曲拉通和硝酸混合溶液直接提取快速测定草鱼中铅含量

为建立快速测定草鱼中铅含量的方法,通过分析曲拉通和硝酸混合溶液浓度、提取时间、称样定容体积比例等因素的影响,以及基体改进剂的使用效果,确定了草鱼中铅元素提取测定的最佳条件。验证结果显示：采用曲拉通和硝酸混合溶液提取草鱼中铅元素方法的提取率为86.5%～95.6%,加标回收率为91.5%～95.6%,精密度均小于4.0%,检出限和定量限分别为0.011和0.032 mg/kg,满足了国家标准GB 5009.12—2017第一法石墨炉原子吸收光谱法的要求。与国家标准方法比较,本研究建立方法的样品前处理时间从4～12 h缩短至0.2 h内,酸试剂用量从湿法消解的7～12 mL减少至1～2 mL;前处理过程无需高温消解,无需其他前处理设备,避免了样品污染和待测元素损失,实现了降低分析成本以及保护环境和试验人员的目的。结果表明,该方法是一种简单、准确、绿色、快速测定草鱼中铅含量的方法,尤其适合大量样品检测。     

三棱栎种子特性与其致濒关系初步分析

三棱栎是云南特有种,国家二级保护植物,主要分布在澜沧、沧源、孟连、西盟、勐腊等县.研究表明,其萌发温度在20～35℃范围内,萌发率在5.3%～9.1%之间.4个不同分布地和8种温度条件下萌发率差异不显著.本文认为三棱栎濒危的主要原因是:(1)三棱栎果实结实率低;(2)果实的特殊形状,不利于传播;(3)幼苗缺乏竞争力.针对三棱栎的濒危现状和原因,提出了三棱栎的一些保护措施.     

Analysis of the Sediment Development and Trend In Jinshajiang River Drainage Area

Jinshajiang River, which has a drainage area of 485,100 Km 2, average flux of 142.9 billion m 3, and soil conveyance of 247 million t/a, is the largest branch of Changjiang river. It is also the largest soil resource of the Three Gorges reservoir and upper reach of Changjiang River. To research the development and trend of Jinshajiang sediment not only has a relation to Jinshajiang water resource strategy, but also has important meaning to control the silt in Three Gorges reservoir and the Changjiang water resource development. The paper statistically analyses the flux and sediment conveyance of the Pingshan station, which is the primary hydrological station in the Jinshajiang River Drainage Area. Through several non-parameter statistical methods such as Spearman order correlativity check, Kendell order correlativity check, and linear regression check, the paper concludes that the sediment evolvement trend of Pingshan station is not distinct.     

Experimental Study of Multifunctional Acid to Deliquesce Stratum-jam

Aiming at the oneness of acid to deliquesce stratum-jam applied in scene at the present time,which is incapable of deliquescing complex dirty simultaneously,this article confects a new multifunctional O/W acid.This acid is an emulsified mixture containing 15% hydrochloric acid as its extro-posture,high dissolved oil as its internal state under the function of some proper exterior active reagent.It is composed of 0.5%OP-10,0.5%Span80,0.2%Tween80,0.06%imidazole and 0.01%twelve-alcohol,and the content of oil is equal to the acid content.It can be indicated that this acid has good ability of resolving mineral(CaCO_3,MgCO_3) and organic compound(mainly colloidal bitumen) when it was poured into the stratum,so that it can deliquesce oleic stratum-jam,resume and improve the penetrability of stratum,boost the ability of liquid flowing up.     

THE PERFORMANCE ANALYSIS FOR THE HYDRAULIC SERVO-SYSTEM OF HAULAGE PARTY FOR SGW-150 SHEARER WITH CONSTANT POWER SPEED GOVERING

The mechanization of mining thinnest coal seam is a key program in the 7th five-year plan in Sichaan province, It is sponsored by The Scientific and Technieal Commission of Sichuan province. In this paper, the dynamic performance for the hydraulie servo-system of haulage party for SGW-150 shearer with coustant-power speed governing is analysed. It shows that the system designed by us is stability and reasonable for SGW-150 shearer.     

基于单台强震数据软厚场地地震反应不确定性分析

选取新西兰Canterbury地区12个强震台站及2010—2012年间的台站584条记录,以浅硬场地LPCC作为参考台站,系统分析Christchurch市区软厚场地地震效应(即场地放大函数)的不确定性及地震动强度、震级、震源距及震源方位角等因素对场地放大函数不确定性的影响规律。分析结果发现：1)地震动强度水平对场地放大函数均值影响较小,仅在长周期(如大于1.0 s)段趋于增大场地的放大效应;以不同地震动强度值进行分组,地震动强度大于0.6 m/s 2的分组场地放大函数标准差显著高于地震动强度小于0.6 m/s 2分组,特别是地震动强度大于1.0 m/s 2时场地放大函数标准差最大,反映了场地土层非线性提高场地地震效应的不确定性;2)地震震级对场地放大函数不确定性影响小,不同地震震级分组场地放大函数均值及标准差的表现基本相当;3)震源距是场地地震反应不确定性的一个重要因素,震源距小于5 km时场地放大函数的标准差明显大于其它情况,即震源距越小地震反应不确定性越大;4)场地放大函数不确定性与震源方位角的选取基本无关,即选取不同的震源方位角场地放大函数标准差无明显差别。     

Exploration of the Sustainability Design for Industrial Building

Within the domain of comprehensive architecture, the general instructive principles for the sustainability design are applicable to that of industrial building. Based on the analysis of excellent precedents, in this paper, some useful experiences are summarized. It is pointed out that the sustainability design is feasible and should be compulsive for industrial building.     

简单屋顶绿化的滞蓄特性

设计了模拟降雨与数据采集系统,研究了短时强降雨下简单屋顶绿化基质(配比：陶粒57.0%、草炭41.5%、保水剂1.5%)的降雨产流过程,基于37次模拟降雨实验,归纳了降雨产流的一般过程、规律和特性,分析了降雨强度、基质厚度和基质初始含水率对简单屋顶绿化滞流蓄水特性的影响。结果表明：基质厚度和基质初始含水率对简单屋顶绿化的蓄水特性有显著影响,基质初始含水率越低、基质厚度越厚时蓄水特性越佳。建立了产流时间数学模型,简单屋顶绿化降雨产流时间与降雨强度呈负相关,同时也受初始含水量和基质厚度影响。随着干湿循环次数增加,基质的厚度总体呈现下降趋势,储水性能逐渐下降,延迟产流时间逐渐缩短。     

电磁振动排种器的试验研究

对排种盘上的种子进行了运动分析,论述了电磁振动排种器的工作原理。通过试验,找出了振动式排种器各运动参数对排种器排种量的影响规律。对不同形状的中、小粒种子进行了条播和精播台架试验,并对水稻、小麦种子进行了田间试验,结果表明:该排种器适用于各种形状复杂的中、小粒种子,播种精度高,不损伤种子。