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81.
  总被引:4,自引:0,他引:4  
A novel and simple method for the determination of some pesticide residues in strawberries using both focused microwave-assisted extraction (FMAE) and solid-phase micro extraction (SPME), coupled with high-performance liquid chromatography (HPLC), has been developed. The pesticides were first extracted from strawberries with water and the assistance of focused microwaves at 30 W for 7 min. Then, an aliquot of the resulting aqueous extract was subjected to SPME with a 60-microm thick poly(dimethylsiloxane)/divinylbenzene (PDMS/DVB) fiber for 45 min at room temperature, with the solution being stirred at 1000 rpm. The extracted pesticides on the SPME fiber were desorbed into the SPME/HPLC interface for quantitative analysis with a diode array detector (DAD). The whole sample pretreatment procedure before chromatographic analysis did not use any organic solvents or involve any blending or centrifugation steps. The five compounds (carbendazim, diethofencarb, azoxystrobine, napropamide, and bupirimate) were chosen because they cannot be analyzed easily by GC. The efficiency of this relatively fast procedure was comparable to that of previously reported methods, with detection limits at low microg/kg levels and linear responses in the range from 0.05 to 1 mg/kg of pesticide in strawberries, with RSDs between 3 and 7.3%, depending on the analyte. In all but one case results obtained by this method for field-incurred samples were comparable to those obtained with traditional methods.  相似文献   
82.
    
S. Jenni    W. Yan 《Plant Breeding》2009,128(4):374-380
Lettuce is a cool season crop susceptible to physiological disorders when exposed to supra optimal temperatures. Genotype (G) by environment (E) interaction (GE) of rib discolouration, tipburn, premature bolting and ribbiness in crisphead lettuce was characterized under high temperature and long day growing conditions. Replicated data of 10 crisphead lettuce varieties from two plantings in each of four growing seasons at two locations in Quebec were analysed using the GGE biplot method. Head-weight-over-stem-length ratio, ribbiness, rib discolouration incidence and tipburn incidence were affected (P = 0.00001) by E, G and GE. E explained more variation in head-weight-over-stem-length ratio (77.1%) and rib discolouration incidence (77.3%) than G and GE, whereas GE explained more variation (72.4%) in tipburn incidence and G explained more variation (38%) in ribbiness. Strong crossover GE was detected with rib discolouration and tipburn incidence, but not with head-weight-over-stem-length ratio and ribbiness. Under heat stress, varieties of the Vanguard group had lower ribbiness than those of the Great Lakes group. Cultivar 'Estival' showed consistent resistance to bolting, ribbiness, tipburn and rib discolouration across all E.  相似文献   
83.
    
Preface and acknowledgment  相似文献   
84.
数值求解矩形断面蜗壳   总被引:2,自引:0,他引:2  
为实现水流在蜗壳内的自由流动,给出了带有过渡圆弧的矩形蜗壳断面的数值求解原理及算法,显著地提高了蜗壳断面的设计精度及绘形精度。试验表明,给出的方法对改善泵效率指标有明显效果.  相似文献   
85.
Summary The effects of temperature and relative humidity on phenol-formaldehyde resin bonding were evaluated. Two flakes in a lap-shear configuration were bonded under an environment of controlled temperature (110 °C, 120 °C, 130 °C, 140 °C) and relative humidity (41%, 75%, 90%) for a series of time periods (0.25 to 16 min). The lap-shear specimens were then shear-tested on a mechanical testing machine and the results were used to establish a family of bond strength development curves at each temperature and level of relative humidity. At 110°C, the higher relative humidity appeared to retard resin bonding. The effects of relative humidity diminished as temperature increased to 140 °C. Bond strength development was chemical ratecontrolled. The rate of bond strength development at each relative humidity follows a first order reaction mechanism. The activation energy of resin-wood bonding, determined by bonding kinetics, was higher than that of resin alone, determined by differential scanning calorimetry. This comparison indicates that to form a strong resin-wood bond, a higher energy level might be required.This material is based on work supported by the Ministry of International Affairs, Quebec Government, the Natural Sciences and Engineering Research Council of Canada, and Laval University (Quebec City). The work was also supported by the U.S. Department of Agriculture under research joint venture agreement FP-92-1835  相似文献   
86.
This preliminary study evaluated phenoxymethyl penicillin (Penicillin V) as an alternative to parenteral administration of penicillin in horses. Penicillin V was administered orally to five horses at two different doses and plasma levels of the drug were determined at timed intervals. The results were evaluated by regression analysis. Following the administration of penicillin V at a dose of 66,000 IU/kg or 110,000 IU/kg, the mean peak plasma levels obtained were 1.55 micrograms/mL and 2.34 micrograms/mL respectively. A plasma level two to four times above the minimal inhibitory concentration level of Streptococcus equi and Streptococcus zooepidemicus was maintained for 325 minutes at 66,000 IU/kg and 349 minutes at 110,000 IU/kg. Penicillin V given orally was thus shown to be an acceptable alternative to parenteral administration of penicillin in the horse.  相似文献   
87.
  总被引:1,自引:0,他引:1  
Clinical and pathological features of ovarian dysgerminomas occurring in two dogs and a cat are presented. The feline neoplasm had morphological characteristics closely resembling those of dysgerminomas in women. The feline and one canine neoplasm occurred in young animals as compared to other reported animal dysgerminomas. Findings are discussed in relation to other reports of these tumors in animals and in women.  相似文献   
88.
Self-incompatibility in flowering plants prevents inbreeding and promotes outcrossing to generate genetic diversity. In Solanaceae, a multiallelic gene, S-locus F-box (SLF), was previously shown to encode the pollen determinant in self-incompatibility. It was postulated that an SLF allelic product specifically detoxifies its non-self S-ribonucleases (S-RNases), allelic products of the pistil determinant, inside pollen tubes via the ubiquitin-26S-proteasome system, thereby allowing compatible pollinations. However, it remained puzzling how SLF, with much lower allelic sequence diversity than S-RNase, might have the capacity to recognize a large repertoire of non-self S-RNases. We used in vivo functional assays and protein interaction assays to show that in Petunia, at least three types of divergent SLF proteins function as the pollen determinant, each recognizing a subset of non-self S-RNases. Our findings reveal a collaborative non-self recognition system in plants.  相似文献   
89.
Journal of Soils and Sediments - To understand the impact of geochemical sedimentation history for arsenic (As) distribution in the sediment profiles of the Hetao Basin, we (1) evaluated sediments...  相似文献   
90.
Pulmonary deposition and clearance of bacteria were measured in weanling pigs, half of which had been inoculated at age 31 days with larvated Ascaris suum ova. Seven days later, when breathing signs of larval migration were pronounced, all pigs were exposed to aerosolized Escherichia coli (strain B). Then, either immediately after aerosol exposure (for deposition assessment) or immediately after a 120 minute period in filtered air (for clearance), bacteria in the pigs' lungs were counted. Ascarid ova-inoculated pigs did not differ significantly from control pigs for number of bacteria in the lungs after aerosol exposure, but after the 120 minute clearance period they had 7.2 times more than did the control pigs. Thus, in weanling pigs, the breathing-pattern changes that were evident during ascarid-larval migration did not affect pulmonary deposition of inhaled bacteria significantly, but the presence of ascarid larvae in the lungs was associated with impaired pulmonary bacterial clearance.  相似文献   
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