SH—E型射频原油含水分析仪的在线测定

原油交接点的含水测定，目前大部分沿用手工法和蒸馏法，２ｈ采样，４ｈ人工化验，采样不具有代表性，化验方法带有人为干扰。为了克服上述缺点，中国计量科学研究院研制了ＳＨ－Ｅ型射频原油含水分析仪，实现了原油含水量在线连续测定，瞬时显示，２ｈ取平均值打印，基本上排除了人为因素的干扰，使测出的原油含水率具有代表性。射频原油含水分析仪由射频法含水率测量传感器和以Ｚ８０单板机为核心的信号分析仪组成。射频法测量原油     

TEOM1405F型PM2.5颗粒物分析仪校准方法的建立

对美国赛默飞世尔公司TEOM1405F颗粒物分析仪制定合理可行的校准方法,并且根据标准方法对仪器进行检定.校准结果为:环境温度传感器误差小于±2℃,环境气压传感器误差小于1 kPa,采样流量相对误差小于±3％,弹性常数K0＜±2％,绝缘阻抗＞20MΩ,满足校准方法技术要求.根据检定结果,该仪器监测数据准确可靠.     

氮磷调控及紫云英配施提高早稻冠层特性和产量

为揭示不同氮、磷施用量及配合翻压适量紫云英入田对早稻冠层特性和产量的影响,在7个施氮、3个施磷及2个不施氮/磷水平下,开展早稻全生育期叶面积指数LAI、冠层光合有效辐射PAR传输特性、叶片叶绿素SPAD值、生育后期剑叶净光合速率Pn及产量的试验观测。结果表明,氮磷调控可显著影响早稻LAI、叶片叶绿素含量和叶片光合速率,进而通过调节LAI影响冠层PAR传输特性,最终表现为产量上的差异。缺氮对早稻的影响显著高于缺磷,但在施肥充足时,磷肥对产量的影响比氮肥更加显著。早稻冠层特性和产量随氮、磷施用量的增加表现出边际递减效应,当施用量超过某一值时出现拐点,最终表现为产量的下降。在赣抚平原灌区,187.5~225 kg/hm2施氮量和60~120 kg/hm2施磷量以及翻压15 000 kg/hm2紫云英鲜草入田可有效提高早稻LAI和冠层PAR截获率In以及叶片叶绿素含量,维持剑叶生长期内较高的净光合速率Pn,获得高产。     

Neutrophilic myeloperoxidase index and mean light absorbance in neonatal septic and nonseptic foals

Background: Two neutrophilic indices reported by the ADVIA 120 Hematology Analyzer, neutrophilic myeloperoxidase index (MPXI), and mean light absorbance (neutrophil X mean [NXM]) have been proposed as indicators of systemic inflammatory disease in horses and of neutrophil activation in coronary ischemic syndromes in people. Objective: The aim of this study was to evaluate NXM and MPXI in healthy, sick nonseptic, and sick septic foals to determine whether conditions likely associated with neutrophil activation result in decreases in these variables. Methods: In this retrospective study, CBC data from 61 neonatal foals presented to the Equine Teaching Hospital of Barcelona were evaluated for correlations between MPXI, NXM, percentage of large unstained cells, neutrophil count, and percentage of band neutrophils. Results obtained in septic (n=32), sick nonseptic (n=22), and healthy foals (n=7) were compared. In addition, results recorded in septic/neutropenic (n=12), septic/non‐neutropenic (n=20), nonseptic/neutropenic (n=8), nonseptic/non‐neutropenic (n=14), and healthy foals (n=7) were also compared. Results: A weak negative correlation was found between MPXI and neutrophil count and between NXM and percentage of band neutrophils. Septic/neutropenic foals had significantly higher MPXI values (median 17.9, minimum–maximum 4.7–42.5) than did septic/non‐neutropenic (1.5, ?24.4 to 22.3), nonseptic/neutropenic (6.6, 0.6–17.9), and nonseptic/non‐neutropenic foals (8.8, ?10.1 to 16.8) but did not differ significantly from controls (12.8, ?8.5 to 20.4). Conclusions: Significant differences in NXM or MPXI were not found when disease groups were compared with controls; however, septic/neutropenic foals had significantly higher median MPXI than other groups of sick foals. Further prospective studies are needed to clarify if this finding is related to decreased neutrophil function or activation in septic/neutropenic foals.     

Clinical hematology practices at veterinary teaching hospitals and private diagnostic laboratories

The clinical hematology practices utilized at veterinary teaching hospitals and private veterinary diagnostic laboratories were surveyed using a questionnaire. The hematology caseload at private diagnostic laboratories was larger, and comprised predominantly of canine and feline submissions. The Coulter S Plus IV and Serono Baker 9000 were the hematology analyzers used most frequently at veterinary medical laboratories. The Abbott Cell-Dyn 3500, a multispecies analyzer capable of leukocyte differential counting, was utilized more by private laboratories. Commercial hematology control reagents were used at all laboratories; teaching hospital laboratories more often used reagents supplied by the manufacturer of the analyzer. A greater percentage of private diagnostic laboratories participated in the external quality assurance programs offered by Veterinary Laboratory Association and College of American Pathologists. While private diagnostic laboratories retained the EDTA blood specimens longer after initial testing, the teaching hospital laboratories retained blood smears and complete blood count reports longer. The complete blood count reports at veterinary teaching laboratories more often included red blood cell volume distribution width, mean platelet volume, manual hematocrit, plasma protein, and leukocyte differentials as absolute concentrations. The laboratory practices utilized by these veterinary medical laboratories were generally similar, and differences were attributed to divergent emphasis on economic accountability and clinical investigation.     

农田灌溉水中挥发酚的流动分析-分光光度分析法的建立

主要通过使用流动分析仪对农田灌溉水中的挥发酚进行测定，有效地提高了检测的精密度与准确度。相比传统分光光度计检测法，此法更方便和快捷，大大降低了样品的使用量，节省了人力物力，较好地满足了批量样品测定的要求，值得大力推广和应用。     

同时蒸馏萃取-GC/MS法分析檵木与红花檵木叶挥发油成分

[目的]分析比较檵木和红花檵木叶片挥发油的成分,为进一步开发利用积累数据。[方法]采用同时蒸馏萃取提取檵木叶、红花檵木绿叶和红花檵木红叶的挥发性成分,用气相色谱-质谱联用技术对其进行分离鉴定。[结果]在3种叶片中分别分离出44、55、36种成分,分别鉴定出25、21、23种成分,已确定组分分别占总峰面积的74.11%、83.94%、76.88%。含量较多的组分有：顺-3-己烯-1-醇（38.79%、12.73%、30.47%）、棕榈酸（5.31%、17.47%、6.02%）、硬脂酸（1.99%、5.03%、2.55%）油酸（2.63%、33.31%、9.13%）。[结论]其主要成分在医药卫生、香料、食品添加剂和抗菌杀虫剂等领域有很好的开发前景。     

自动定氮仪碱解蒸馏法测定土壤中水解性氮含量

介绍了自动定氮仪碱解蒸馏法测定土壤中水解性氮含量的方法,探讨了试验中主要影响因素。与现行林业行业标准碱解扩散法相比,该方法具有操作简便、快捷、干扰小、精度高、准确性好的优点,特别适合大批量样品的分析。值得在土壤分析工作中参考应用。     

Clinical evaluation of the CA530-VET hematology analyzer for use in veterinary practice

BACKGROUND: The CA530-VET is a completely automated impedance cell hematology analyzer, which yields a 16-parameter blood count including a 3-part leukocyte differential. OBJECTIVES: The aim of this study was to examine the operational potential of the CA530-VET and its value for use in veterinary practice. METHODS: The analyzer was tested for blood carry-over, precision, and accuracy. Comparison methods included the CELL-DYN 3500, microhematocrit centrifugation, manual platelet (PLT) counting for feline and equine species, and a 100-cell manual WBC differential. Blood samples for comparison of the methods were obtained from 242 dogs, 166 cats, and 144 horses. RESULTS: The carry-over ratio (K) was 0.28% for RBC, 0.59% for PLT, 0.32% for WBC, and 0.18% for hemoglobin (HGB) concentration. Coefficients of variation (CVs) for within-batch precision and duplicate measurement of blood samples were clearly within the required limits, except for duplicate platelet counts in cats (8.7%) and horses (9.5%). The WBC count was in excellent agreement for dogs and horses and RBC count was in excellent agreement for horses. The accuracy of feline WBC counts was not acceptable, with the exception of values at the high end of the range. RBC counts in dogs and cats, and HGB concentration and MCV in all 3 species were sufficiently accurate. The CA530-VET HCT results were in excellent agreement with microhematocrit results in horses but exceeded the maximum allowed inaccuracy for cats and dogs. In all species, PLT counts established mechanically and manually were not in adequate agreement. Large differences were found between the CA530-VET and the manual differential percentage for lymphocytes and "mid-sized cells" (monocytes and basophilic granulocytes). CONCLUSIONS: The CA530-VET can be considered useful for routine canine, feline, and equine blood cell analyses. It should not be considered accurate, however, for PLT counts, feline total WBC counts in the subnormal and normal range, and leukocyte differentials, except for granulocytes.