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31.
Dr. Hiromu Kajita Dr. Junsuke Mukudai Dr. Hiroyuki Yano 《Wood Science and Technology》1991,25(3):239-249
Summary Specimens of four commercially produced particleboards were exposed to various accelerated aging treatments: 1) 6-cycle ASTM D-1037 exposure, 2) 6-cycle WCAMA exposure, 3) BS 5669 test, 4) cyclic soak-dry test, and 5) cyclic boil-dry test. Thickness swelling (TS) and internal bond strength (IB) were measured after each step of each cycle. Phenol and phenol (face)/isocyanate (core)bonded boards are more durable than urea and melamine urea bonded boards. The effect of treatment 1) is most severe on TS and IB retention, followed in order by treatments 2), 5), 4) and 3). When the value of springback reached about 35%, IB became equal to zero. 相似文献
32.
For the fundamental study of oxygen delignification of kraft pulp, structural changes of kraft lignin during alkaline oxygen treatment were investigated with the use of infrared measurement with attenuated total reflectance (ATR) technique. In the neutralized reaction mixture of alkaline oxygen-treated kraft lignin, there is a significant amount of NaCl, so that the spectral changes of water due to the coexistence of NaCl was investigated, and how to remove the huge absorption of NaCl solution is discussed. Sodium vanillate–NaCl solutions were employed as model solutions for the reaction mixture. Partial least square (PLS) regression was applied for the prediction of NaCl concentration, and the spectrum of NaCl solution was subtracted from the spectrum of sodium vanillate–NaCl solution as background measurement. This allowed us to obtain the vanillate spectra free from the absorption of NaCl solution. In addition, the mathematical method for reconstructing the spectrum of NaCl solution is discussed. The spectrum of NaCl solution is reconstructed as the linear combination of basic spectra calculated by singular value decomposition (SVD), and it was subtracted from that of the sodium vanillate–NaCl solution. By this procedure, the vanillate spectra were also obtained quantitatively, as has been demonstrated in PLS regression study. It was also confirmed that the quantitative spectra of high molecular weight fraction of alkaline oxygen-treated kraft lignin were obtained by the use of this reconstruction technique.Parts of this report were presented at the 52nd Annual Meeting of the Japan Wood Research Society, Gifu, Japan, April 2002 and the 12th International Symposium on Wood and Pulping Chemistry, Madison, USA, June 2003 相似文献
33.
34.
Takahisa Nakai Hiroyuki Yamamoto Masatoshi Hamatake Tetsuya Nakao 《Journal of Wood Science》2006,52(6):539-543
This study investigated the relationship between the initial shape of the stress (σ)-strain (ε) curve of a Chamaecyparis obtusa wood specimen subjected to repeated combined compression and vibration stresses at various angles between the fiber direction
and load direction and the piezoelectric behavior. The main findings of the study are: (1) the σ-ε curve became convex initially, and then the stress was proportional to the strain. The σ-ε curve had almost the same shape during both loading and unloading. (2) The σ-piezoelectric voltage (P) curve was nonlinear, with a maximal point or cusp on the curve, which had almost the same shape during both loading and
unloading, as was also observed for the σ-ε curve. (3) The plot of the first derivative of the stress [dσ/dε (= σ′)] against ε was nonlinear. The σ′-ε and P-ε curves at various angles were fairly similar. (4) The stress at the maximal point (or cusp) of the σ-P curve decreased with an increase in the angle between the fiber direction and load direction. The tendency of the stresses
was very similar to that of Young’s modulus and compression strength calculated from Hook’s law and Hankinson’s law, respectively. 相似文献
35.
This study examined how boiling and drying treatments influenced various physical properties of the tension wood with gelatinous
fibers (G-fibers) of a 29-yearold Zelkova branch. By boiling treatment, tension wood with numerous G-fibers contracted considerably in the longitudinal direction and
the longitudinal Young’s modulus decreased in spite of the water-saturated condition. The drying treatment caused green tension
wood and boiled tension wood with numerous G-fibers to shrink longitudinally and increased their longitudinal Young’s moduli.
These specific behaviors in tension wood were highly correlated with the proportion of G-fibers in a specimen and were probably
caused by the microscopic behavior of cellulose microfibril (CMF) in the gelatinous layers (G-layers). The longitudinal shrinkage
of tension wood due to drying suggests the existence of a hygro-sensible, noncrystalline region in the CMF, which is abundant
in the G-layer. Furthermore, the noncrystalline region in the CMF softens during boiling treatment, resulting in the reduction
of the longitudinal Young’s modulus in tension wood. The longitudinal contraction of tension wood with G-fibers by boiling
might be caused by the tensile growth stress remaining in green G-layers. However, no changes were detected in the 004 d-spacing of cellulose crystal in tension wood from the boiling and drying treatments, regardless of the proportion of G-fibers. 相似文献
36.
37.
Dielectric properties in three main directions for hinoki wood (Chamaecyparis obtusa) specimens conditioned at various levels of relative humidity were measured in the frequency range from 20 Hz to 10 MHz over
the temperature range from −150°C to 20°C. Three relaxations were observed in the specimens conditioned at high levels of
relative humidity. The relaxation in the highest frequency range was ascribed to the motions of adsorbed water molecules.
The relaxation in the middle frequency range remained unchanged by the ethanol–benzene extraction of specimens. The relaxation
location was independent of measuring directions. The relaxation in the lowest frequency range was not detected in the specimens
impregnated with methyl methacrylate (MMA). This result suggested that the relaxation was due to electrode polarization. The
Cole-Cole circular arc law applied well to two relaxations recognized in the specimens impregnated with MMA. The relaxation
magnitude in the middle frequency range was extremely large, and the distribution of relaxation times was very narrow. These
characteristics suggested relaxation of the Maxwell-Wagner type resulting from the interfacial polarization in the heterogeneous
structure, which included adsorbed water with large electrical conductivity within the insulating cell walls. 相似文献
38.
Takahisa Nakai Hiroyuki Yamamoto Tetsuya Nakao Masatoshi Hamatake 《Wood Science and Technology》2006,40(8):683-695
This study investigated the relationship between the cellulose crystal lattice strain (crystalline region) and the macroscopic surface strain in specimens of Chamaecyparis
obtusa wood under repeated uniaxial tension stress in the fiber direction. Changes in the strain of the crystal lattice were measured from the peak of (004) reflection using the transit X-ray method. The macroscopic surface strain of each specimen was measured with a strain gauge. In both loading and unloading, the surface strain changed linearly with changes in stress. However, crystal lattice strain was not linear but exhibited changes along a curve with changing stress. Under stressed conditions, the crystal lattice strain was always less than the surface strain, regardless of the frequency of repetition in the loading and unloading cycle. The ratio of the crystal lattice strain to the surface strain showed a negative correlation for stress in both loading and unloading. That is, the ratio decreased with increasing stress, and finally tend to converge to a specific value. The ratio (I/I
0) between the diffracted intensity (I
0) in the (004) plane in the unloaded condition and the diffracted intensity (I) in the (004) plane in the loaded condition tend to converge on a specific value with increasing frequency of repetition. When the substantial tension Young’s modulus of the wood in the longitudinal direction decreased, the ratio of the strain of the crystal lattice to the surface strain also decreased. Moreover, the ratio decreased with increasing microfibril angle of the specimen. 相似文献
39.
Toru Kohama Nobuya Mizoue Satoshi Ito Akio Inoue Kotaro Sakuta Hiroyuki Okada 《Journal of Forest Research》2006,11(4):235-242
We examined the extent to which direct and indirect measures of light and microsite conditions could explain variation in
tree height and diameter at the base of 6-year-old Cryptomeria japonica trees planted in a group selection opening of about 0.32 ha on a steep slope at Shiiba, Miyazaki Prefecture, southern Japan.
We first used the gap light index (GLI) and soil thickness (ST) as directly measured indices. For an indirect measure of light, we used a between-cohort competition index (BCI) estimated from the position and total height of residual trees. For indirect measures of microsite, we examined topographic
indices (slope, plan and profile curvature, average slope gradient, and relative elevation) derived from digital elevation
models (DEMs) with different resolutions ranging from 2 to 10 m. The multiple linear regression using GLI and ST explained about 45% of variation in tree size, while simple regression using only GLI explained about 35%. The contribution of ST was about half of GLI. The multiple regressions using BCI and the topographic indices did not explain any more variation than using BCI alone (R
2 of about 0.26). We conclude that microsite conditions with shallower soil and steeper slope have negative effects on tree
growth in group selection openings, although the relative importance is smaller than light conditions. More comprehensive
studies considering several openings with more heterogeneous topography including different species are needed to generalize
our growth prediction using the indirect measures, which are useful for practical forest management. 相似文献
40.
Naruyuki?Kamo Hiroyuki?Okamura Mitsuo?Higuchi Mitsuhiro?MoritaEmail author 《Journal of Wood Science》2004,50(3):236-241
Propylene carbonate (PC) is known as one of the cure accelerators for alkaline phenol–formaldehyde resins. To elucidate the cure-acceleration mechanisms, the effects of PC on the condensation reactions of monomeric hydroxymethylphenols (HMPs) were investigated and compared with those of PC hydrolysate, sodium bicarbonate (NaHCO3) and ethyl formate. Immediately after the reaction started, PC, decomposing itself simultaneously, accelerated the formation of the ortho-para methylene-bonded dimer of 2,4,6-trihydroxymethylphenol. This effect of PC was very similar to that of ethyl formate. To the contrary, PC hydrolysate accelerated the formation of the para-para methylene-bonded dimer throughout the course of the reaction. This effect of PC hydrolysate was identical to that of NaHCO3. These results indicate that PC increases the reactivity of the ortho-hydroxymethyl group, presumably through transesterification. On the other hand, NaHCO3 is formed by the hydrolysis of PC or decomposition of the transesterified HMPs and it increases the reactivity of the para-hydroxymethyl group. 相似文献