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901.
A H Wu T Rotunno H V Malmstadt 《Journal of the Association of Official Analytical Chemists》1979,62(5):969-975
The determination of protein nitrogen in feeds and wheat by microcomputer controlled titration is described. The method involves direct titration of ammonia with standard hypochlorite titrant in the presence of bromide. The titrant is delivered by an automatic buret, and the microcomputer controlled, automatically computed potentiometric end points are precise to 0.1% over a 5-fold concentration range of nitrogen. Digestions performed with both mercury and copper catalysts show comparable results. Samples are weighed before digestion by an electronic balance interfaced to the computer which records sample number and weight. An automatic pipet aliquots, dilutes, and buffers samples directly from the digestion tubes; the samples can be immediately titrated with the automatic titrator. The results for protein in NBS standards and check feed samples from an offical testing program compare closely with average values reported for these standards. Results show that feed and wheat samples contained 10-100% protein. Precision for successive aliquots of the same digests is 0.1-0.4%relative standard deviation; precision for multiple digestions of the same sample is 0.1-0.8%. 相似文献
902.
Three groups of anions were distinguished in order of effectiveness with respect to the dispersion and flocculation of soil samples treated with Fe(III) polycations: phosphate and fulvate citrate, oxalate, silicate and tartrate and salicylate, catechol, aspartate, lactate and acetate. This was also the order of the amount of anion adsorbed by the soil. The addition of phosphate and fulvate to soil samples with a net charge of zero lowered the zero point of charge producing particles with a net negative charge. This increased the amount of dispersible clay present from 0 to 9% by weight of soil. The sorption of phosphate and fulvate by soil samples with a net positive charge reduced the zero point of charge and caused flocculation of dispersed clay. Electrophoretic and electron microscopic studies confirmed the dispersion-flocculation phenomena.Treatments which produced dispersed clay led to increased bulk densities, plastic limits and moduli of rupture but lower porosities, water holding capacities and hydraulic conductivities. The sorption of anions on soil samples with a net charge of zero reduced friability. 相似文献
903.
Changes in soil properties and yield response in relation to tillage and residue management treatments in an irrigated groundnut (Arachis hypogea L.)—wheat (Triticum aestivum, L.) rotation on a sandy soil (1972–1974) and on a sandy loam soil (1974–1976) were evaluated. Tillage treatments (T1 and T2) did not cause significant changes in soil properties. Incorporation of crop residues (5 t residue per ha per crop, T3) caused a substantial increase in organic C, available N, and NaHCO3 -extractable P contents in the top 15 cm of both soils. Residue management treatments (T3, T4 and T5) showed no significant effect on soil bulk density and exchangeable K. Crop yields under no-tillage (T1) and conventional tillage (control, T2) were comparable on sandy soil but on the sandy loam soil, no-tillage yielded significantly lower than conventional tillage. Compared with the control, incorporation of crop residues (T3) caused higher yields on sandy soil for groundnut and wheat by 34.1 and 47.4%, respectively, and on sandy loam by 17.1 and 7.2%, respectively. Mulching with crop residues conserved soil moisture and reduced maximum soil temperature (1.5–5.3°C in groundnut and 1.5–2.9°C in wheat) but other measured soil properties were not significantly affected. Significant yield increase due to residue mulching (T4) was observed in sandy soil but it was significantly less than when total crop residue was incorporated (T3). Increased wheat root-weight density in the top 15 cm soil with residue mulching was not reflected in grain yield. Compared with the incorporation of the total amount of crop residue (T3), incorporation of half the amount and application of the other half as mulch (T5) caused lower yields — on sandy soil for groundnut and wheat by 31.5 and 15.7%, respectively, and on sandy loam by 4.8 and 3.6%, respectively. 相似文献
904.
The oxidation-reduction regimes of some Oxisols of tropical China were investigated on the basis of the Eh values and the amounts of reducing substances, both measured by newly devised methods. The Eh values in the surface layers of soil profiles under natural forest and commercial forest were 400–550 mV, lower by 100–200 mV than the deeper horizons. The concentrations of reducing substances in the surface layers corresponded to 0.5–5.0 · 10?5M of Mn2+. In the cultivated layer of a submerged paddy soil the concentration of reducing substances was as high as 13·10?5M, with an Eh value of less than 100 mV. There was a negative correlation between the Eh value and the logarithm of the concentration of reducing substances, showing that the intensity aspect and the capacity aspect of the oxidation-reduction status of a soil are closely interrelated. 相似文献
905.
M Yamamoto M Ishikawa T Masui H Nakazawa Y Kabasawa 《Journal of the Association of Official Analytical Chemists》1985,68(3):493-494
A simple and rapid liquid chromatographic method is described for the determination of barbaloin (aloin, 10-D-glucopyranosyl-1,8-dihydroxy-3-(hydroxymethyl)-9(10H)-anthraceno ne) in foods. Barbaloin is extracted with water from foods containing aloe and the extract is cleaned up on a disposable cartridge by using methanol-water (55 + 45) as eluant. The eluted barbaloin is separated by liquid chromatography on a YMC A-302 column with methanol-water (50 + 50) mobile phase, and detected at 293 nm. Recoveries of barbaloin added to foods at the levels of 0.05 and 0.50 mg/g were 94.4-100%. Assay results for commercial food samples indicated that the present method is applicable to a variety of foods supplemented with aloe. 相似文献
906.
This study highlights the previously expressed concerns of soil researchers who have indicated that compaction pressures or stresses in the deeper layers of soil are determined by the amount of surface load. Modifications of Boussinesq theory by Froelich and further modification of Froelich's equations by Soehne were used to predict and develop graphical relationships for maximum allowable loads and/or mean surface contact pressures beneath loaded farm machinery tyres. Vertical compressive stresses at different subsoil depths were calculated and design loads for a currently used high flotation tyre were examined for comparative purposes. For highly compactible soils the results indicate that mean surface contact pressures should not exceed maximum allowable stresses in the subsoil for individual wheel loads which exceed approximately 30 kN. Thus, it appears that future designs based upon limited ground contact pressures are essential. This will require limitations on vehicle wheel loads and the use of more tyres and axles on heavy equipment. 相似文献
907.
Most of the methods available for plant rooting studies in field soil are very tedious and time-consuming. Several investigations have shown that the core-break technique, in which roots are counted that appear at the faces of a broken core of soil, provides acceptable estimates of root length density in some situations. We investigated the usefulness of the core-break technique for evaluating rooting density of four plant species in two soil types. We encountered several problems, but recommend the core-break method to researchers who wish to quantify root development rapidly under various soil tillage practices. 相似文献
908.
Adsorption of sulphate and fluoride by variable charge soils 总被引:2,自引:0,他引:2
The adsorption of sulphate and fluoride by three variable charge soils was studied. Adsorption increased with increase in the amount of sulphate added at constant p H, and decreased with increase of p H.
The ratios of the amount of released OH− to that of the adsorbed SO2- 4 at pH 5–0 were 0.12, 0.14 and 0.20 for the three soils, respectively, much lower than the corresponding OH− /F− ratios which ranged from 0.3 to 1.0. For a ferric acrisol the OH− released accounted, on average, for only 15% of the SO2- 4 adsorbed, leaving more than 60% to be explained by the decrease in positive charge and the increase in negative charge carried by the soil. 相似文献
The ratios of the amount of released OH
909.
At Onne in South-east Nigeria, drainage water was collected from four monolith lysimeters and analysed for nitrate. The lysimeters contained an acid sandy loam. At the start of the first rainy season two lysimeters received urea labelled with 15 NO3 – and two received no nitrogen fertilizer; all four were uncropped in the first year.
The peak concentrations of15 NO3 – and of unlabelled (soil) NO3 – were found after 2.5 pore volumes of water had passed through the lysimeters. Using the same soil in the laboratory after fine sieving, the peak concentration of tritiated water was found at 1 pore volume whereas nitrate leaching was retarded. The pattern of nitrate leaching was well described by miscible and immiscible models which included an adsorption coefficient for nitrate. Over the 2 years 81.4% of the 15 N added at the start of the first rainy season was recovered in the drainage water. 相似文献
The peak concentrations of
910.
Laterite profiles in the Sydney area are generally regarded as fossil soils, formed during the Miocene, on a peneplain, under a tropical climate. It is also held that subsequent uplift and dissection destroyed much of this surface together with the laterite profiles. These views are poorly established yet widely accepted. This study demonstrates that there is a very close mineralogic and stratigraphic relationship between the “laterite profiles” and the Triassic Hawkesbury Sandstone, such that the profiles are best regarded as iron rich sandstone units undergoing contemporary near-surface alteration including the mobilization of iron minerals as crystalline solids. 相似文献