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111.
Process for isolation of cardanol from technical cashew (Anacardium occidentale L.) nut shell liquid
Phani Kumar P Paramashivappa R Vithayathil PJ Subba Rao PV Srinivasa Rao A 《Journal of agricultural and food chemistry》2002,50(16):4705-4708
Commercially available technical cashew (Anacardium occidentale L.) nut shell liquid (CNSL) contains mainly cardanol (decarboxylated anacardic acid) and cardol. Cardanol, the monophenolic component of technical CNSL, is widely used as a synthon for the preparation of a number of polymers and agricultural products. This paper describes the separation of cardanol from toxic cardol. Technical CNSL was dissolved in a mixture of methanol and ammonium hydroxide (8:5) and extracted with hexane to obtain cardanol. The resultant methanolic ammonia layer was extracted with a mixture of ethyl acetate and hexane to yield cardol. This is the first industrially feasible process based on solvent extractions for the isolation of cardanol from technical CNSL. 相似文献
112.
Priyadarsini KI Khopde SM Kumar SS Mohan H 《Journal of agricultural and food chemistry》2002,50(7):2200-2206
Ellagic acid, a plant-derived polyphenol, inhibits gamma-radiation (hydroxyl radical) induced lipid peroxidation in rat liver microsomes in a dose- and concentration-dependent manner. Its antioxidant capacity has been estimated using the 1,1-diphenyl-2-picrylhydrazyl radical assay. To understand the actual mechanisms involved in antioxidant activity and the free radical scavenging ability,a nanosecond pulse radiolysis technique has been employed. The rate constants for the reactions of several reactive oxygen species and reactive nitrogen species such as hydroxyl, peroxyl, and nitrogen dioxide radicals have been found to be in the range of 10(6)-10(9) M(-1) s(-1). The ellagic acid radicals have been characterized by the absorption spectra and decay kinetics. Studies on the reactions of ellagic acid with the 2,2'-azinobis(3-ethylbenzothiazoline-6-sulfonate) radical and the radicals of ellagic acid with ascorbate have been used to estimate its one-electron reduction potential. Ellagic acid has also been found to be a good scavenger of peroxynitrite. Using stopped-flow reaction analyzer with absorption detection, the rate constant for this reaction has been determined to be 3.7 x 10(3) M(-1) s (-1). The electron spin resonance spectra of the oxidized ellagic acid radicals have been recorded by horseradish peroxidase and hydrogen peroxide method. 相似文献
113.
Studies on reproductive biology are difficult but useful in species like Aegle marmelos (Linn.) Correa which is of considerable socio-economic importance and possess morphogenetic variation and qualities of wider
adaptability to different soils. Cytology, phenology, pollination, breeding system and natural regeneration of wild and cultivated
trees from India revealed the existence of diploid (2n = 18) and tetraploid trees (2n = 36) in Pachmarhi hills and only diploid
trees in Punjab plains and Shiwalik hills. The diploid and tetraploid trees showed normal meiosis and high pollen fertility.
Phenological events which included leaf fall, leaf emergence, floral bud break, flowering and fruiting are nearly the same
in wild and cultivated trees. Natural pollen transfer in the species was highly efficient. Levels of fruit set following open
pollination was quite high and is reduced considerably following hand pollination probably due to some injury caused to stigma
during experiments. Inspite of synchronous nature of anther dehiscence and stigmatic receptivity, selfing in a flower was
avoided due to herkogamy. Some selfing, however, occurred through geitonogamous mode as bagging of panicles yielded 12.21 ± 0.99
to 14.12 ± 0.91% fruit set. High pollen ovule ratio (9,250–10,600) indicated toward the obligate outbreeding nature. The species
suited to insect and wind mode of pollination. High amount of air borne pollen grains deposited on glycerine smeared glass
microscopic slides suggested towards the wind mode of pollination. Though flowers are dull coloured a variety of insects visited
the flowers due to sweet fragrance and stamen/pollen as food reward. Among insect pollinators, honey bee (Apis dorsata) was the major and legitimate pollinator while the rest were either minor pollinators or mere visitors. Inspite of high fruit/seed
set, natural regeneration through seeds was poor as fallen fruits were destroyed by fungal pathogens and white ants. The species
also propagated vegetatively through coppices and root suckers. It lacks agamospermy as bagging of emasculated flowers yielded
no fruit. It is inferred that ‘bael’ which lacks agamospermy reproduced successfully through gamospermy (xenogamy and geitonogamy)
and vegetative mode (coppices and root suckers). We also concluded that tetraploid trees growing in the Pachmarhi hills with
large sized fruits possessed better potentialities in horticulture if planted through root suckers or coppices. 相似文献
114.
In the present study, we are reporting permeability and pharmacokinetics of nobiletin in rat plasma and brain, using a validated reverse phase high performance liquid chromatographic method. Protein precipitation method was used for the extraction of nobiletin and coumarin (IS) from rat plasma and brain tissue. The system was run in isocratic mode with mobile phase consisting of potassium dihydrogen ortho-phosphate (pH 4.5; 0.04 mM) and acetonitrile in ratio of 50:50, v/v. The total chromatographic run time was 9.0 min. The method was proved to be accurate and precise at linearity range of 0.05–10 μg/mL with a correlation coefficient (r) of ≥ 0.994 in rat plasma and ≥ 0.995 in rat brain. The intra- and inter-day precision and accuracy values are found to be within the assay variability limits as per the FDA guidelines. Nobiletin was found stable in the battery of stability studies viz., bench-top, auto-sampler, freeze/thaw cycles and long term storage in a freezer at − 70 ± 10 °C. Maximum concentrations of nobiletin in both plasma and brain were observed at 1 h after single oral dosing (50 mg/kg). The maximum concentration in plasma and brain were 1.78 and 4.20 μg/mL, respectively. The AUC0–t in plasma and brain were 7.49 and 20.66 μg·h/mL, respectively. The mean elimination half life (t1/2) in plasma and brain were 1.80 and 11.42 h, respectively. The Parallel Artificial Membrane Permeability Assay (PAMPA) permeability of nobiletin was found to be high at both pH 4.0 and 7.0. 相似文献
115.
Schizostachyum dullooa (Gamble) Majumder ‘dolu bamboo’ is a thin walled sympodial moderate sized to large tufted bamboo, dominant in the successional fallows of northeast India.
The impact of resource management on productivity and sustainability of the species was evaluated by investigating the population
status and regeneration in Cachar tropical semi evergreen forest under private property resource management (PPRM) and common
property resource management (CPRM) regimes. Population status revealed current-year, one-year, two-year and three-year-old
culms contribute 54%, 24%, 16% and 6% of the total culms per clump, respectively, under PPRM. Three-year-old culms were absent
in CPRM and population status was thus represented by current year (83%), one-year (16%) and two-year (1%) old culms. Net
change, rate of change and % gain in population for different age classes showed the prevalence of management practices under
CPRM was unscientific. Efficiency of new culm production per clump used as an index of regeneration was 69.7% in PPRM and
59.88% in CPRM. New culms produced under CPRM were small and thin. We conclude that CPRM is inappropriate for a long term
economic and ecological sustainability of the species and alternative management protocols are needed for conservation of
the species. 相似文献
116.
Rakhee Dangi Shubhada Tamhankar Ritesh Kumar Choudhary Suryaprakasa Rao 《Genetic Resources and Crop Evolution》2016,63(1):79-96
The genus Trigonella includes the widely cultivated T. foenum-graecum and a number of other medicinal and aromatic plant species distributed around the Mediterranean region. Sectional delimitation of Trigonella species is still based on morphology and interspecific relationships within the genus are not yet sufficiently resolved. Phylogenetic relationships in 22 species representing 11 of the 12 sections recognized within the genus Trigonella were analyzed using nuclear ITS and plastid trnL-F DNA sequences. Within nuclear ITS region, ITS-II was found to evolve faster compared to ITS-I. Maximal phylogenetic resolution and support was obtained in the combined analysis of the two selected regions. Trees resulting from maximum parsimony as well as Bayesian inference of combined data provided evidence for Trigonella being monophyletic with high support but did not agree with the traditional subgeneric division. Phylogenetic reconstructions indicated three major lineages supported by apomorphies in inflorescence and stipule. The phylogram supported the sectional delimitation of sections Cylindricae, Vérae, Samaroideae, Pectinatae, Erosae and Callicerates. There is strong support to combine monotypic sections Pectinatae and Erosae into one. However, species belonging to section Foenum-graecum and Falcatulae clustered in different subclades, contrary to their current classification. Inflorescence type appears to be a useful character with taxonomic potential for phenetic implications at subgeneric and sectional level within the genus. Moreover, some legume and seed characteristics, considered important in existing taxonomy, appear to have arisen more than once in Trigonella and are homoplastic. 相似文献
117.
Maneesh Kumar S. K Singh J. S Bohra 《Communications in Soil Science and Plant Analysis》2020,51(5):658-674
ABSTRACTField experiments were conducted for 2 years in sandy loam soil, to study the direct effect of organic manures i.e. sewage sludge (SS), vermicompost (VC) and sesbania (SB) and chemical fertilizers on rice (Oryza sativa) and their residual effect on wheat (Triticum aestivum) grown in sequence in winter (Rabi) and summer (Kharif) season during 2015–2016 to 2016–2017 at Varanasi, Uttar Pradesh. Residual effect of organic sources of nutrients as SS, VC and SB were monitored up to fourth crop (II wheat) in sequence applied in conjunction with 75% recommended dose of fertilize (RDF). Among the nutrient sources, the maximum grain yield in I rice (4.89 t ha?1), II rice (4.95 t ha?1), was recorded in treatment T3 (100% RDF with S, Zn, B) whereas in I wheat (4.68 t ha?1) and II wheat (4.59 t ha?1), it was recorded in T4 (customized fertilizer). The maximum straw yield during all four crops was recorded in T3 (100% RDF with S, Zn, B) in rice and T4 (customized fertilizer) in wheat crop, which showed 25, 32, 23 and 28% increase over 100% RDF (T2). Application of 100% RDF along with S, Zn, B and customized fertilizer increased the total uptake of N, P, K, S and B and also in net returns and B:C ratio followed by organic treatments. 相似文献
118.
Kulvir Singh Harinder Pal Singh Sudhir Kumar Mishra 《Communications in Soil Science and Plant Analysis》2020,51(7):919-931
ABSTRACTDelayed sowing and imprecise application of irrigation water to cotton has been the major hurdle in sustaining cotton yield in north-western India. Therefore, studies were initiated to ascertain the impact of heavy or normal level of presowing irrigation (PSI), scheduling time of first postsowing irrigation (POSI) under two sowing dates (SDs) on cotton arranged in a split block design replicated thrice. PSIh (100 mm) recorded 23.2% higher seed cotton yield over PSIn (70 mm) owing to better yield attributes and higher stand. First POSI at 4 weeks after sowing (WAS) resulted the highest yield (3072 kg ha?1), while one at 6 WAS (POSI6) recorded least due to poor population and reduced yield attributes. Water productivity under POSI6 was lesser by 29.1%, 25.2%, and 16.2% as compared to POSI3, POSI4, and POSI5, respectively. April sown crop out yielded the May sown cotton crop by 939 kg ha?1 due to better yield attributes. Nitrogen factor productivity (NFP) among SD remained higher by 23.3% for April as compared to May sowing. PSIh exhibited better NFP over PSIn. POSI6 recorded least NFP by 24.4%, 28.5%, and 16.3% as compared to POSI3, POSI4, and POSI5, respectively and was indicative of relatively poor utilization of N under delayed schedules. Therefore, planting in April after heavy PSI and scheduling first POSI at 4 WAS is best strategy for sustaining cotton yield and maximizing farmer profitability. 相似文献
119.
AbstractMaize response to deficit water and nitrogen for assessing phenological development and yield was studied under semi-arid conditions. Experiment consisting three drip irrigation levels, replenish 60 (DI60), 80 (DI80) and 100 percent (DI100) of cumulative pan evaporation, and four nitrogen doses 50 (RN50), 75 (RN75), 100 (RN100) and 125 (RN125) per cent of recommended nitrogen. A Furrow irrigated treatment was kept as control/check. Significant earliness in visibility of collar of 8th leaf, tasseling, silking and significant delay in dough stage and physiological maturity was recorded under well water treatment DI100 as compared to DI60. Days to collar of 8th leaf, tasseling and silking had significant negative correlation, and duration of yield formation phase and days to physiological maturity had significant positive correlation with grain yield. Higher DM production, longer yield formation phase and late physiological maturity led to significantly higher grain yield under DI100. In case of nitrogen levels, phonological characteristics like collar of 8th leaf, tasseling and silking were significantly delayed, and dough stage and physiological maturity were advanced under nitrogen deficit treatment RN50 as compared to RN100 and RN125. Significantly higher dry matter production and longer yield formation phase observed led to significant higher SCY under RN100 and RN125 as compared to RN50. Yield formation phase was significantly longer under drip irrigated crop as compared to control during 2nd year of study. Crop phenological development significantly affected by drip irrigation regimes and nitrogen levels, and there was significant correlation between phenological stages development and grain yield. 相似文献
120.
Biswas A Adhvaryu A Gordon SH Erhan SZ Willett JL 《Journal of agricultural and food chemistry》2005,53(24):9485-9490
Specialty chemicals based on renewable resources are desirable commodities due to their eco-friendly nature and "green" product characteristics. These chemicals can demonstrate physical and chemical properties comparable to those of conventional petroleum-based products. Suitably functionalized amines in the triacylglycerol structure can function as an antioxidant, as well as an antiwear/antifriction agent. In addition, the amphiphilic nature of seed oils makes them an excellent candidate as base fluid. The reaction of amine and epoxidized seed oils in the presence of a catalyst almost always leads to different intra/intermolecular cross-linked products. In most cases, the triacylglycerol structure is lost due to disruption of the ester linkage. Currently, there is no reported literature describing the aminolysis of vegetable oil without cross-linking. Here the epoxy group of the epoxidized soybean oil has been selectively reacted with amines to give amine-functionalized soybean oil. The optimization procedure involved various amines and catalysts for maximum aminolysis, without cross-linking and disruption of the ester linkage. Diethylamine and ZnCl2 were found to be the best. NMR, IR, and nitrogen analysis were used to characterize the products. 相似文献