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本文对茶叶中7种有机氯类和拟除虫菊酯类农药残留检测的前处理技术进行了研究,对比了2种不同的提取溶剂对农药回收率、净化效果的影响,建立了丙酮∶正己烷(1∶1,V/V)提取,Florisil固相萃取小柱净化的方法。本方法回收率在82.3~109.8%之间,变异系数3.3~10.22%,最低检出浓度为0.001mg/kg。该种残留分析前处理方法具有操作简便、成本低、回收率高、精密度好的特点。 相似文献
123.
不同施肥配比对宁夏盐碱土壤油用向日葵产量的影响 总被引:1,自引:0,他引:1
研究了不同施肥配比对宁夏盐碱土壤向日葵产量的影响,建立了一元二次肥料效应函数方程.结果表明:对碱化土壤施氮量达到10.56 kg/667m2时,产量达到最大值183.2 kg/667m2;当施磷量达到5.71 kg/667m2时,产量达到最大值156.9 kg/667m2;最高产量施肥配方氮磷钾配比为10.56∶5.7... 相似文献
124.
作为玉米生产加工过程的农业废弃物,玉米芯的产量巨大,生物质气化工业利用玉米芯原料制备生物质燃气的过程中将产生大量的玉米芯灰。为了全面认识这些废弃玉米芯灰的灰特性及可能的应用,通过激光粒度分析、X射线荧光(X-ray fluorescence,XRF)、X射线衍射(X-ray diffraction,XRD)、热重和差热分析(thermal gravimetric and differential thermal analysis,TG-DTA)、扫描电镜(scanning electron microscopy,SEM)、能谱分析(energy dispersive X-ray,EDX)等方法对其进行深入研究。结果表明:玉米芯灰的粒度较小且分布不均,平均粒径为12.96μm;灰的元素组成中K和Si所占的比重最大;富含K、Ca、S和Cl等元素使玉米芯灰可用作土壤改良剂,而且灰中大量的Si O2和Al2O3使其可以用来制备抗压强度较高的水泥混凝土;灰中存在多种含钾元素的KHCO3、KAl Si O4、KAl Si2O6、KCl和K2SO4等结晶相矿物成分;灰粒的形状极不规则,树枝状的团聚灰渣具有丰富的空隙,易逐级吸附小颗粒,灰粒表面存在大量弱粘结的絮状物,断面多为孔状结构;熔融灰粒表面存在富钾现象,且多以KCl形式存在;飞灰的热解具有分段机制,加热到1 200℃时,其总失重和最大失重速率均随着氧气浓度的升高而增加;氮气中620℃的吸热峰是由KCl熔融吸热所致,而有氧气氛中在630℃处的放热峰则是未燃尽的残碳继续燃烧或有机物分解放热所致。 相似文献
125.
Walter E. Riedell 《Journal of plant nutrition》2016,39(14):2115-2125
Ion inclusion or ion exclusion are the two main strategies developed by plants to tolerate saline environments. Shoot sodium (Na+), potassium (K+), and calcium (Ca2+) in four perennial grass species (tall wheatgrass, Nuttall's alkaligrass, creeping foxtail, and switchgrass) treated with nutrient solution salinity levels ranging from 2 to 32 dS m?1 were measured. As the nutrient solution salinity was increased from 2 to 10 dS m?1, tall wheatgrass, creeping foxtail and Nuttall's alkali grass had increased shoot Na+ and decreased Ca2+ concentration while maintaining growth suggesting that these species tolerated these changes in shoot ion concentration. In contrast, switchgrass excluded Na+ from the shoot and maintained K+ and Ca2+ concentrations but suffered dramatic shoot dry weight reduction. Thus, the Na+ exclusion mechanisms present in switchgrass were less efficient in maintaining growth under the 10 dS m?1 nutrient solution treatment than the Na+ inclusion mechanisms used by the other three species. 相似文献
126.
Fang You Ram Dalal David Mulligan 《Communications in Soil Science and Plant Analysis》2015,46(4):375-389
The present study aims to evaluate carbon recovery and analytical precision of two methods based on dry combustion for organic carbon (OC) quantification in base metal mine tailings: (1) IC subtraction method (inorganic C(IC) measured and subtracted from total C) and (2) direct OC quantification after acid pretreatment. Results showed IC subtraction method effectively hydrolyzed a range of IC minerals [calcium carbonate (CaCO3), magnesium carbonate (MgCO3), dolomite, magnesite, calcite] with satisfactory IC (as CO2 released) recovery (87–103 percent). In the direct OC quantification method, 5 M hydrochloric acid (HCl) pretreatment resulted in a satisfactory recovery (76–92 percent) of most organic compounds [ethylenediaminetetraacetic acid (EDTA), cellulose, plant litter, and charcoal], except for water-soluble OC (sucrose, 40 percent recovery). The precision of both methods declined when C levels were <5 g kg?1 with RSD (Relative Standard Deviation) > 10 percent. The OC values in test samples of base metal mine tailings were comparable between the two methods. However, IC subtraction method is not applicable for tailings with low OC levels (<5 g kg?1) until the precision is substantially improved. Moreover, compared to the IC subtraction method, OC values are significantly lower in direct OC quantification method for tailings with high OC levels. 相似文献
127.
The aim of this study was to evaluate the physiological responses of Leymus chinensis (Trin.) Tzvel exposed to long-term salt, salt-alkali, and alkali stress in order to elucidate how L. chinensis can survive under alkaline-sodic soils. L. chinensis (30 days after germination) were stressed with salt [SS; sodium chloride (NaCl)], mixed salt-alkali [MS; molar ratio of NaCl: sodium carbonate (Na2CO3) = 2:1] and alkali salt (AS; Na2CO3) at four different levels of sodium (Na+) concentration (0, 75, 150, and 300 mM) for 60 days. L. chinensis showed 100% survival rate at all treatments except 300 mM SS (33.3%) and AS (18.9%). The growth and physiological parameters of survival plants were measured. As anticipated, growth of L. chinensis was inhibited after stresses, which reflected in the decline of plant height, dry weight and tiller number following the increased Na+ concentration. The content of Na+, proline, and soluble sugar in L. chinensis increased with the increasing Na+ concentration, suggesting that L. chinensis need to accumulate inorganic and organic solutes for resisting osmotic stress induced by various salt stresses. These processes ensure the water balance that can provide a relative normal physiological environment for L. chinensis. Potassium (K+) content of L. chinensis kept at a relative lower level than control to ensure the normal physiological processes. Chlorophyll content of stressed plant increased slightly compared to control plants, which can produce more energy for L. chinensis resisting various stresses. The increased malondialdehyde (MDA) content of stressed plants showed the damage of various stresses. Among the three treatments (SS, MS, and AS), the injury extent for L. chinensis can be expressed by AS>SS>MS, and MS was the most complicated for the counterbalance effects of soil electrical conduction and pH. 相似文献
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129.
磷素营养对星星草幼苗抗碱性的影响 总被引:2,自引:0,他引:2
通过以不同水平磷素营养培养星星草幼苗,研究磷素营养对星星草幼苗抗碱性的影响,试验结果表明:在2.0%Na2CO2胁迫下星星草苗磷素营养的最适浓度为2.8mmol·L^-1KH2PO4,此条件下仅对株高,干重和鲜重的增长有促进作用,而且受害程度最小,对Na2CO3胁迫的缓解作用最强,在一定程度上可提高星星草幼苗对Na2CO3胁迫的抗性。 相似文献
130.