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181.
The 351-nanometer photoelectron spectrum of the planar cyclooctatetraene radical anion (COT·-) shows transitions to two electronic states of cyclooctatetraene (COT). These states correspond to the D4h 1A1g state, which is the transition state for COT ring inversion, and the D8h 3A2u state. The electron binding energy of the 1A1g transition state is 1.099 ± 0.010 electron volts, which is lower by 12.1 ± 0.3 kilocalories per mole than that of the 3A2u state. The photoelectron spectrum shows that the singlet lies well below the triplet in D8h COT and confirms ab initio predictions that the molecule violates Hund's rule. Vibrational structure is observed for both features and is readily assigned by use of a simple potential energy surface. 相似文献
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MJ Thompson J Toomre ER Anderson HM Antia G Berthomieu D Burtonclay SM Chitre J Christensen-Dalsgaard T Corbard M DeRosa CR Genovese DO Gough DA Haber JW Harvey F Hill R Howe SG Korzennik AG Kosovichev JW Leibacher FP Pijpers J Provost EJ Rhodes J Schou T Sekii PB Stark PR Wilson 《Science (New York, N.Y.)》1996,272(5266):1300-1305
Splitting of the sun's global oscillation frequencies by large-scale flows can be used to investigate how rotation varies with radius and latitude within the solar interior. The nearly uninterrupted observations by the Global Oscillation Network Group (GONG) yield oscillation power spectra with high duty cycles and high signal-to-noise ratios. Frequency splittings derived from GONG observations confirm that the variation of rotation rate with latitude seen at the surface carries through much of the convection zone, at the base of which is an adjustment layer leading to latitudinally independent rotation at greater depths. A distinctive shear layer just below the surface is discernible at low to mid-latitudes. 相似文献
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Jos Janderson Ferreira COSTA lvio GIASSON Elisngela Benedet DA SILVA Tales TIECHER Antonny Francisco Sampaio DE SENA Ryshardson Geovane Pereira de Oliveira E SILVA 《土壤圈》2022,32(2):294-306
Knowing the spatial distribution of soil texture,which is a physical property,is essential to support agricultural and environmental decision making.Soil texture can be estimated using visible,near infrared,and shortwave infrared(Vis-NIR-SWIR)spectroscopy.However,the performance of spectroscopic models is variable because of soil heterogeneity.Currently,few studies address the effects of soil sample variability on the performance of the models,especially for larger spectral libraries that include soils that are more heterogeneous.Therefore,the objectives of this study were to:i)apply Vis-based color parameters on the stratification of a regional soil spectral library;ii)evaluate the performance of the predictive models generated from the spectral library stratification;iii)compare the performance of stratified models(SMs)and the model without stratification(WSM),and iv)explain possible changes in prediction accuracy based on the SMs.Thus,a regional soil spectral library with 1535 samples from the State of Santa Catarina,Brazil was used.Soil reflectance data were obtained by Vis-NIR-SWIR spectroscopy in the laboratory using a spectroradiometer covering the 350–2500 nm spectral range.Sand,silt,and clay fractions were determined using the pipette method.Twenty-two components of color parameters were derived from the Vis spectrum using the colorimetric models.A cubist regression algorithm was used to assess the accuracy of the applicability of the initial models(SMs and WSM)and of the validation between the clusters.Fractional order derivatives(FODs)at 0.5,1.5,and 2 intervals were used to explain possible changes in the performance of the SMs.The SMs with higher contents of clay and iron oxides obtained the highest accuracy,and the most important spectral bands were identified,mainly in the 480–550 and 850–900 nm ranges and the 1400,1900,and 2200 nm bands.Therefore,stratification of soil spectral libraries is a good strategy to improve regional assessments of soil resources,reducing prediction errors in the qualitative determination of soil properties. 相似文献
185.
F. M. R. DA SILVA JNIOR P. F. SILVA F. S. GUIMARES K. A. DE ALMEIDA P. R. M. BAISCH A. L. MUCCILLO-BAISCH 《土壤圈》2014,24(2):280-284
The demand for simple and rapid bioassays in ecotoxicological evaluations is of paramount importance in order to speed up environmental monitoring programs. In this study we performed bioassays with lettuce seeds and two species of terrestrial isopods (Armadillidium vulgare and Porcellio dilatatus) for the ecotoxicological assessment of a landfarming soil from a petrochemical complex area. The solubilized content of test soil demonstrated a concentration-response type toxic effect on seed germination rate, and a delay on germination, but showed toxic effect on seedlings wet weight only at the highest concentration. Toxic effects were also observed in mortality rate and avoidance behavior of the two woodlice species. These results demonstrated the sensitiveness of the organisms studied, and highlighted the possibility to use these bioassays in environmental monitoring programs in areas contaminated with fossil fuels. 相似文献
186.
Edson M. MATTIELLO Eduardo L. CANCELLIER Rodrigo C. DA SILVA Fien DEGRYSE Roslyn BAIRD Mike J. MCLAUGHLIN 《土壤圈》2021,31(4):531-537
A very small amount of applied zinc (Zn) is taken up by crops, resulting in low recovery by plants. Adding elemental sulphur to zinc oxide (ZnO) fertiliser could improve Zn solubilisation and exert a higher residual effect on crops than soluble Zn sources. We produced an isotopically labelled Zn-elemental sulphur fertiliser and evaluated its performance in comparison to traditional Zn sources during sequential crop cultivation. Three 67Zn-labelled fertilisers, ZnO, zinc sulphate (ZnSO4), and ZnO co-granulated with elemental sulphur (ZnOS0), were soil applied, and their contributions to the uptake of Zn by three consecutive crops, wheat, ryegrass, and corn, were assessed in a 294-d pot experiment. The contributions of Zn fertilisers followed the order:ZnSO4 > ZnO=ZnOS0. The relative contributions of Zn fertilisers were lower in the first crop than in the subsequent crops. The overall recovery of applied Zn by the three crops was higher for ZnSO4 than for ZnO and ZnOS0, reaching 1.56%, 0.45%, and 0.33% of the applied Zn, respectively. Zinc recovery by plants was very low, regardless of the source of Zn. Adding elemental sulphur to ZnO did not increase its effectiveness up to 294 d after application. Fertiliser contribution was higher for the subsequent crops than for the initial crop, indicating the importance of assessing the residual effects of Zn fertilisers. 相似文献
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