ingested increased, a linear relationship was seen between the number of holes and number of insects. Results indicated that forage destruction by the two pests was significantly reduced by esfenvalerate application. Esfenvalerate was extracted from broccoli at 1 h and 1, 3, 7, 10, and 14 days post-application for residue analysis. Residues on spring broccoli were 12.2, 5.2 and 2.9 micrograms cm-2 on the leaves and 0.13, 0.05 and 0.02 microgram g-1 on the heads at 1 h, 1 and 3 days, respectively. Only trace levels (0.001 microgram g-1) were detected in/on the heads 14 days after spraying. On the basis of half-life (T1/2) values, persistence of esfenvalerate on spring broccoli leaves (T1/2 = 1 day) was shorter than on fall broccoli (T1/2 = 1.6 days). T1/2 values were 2.1 and 3.6 days on spring and fall broccoli heads, respectively. The implications of these residue levels on re-entry times into treated fields are discussed. 相似文献
106.
论述和分析木质剩余物复合材料老化的原因,主要有木质剩余物的老化、胶粘剂的老化、木质剩余物的回弹和膨胀—收缩应力。综合论述木质剩余物复合材料加速老化试验方法,指出木质剩余物复合材料在加速老化试验方面的研究,适宜采用ASTM D1037六循环加速老化法和老化仪检侧法。分析木质剩余物复合材料老化的影响因素,如温度、湿度、试件尺寸等。 相似文献
107.
108.
为了建立同时测定猪粪便中二甲氧苄啶、磺胺对甲氧嘧啶、恩诺沙星、金霉素、泰乐菌素5种兽药残留量的超高效液相色谱-串联质谱(UPLC-MS/MS)分析方法,样品经McIllvaineNa_2EDTA缓冲溶液提取,C18粉吸附杂质,HLB固相萃取小柱净化,浓缩富集后用0.1%甲酸甲醇溶液复溶,过滤上机,基质液外标法定量。结果显示,5种兽药在10~500μg/kg的质量浓度范围内线性良好,在添加浓度50~500μg/kg,平均回收率为53%~85%,RSD为1.87%~18.81%。该方法具有较好的准确度与精密度,能快速、准确测定猪粪便中5种兽药残留,为养殖环节实时监测兽药使用情况提供了技术支持。 相似文献
109.
兽药残留检测技术应用现状及发展方向 总被引:1,自引:0,他引:1
概述了畜禽产品中兽药残留的“快速筛查方法”和“确证检测方法”,分别介绍了各种检测方法的特点和应用现状,并对兽药残留检测技术在未来的研究方向进行了展望,为研究更高效的检测方法提供参考,进而推动畜禽产品质量安全监管工作,保障畜禽产品质量安全。 相似文献
110.
指出了随着生活水平的提高,食品安全已逐渐成为人们普遍关注的一个社会热点问题,尤其是肉、乳品、蛋和水产品等动物性食品的安全引起了社会普遍关注。概述了兽药的概念及分类、兽药残留的危害、兽药残留现状及原因和我国兽药管理方面的法规标准等。 相似文献