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961.
Flavonoid constituents of Chorizanthe diffusa with potential cancer chemopreventive activity 总被引:11,自引:0,他引:11
Chung HS Chang LC Lee SK Shamon LA van Breemen RB Mehta RG Farnsworth NR Pezzuto JM Kinghorn AD 《Journal of agricultural and food chemistry》1999,47(1):36-41
An ethyl acetate-soluble extract of Chorizanthe diffusa was found to exhibit significant antioxidant activity, as judged by scavenging stable 1,1-diphenyl-2-picrylhydrazyl (DPPH) free radicals and inhibition of 12-O-tetradecanoylphorbol 13-acetate (TPA)-induced free radical formation with cultured HL-60 cells. Bioassay-directed fractionation of this extract using the DPPH antioxidant assay as a monitor led to the isolation of five structurally related flavonoids (1-5), including the novel compound 5,8,3',4',5'-pentahydroxy-3, 7-dimethoxyflavone (1). Isolates 1-5 demonstrated varying degrees of antioxidant or antimutagenic activity. Two of the compounds, 5,7,3', 4'-tetrahydroxy-3-methoxyflavone (2) and quercetin (4), were subsequently found to inhibit carcinogen-induced preneoplastic lesions in a mouse mammary organ culture model. Inhibitory activity of this type is known to correlate with cancer chemopreventive effects in full-term models of tumorigenesis. 相似文献
962.
Changes in soil properties and yield response in relation to tillage and residue management treatments in an irrigated groundnut (Arachis hypogea L.)—wheat (Triticum aestivum, L.) rotation on a sandy soil (1972–1974) and on a sandy loam soil (1974–1976) were evaluated. Tillage treatments (T1 and T2) did not cause significant changes in soil properties. Incorporation of crop residues (5 t residue per ha per crop, T3) caused a substantial increase in organic C, available N, and NaHCO3 -extractable P contents in the top 15 cm of both soils. Residue management treatments (T3, T4 and T5) showed no significant effect on soil bulk density and exchangeable K. Crop yields under no-tillage (T1) and conventional tillage (control, T2) were comparable on sandy soil but on the sandy loam soil, no-tillage yielded significantly lower than conventional tillage. Compared with the control, incorporation of crop residues (T3) caused higher yields on sandy soil for groundnut and wheat by 34.1 and 47.4%, respectively, and on sandy loam by 17.1 and 7.2%, respectively. Mulching with crop residues conserved soil moisture and reduced maximum soil temperature (1.5–5.3°C in groundnut and 1.5–2.9°C in wheat) but other measured soil properties were not significantly affected. Significant yield increase due to residue mulching (T4) was observed in sandy soil but it was significantly less than when total crop residue was incorporated (T3). Increased wheat root-weight density in the top 15 cm soil with residue mulching was not reflected in grain yield. Compared with the incorporation of the total amount of crop residue (T3), incorporation of half the amount and application of the other half as mulch (T5) caused lower yields — on sandy soil for groundnut and wheat by 31.5 and 15.7%, respectively, and on sandy loam by 4.8 and 3.6%, respectively. 相似文献
963.
This study highlights the previously expressed concerns of soil researchers who have indicated that compaction pressures or stresses in the deeper layers of soil are determined by the amount of surface load. Modifications of Boussinesq theory by Froelich and further modification of Froelich's equations by Soehne were used to predict and develop graphical relationships for maximum allowable loads and/or mean surface contact pressures beneath loaded farm machinery tyres. Vertical compressive stresses at different subsoil depths were calculated and design loads for a currently used high flotation tyre were examined for comparative purposes. For highly compactible soils the results indicate that mean surface contact pressures should not exceed maximum allowable stresses in the subsoil for individual wheel loads which exceed approximately 30 kN. Thus, it appears that future designs based upon limited ground contact pressures are essential. This will require limitations on vehicle wheel loads and the use of more tyres and axles on heavy equipment. 相似文献
964.
Adsorption of sulphate and fluoride by variable charge soils 总被引:2,自引:0,他引:2
The adsorption of sulphate and fluoride by three variable charge soils was studied. Adsorption increased with increase in the amount of sulphate added at constant p H, and decreased with increase of p H.
The ratios of the amount of released OH− to that of the adsorbed SO2- 4 at pH 5–0 were 0.12, 0.14 and 0.20 for the three soils, respectively, much lower than the corresponding OH− /F− ratios which ranged from 0.3 to 1.0. For a ferric acrisol the OH− released accounted, on average, for only 15% of the SO2- 4 adsorbed, leaving more than 60% to be explained by the decrease in positive charge and the increase in negative charge carried by the soil. 相似文献
The ratios of the amount of released OH
965.
Determination of insoluble, soluble, and total dietary fiber in foods and food products: interlaboratory study 总被引:12,自引:0,他引:12
L Prosky N G Asp T F Schweizer J W DeVries I Furda 《Journal of the Association of Official Analytical Chemists》1988,71(5):1017-1023
A collaborative study was conducted to determine the insoluble dietary fiber (IDF), soluble dietary fiber (SDF), and total dietary fiber (TDF) content of food and food products by using a combination of enzymatic and gravimetric procedures. The method was basically the same as that developed for TDF only, which was adopted official final action by AOAC, except for changing the concentration of buffer and base and substituting hydrochloric acid for phosphoric acid. These changes were made to improve the robustness of the method. Duplicate blind samples of soy isolate, white wheat flour, rye bread, potatoes, rice, corn bran, oats, Fabulous Fiber, wheat bran, and a high fiber cereal were analyzed by 13 collaborators. Dietary fiber values (IDF, SDF, and TDF) were calculated as the weight of residue minus the weight of protein and ash. The coefficients of variation (CVs) of both the independent TDF determination and the sum of IDF and SDF were better than 15 and 18%, respectively, with the exception of rice and soy isolate. These 2 foods, however, contained only about 1% TDF. The CVs of the IDF were equally good, except for Fabulous Fiber, for which filtration problems occurred. The CVs for the SDF were somewhat high, but these products had very low SDF content. There was excellent agreement between the TDF determined independently and the TDF determined by summing the IDF and SDF. The method for separate determination of IDF and SDF requires further study. The modifications (changes in concentration of buffer and base and the use of hydrochloric acid instead of phosphoric acid) to the official final action method for TDF have been adopted. 相似文献
966.
Summary We studied the effect of three successive cuttings on N uptake and fixation and N distribution in Leucaena leucocephala. Two isolines, uninoculated or inoculated with three different Rhizobium strains, were grown for 36 weeks and cut every 12 weeks. The soil was labelled with 50 ppm KNO3 enriched with 10 atom % 15N excess soon after the first cutting. Except for the atom % 15N excess in branches of K28 at the second cutting, both the L. leucocephala isolines showed similar patterns of total N, fixed N2, and N from fertilizer distribution in different parts of the plant at each cutting. The Rhizobium strain did not influence the partitioning of 15N among the different plant parts. Significant differences in 15N enrichment occurred in different parts. Live nodules of both isolines showed the lowest atom % 15N excess values (0.087), followed by leaves (0.492), branches (0.552), stems (0.591), and roots (0.857). The roots contained about 60% of the total plant N and about 70% of the total N derived from fertilizer over the successive cuttings. The total N2 fixed in the roots was about 60% of that fixed in the whole plant, while the shoots contained only 20% of the fixed N2. We conclude that N reserves in roots and nodules constitute another N source that must be taken into account when estimating fixed N2 or the N balance after pruning or cutting plants. 15N enrichment declined up to about fivefold in the reference and the N2-fixing plants over 24 weeks following the 15N application. The proportion and the amounts of N derived from fertilizer decreased, while the amount derived from N2 fixation increased with time although its proportion remained constant. 相似文献
967.
N J Yess M G Houston E L Gunderson 《Journal of the Association of Official Analytical Chemists》1991,74(2):265-272
Pesticide residues in foods are reported for the 5-year period 1978-1982 [fiscal years (FY) 78-82]. Results were compiled from the 2 complementary elements that comprise the Food and Drug Administration's (FDA) program for monitoring pesticide residues in foods. Under regulatory monitoring, which focuses on residues in raw agricultural commodities, a total of 49,877 samples (30,361 domestic and 19,516 import) that included fresh fruits and vegetables, grains, milk and dairy products, seafoods, and a variety of processed foods were analyzed. No residues were found in about 55 and 44% of the domestic and import samples, respectively. About 3% of the domestic and 7% of the import samples were classed as violative. Data from the Total Diet Study, which is conducted to determine dietary intakes of a variety of chemicals, showed that residues of 42 pesticides were found in 1044 composites of table-ready foods. Results of FDA's monitoring for FY78-82 demonstrate that pesticide residue levels in the U.S. food supply were generally well below regulatory limits, and dietary intakes were manyfold lower than the Acceptable Daily Intakes established by international agencies. 相似文献
968.
Asubiojo O. I. Aina P. O. Oluwole A. F. Arshed W. Akanle O. A. Spyrou N. M. 《Water, air, and soil pollution》1991,(1):819-828
The effects of cement production on the elemental composition of soils in the neighborhood of two cement factories in Nigeria have been investigated using the XRF and PIXE/RBS techniques. The concentration of 21 elements viz:-Mg, Al, Si, P, S, K, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Sr, Pb, As, Zr, Rb and Br, were determined in about 30 samples. Calcium, P, S, Cr, Ni, Cu and Zn, were found to be relatively enriched in the soils of the cement factory premises. Calcium, a cement marker element, was found to be well correlated with Mg, S, Fe, Ni and Cu in the soils, and inversely proportional to the Si and Ti concentrations. From Ca/Si ratios and enrichment factors of the marker elements, it was found that soil contamination due to cement drops sharply with distance from the factories, and with increasing depth from the surface. 相似文献
969.
D Veierov N Aharonson 《Journal of the Association of Official Analytical Chemists》1978,61(2):253-260
A new cleanup procedure is described for chlorinated hydrocarbon residues in butterfat. The method is based on the dropwise addition of H2SO4 to a fat solution column and continuous removal of the lipids and the acid. The cleanup of 0.25-2.0 g fat requires only 10-40 ml sulfuric acid and 12-17 ml petroleum ether. There is no need for any further cleanup step, solvent evaporation, or centrifugation. The method is easy to standardize and is suitable for automation. At least 30 fat samples can be cleaned up manually by one analyst in one day. Recoveries were complete (greater than 90%) for polychlorinated biphenyl compounds and for 13 chlorinated pesticides of 16 examined. The method was tested on chlorinated hydrocarbon residues in commercial butter and the results were compared with those obtained with the acetonitrile method. The versatility and limitations of the method were investigated by varying the sulfuric acid strength, initial fat solution concentration, and column dimensions. 相似文献
970.
Piet?C.?N.?GroenewaldEmail author Carin?S.?Viljoen 《Journal of Agricultural, Biological & Environmental Statistics》2003,8(1):75-83
This article aims to determine the effect of certain covariates, such as season of kidding, parity, and time of kidding on
the characteristics of the lactation curve of Saanen dairy goats. Characteristics investigated are peak milk yield, time of
peak milk yield, total milk production, persistency, and the relationship between fat and protein in milk composition, as
well as between lactation curves of the same animal in successive years. The analysis is carried out using a hierarchical
Bayesian approach, together with Wood’s model, to model lactation. Posterior distributions of quantities of interest are obtained
by means of the Markov chain Monte Carlo (MCMC) methods. These clearly illustrate the significant effect of especially parity,
but also season and time of kidding on the characteristics of the lactation curve. Total and peak milk yield increase with
increasing parity up to about the third or fourth parity, while peak yield is later for first than for later parities. The
analysis also enables estimation of lactation characteristics of untested animals, prediction of future characteristics and
identification of exceptional animals. 相似文献