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41.
42.
为了建立宫衣净酊中葛根素的高效液相色谱(HPLC)测定方法,应用色谱柱为安捷伦Eclipse XDB-C18(4.6mm×250mm,5μm),流动相为甲醇-水(25∶75),流速为1mL/min,检测波长为250nm,柱温为30℃。结果表明,在此色谱条件下,葛根素的线性范围为18.25μg/mL~584.00μg/mL(r=0.999 9,n=6),平均回收率为108.83%(RSD=1.03%)。说明本方法简便、准确、重现性好,可以作为宫衣净酊的质量控制方法。 相似文献
43.
于2017—2018年和2018—2019年,在西北中部旱作雨养农业区以冬小麦‘康庄974’为试验材料,设秸秆带状覆盖(SM)、地膜覆盖(PM)和无覆盖对照(CK)共3个栽培处理,分析不同覆盖方式对小麦灌浆期土壤水分和温度及抗氧化能力的影响,探讨花后干物质积累量和粒重形成的关系。结果表明,随生育期推进,花后旗叶相对含水量(RWC)逐渐降低,丙二醛(MDA)含量逐渐升高,且PM较SM降、升幅度明显。与CK相比,覆盖显著提高花后旗叶抗氧化酶活性,增加渗透调节物质含量;开花时间越长,SM抗氧化酶活性升高的幅度越大,而PM主要提高花后7 d旗叶抗氧化能力。SM和PM的粒重分别较CK增加14.3%和19.1%(P<0.05)。相关分析表明,土壤水分(SW)是影响旗叶生理活性的关键因子,提高SW,有利于增加RWC(r=0.84**),从而提高旗叶抗氧化能力,其中RWC和抗坏血酸酶(ASA)活性呈极显著正相关关系(r=0.82**);ASA活性和脯氨酸(Pro)含量呈极显著正相关关系(r=0.94**),和MDA含量呈极显著负相... 相似文献
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45.
三氯蔗糖在食品加工中的应用及测定方法的研究概况 总被引:1,自引:0,他引:1
施雅梅 《农产品加工.学刊》2007,(12):80-82
介绍了三氯蔗糖的特性。阐述了三氯蔗糖在食品加工中的应用及测定方法的研究概况。 相似文献
46.
At present 18 wastewater treatment plants operateing in the Small towns of Three Gorge Areas of Chongqing Municipality, producing 132.95 tons surplus sludge everyday. As regards to the disposition of such numerous surplus sludge, the major disposition technique in these wastewater water treatment plants, i. e. , thickening and mechanical dewatering technique followed by feeding into the municipal solid waste landfill, seems to have a rather bad effect on the normal operation of the municipal solid waste landfill, due to the unstabilized sludge resulted from this technique of the sludge disposition and high moisture in the sludge, which is higher than 80%. This paper has paid some attention to this phenomenon. With respect to the small towns having the the municipal solid waste landfill, the techniques of mechanical dewatering, calcareousness stabilized etc. before feeding into the municipal solid waste landfill, seem to be feasible, while the composting and comprehensive utilization of sludge is available in the small towns which have no municipal solid waste landfills. 相似文献
47.
The following details are discussed in the present paper, after high titanium slag and H3PO4 is put in the closed system,the .reaction takes place under controlled temperature conditions, and the gas produced is collected. The two phases of gas liquid attain kinetic equilibrium, ihe gas above the liquid is used to make GC analysis with the aid of chromatographic column of 5A molecular sieve, TCD and N2 30ml/min. Satisfactory quantitative results can be achieved with simple instruments and uncomplicated operation technique. 相似文献
48.
In the course of searching immunodulators from natural herbal sources,the polysaccharide has been isolated from the water extract of duckweed(Herba Spirodelae seu Lemnae).The authors aim at investigating the methods that determine the content of total saccharides in the mixture,accordingly,to be used as a quality control in the procedure of producing polysaccharides from duckweed.The contents of saccharides in the extraction were mensurated by spertrophotometry of sulphuric acid-phenol and sulphuric acid-anthrone.And the validitiy of methods was evaluated through some indexes such as linearity and range,precision,stability,and accuracy.The results reveal the methods are convenient,rapid,accurate,and high sensitive,thereby leading to a wide and effective use in determining the saccharides contents in polysaccharides extraction from Herba Spirodelae seu Lemnae. 相似文献
49.
The author introduces a method and experimental procedures that determine dn/dc,molecular weight and its distribution of the hyroxyethyl starch(HES) by means of Gel Permeation Chromatography-Refractive index-Multi-angle laser light scattering detection(GPC-RI-MALLS)techniques.The key experimental technique and results are discussed.The method takes CH3COOH/CH3COONa as mobile phase and solvent.The experiment gets satisfactory results.It can be used as a routine method to determine the hyroxyethyl starch(HES) molecular weight and its distribution. 相似文献
50.
Chen Qigao Feng Ya 《保鲜与加工》1993,(1)
This paper analyses the thermal moist characteristics of the hull layer beside an air layer at lower temperature in an envelope for a cold storage and presents a new method of waterproof by air layer. With test data from engineering practice, the theory on the barrier of self moisture proof at the surface sublayer of the hull layer in an attic on a cold storage is proven. The dried zone about three phase point is confirmed. It is a new knowledge for thermophysics on thermal design of a cold storage with an optimum thermal performance. 相似文献