Transverse impact characterization of carbon woven fabric-foam sandwich composites with carbon nanotubes

Different contents of carbon nanotubes were incorporated in an epoxy matrix that was then reinforced with carbon woven fabric and foam to manufacture the carbon woven fabric-foam sandwich composites. The transverse impact characterizations of the sandwich composites were reported. The split Hopkinson pressure bar apparatus were employed to test the transverse impact behaviors. The impact wave signals were recorded and the impact load versus displacement curves and impact damages of the sandwich composites were observed to analyze the energy absorption and the impact damage mechanisms. It was found that the failure area and energy absorption is increased as the increase of impact velocity and decrease of carbon nanotubes content. The main failure modes are foam breakage and the interface delamination between the woven fabric and foam.     

Woven Kenaf/Kevlar Hybrid Yarn as potential fiber reinforced for anti-ballistic composite material

Woven Kenaf/Kevlar Hybrid Yarn is the combination of natural and synthetic fibers in the form of thread or yarn. The yarn is weaved to form a fabric type of fiber reinforced material. Then, the fabric is fabricated with epoxy as the resin to form a hybrid composite. For composite fabrication, woven fabric Kenaf/Kevlar hybrid yarn composite was prepared with vacuum bagging hand lay-up method. Woven fabric Kenaf/Kevlar hybrid yarn composite was fabricated with total fiber content of 40 % and 60 % of Epoxy as the matrix. The fiber ratios of Kenaf/Kevlar hybrid yarn were varied in weight fraction of 30/70, 50/50 and 70/30 respectively. The composites of woven fabric Kenaf/Epoxy and woven fabric Kevlar/Epoxy were also fabricated for comparison. The mechanical properties of five (5) samples composites were tested accordingly. Result has shown that of value of strength and modulus woven fabric Kenaf/Kevlar Hybrid Yarn composite was increased when the Kevlar fiber content increased. Therefore, among the hybrid composite samples result showed the woven fabric Kenaf/Kevlar Hybrid Yarn composites with the composition of 30/70 ratio has exhibited the highest energy absorption with 148.8 J which 28 % lower than Kevlar 100 % sample. The finding indicated there is a potential combination of natural fiber with synthetic fiber that can be fabricated as the composite material for the application of high performance product.     

Nonwoven fabric/spacer fabric/polyurethane foam composites: Physical and mechanical evaluations

In the first stage, polyethylene terephthalate (PET) fibers and Kevlar fibers are combined at a blending ratio of 80/ 20 wt% in order to form PET/Kevlar nonwoven fabrics. Two pieces of PET/Kevlar nonwoven fabrics that enclose a carbonfiber (CF) interlayer are then needle punched in order to form PET/Kevlar/CF (PKC) composites. In the second stage, the sandwiches compose PKC composites as the top and the bottom layers, as well as an interlayer that is composed of a spacer fabric and polyurethane (PU) foam. PU foams have different densities of 200, 210, 220, 230, and 240 kg/m³. These resulting nonwoven fabric/spacer fabric/PU foam sandwiches are then tested using a drop-weight impact test, a compression test, a bursting strength test, a sound absorption test, and a horizontal burning test. The test results indicate that the optimal properties of sandwiches occur with their corresponding PU foam density as follows: an optimal residual stress (240 kg/m³), an optimal compressive strength (240 kg/m³), and an optimal bursting strength (220 kg/m³). In addition, the sandwiches reach the HF1 level according to the horizontal burning test results. They also have an average electromagnetic interference shielding effectiveness of -48 dB, as well as a sound absorption coefficient of 0.5 in a frequency between 1500-2500 Hz, which indicates a satisfactory sound absorption effect. The nonwoven fabric/spacer fabric/PU foam sandwiches proposed in this study are mechanically strong, sound absorbent, and fire retardant, and can be used in construction material and electromagnetic shielding composites.     

Mechanical properties of denim fabric reinforced poly(lactic acid)

Denim, a twilled cotton fabric, was used to enhance the mechanical and thermal properties of poly(lactic acid) (PLA). The denim fabric reinforced composites with different numbers of denim layers were fabricated by using a hand layup method. The impact, tensile, and dynamic mechanical properties of the composites were observed with increasing denim layers to examine the reinforcing effect of denim fabrics. Numerical analysis was carried out to model the elastic modulus of the composite by using a commercial software. Three-dimensional geometry of the denim fabric reinforced PLA composite was generated through a CAD program, and the elastic modulus was calculated by applying uniform deformation on one surface. The impact strength, tensile strength, and thermal properties of the composites were improved by piling denim fabrics. The denim fabric reinforced composites exhibited outstanding impact strength due to the retarded crack propagation as well as large energy dissipation. The 3 layer denim reinforced composite showed best results among all specimens, and its impact strength, tensile strength, and tensile modulus were measured to be 82 J/m, 75.76 MPa, and 4.65 GPa, respectively. The PLA/denim composites have good mechanical properties and can substitute traditional composites such as glass fiber or carbon fiber reinforced composites.     

Facile fabrication of carbon nanotubes/polystyrene composite nanofibers for high-performance electromagnetic interference shielding

Polystyrene (PS) composites with nanofibrous structure consisting of multi-walled carbon nanotubes (MWCNTs) with 0-10 wt.% of nanofiller have been fabricated via electrospinning technique. The surface morphology and thermal properties of the composites were evaluated by scanning electron microscopy (SEM) and thermo-gravimetric analysis (TGA). The SEM analysis of the composite nanofibers samples revealed that the average diameter of the nanofibers increases with increasing MWCNTs content. The resultant MWCNTs/PS composite nanofibers diameters were in the range of 391±63 to 586±132 nm. The thermal stability of composites was increased after addition of MWCNTs to PS matrix. The electrical conductivity of the composites with different weight percentage of MWCNTs was investigated at room temperature. Electrical conductivity of MWCNTs/PS composite nanofiber followed percolation theory having a percolation threshold V _c= 0.45 vol% (~0.75 wt. %) and critical exponent q=1.21. The electrical conductivity and thermal properties confirmed the presence of good dispersion and alignment MWCNTs encapsulated within the electrospun nanofibers. The electromagnetic interference (EMI) shielding effectiveness of the MWCNTs/PS composites was examined in the measurement frequency range of 8.2-12.4 GHz (X-band). The total EMI shielding efficiency of MWCNTs/PS composite nanofibers increased up to 32 dB. The EMI shielding results for MWCNTs/PS composite nanofibers showed that absorption loss was the major shielding mechanism and reflection was the secondary mechanism. The present study has shown the possibility of utilizing MWCNTs/PS composite nanofibers as EMI shielding/absorption materials.     

Evaluation of the Electromagnetic Shielding Effectiveness of Carbon-Based Screen Printed Polyester Fabrics

Electromagnetic shielding has a very emerging role in the textile applications. Screen-printing is a well-known, easy and cost effective process for textile printing. In this study, carbon black and graphite particles were used to impart electromagnetic shielding property to polyester fabric by screen printing technique. To this aim, printing pastes containing carbon materials were prepared with different binder concentrations. The electrical resistance, surface morphology, color coordinates and washing fastness properties of screen printed polyester fabrics were investigated. The washing durability of electromagnetic shielding effectiveness of carbon based printed fabrics as a function of binder concentration have also been studied. Electromagnetic shielding effectiveness was evaluated in the frequency ranges between 15-3000 MHz. The results showed that the electromagnetic shielding properties of fabric were affected by increased binder concentration. The most durable electromagnetic shielding effectiveness after washing process was obtained at highest binder concentration. The surface morphologies and color difference values of printed fabrics after washing process also provided a positive contribution.     

Carbon Nanostructures Based Mechanically Robust Conducting Cotton Fabric for Improved Electromagnetic Interference Shielding

Herein, an intelligent cotton fabric was fabricated using a non-ionic surfactant based macro structured carbonaceous coating through the ‘knife-over-roll’ technique. The developed novel fabric was tested as flexible, mechanically robust with prolonged chemical/moisture resistance. Various characterization techniques were thoroughly used to analyze the fabric. The as-prepared fabric shows an outstanding electromagnetic interference (EMI) shielding efficiency (SE) of about 21.5 dB even at the lowest possible coating thickness (0.20 mm) where the highest EMI SE of 30.8 dB is obtained at only 0.30 mm coating thickness over the X-band frequency range (8.2-12.4 GHz), possibly due to the three-dimensionally interconnected network structure of conducting carbon particles. The micro-computed tomography disclosed the porous architecture and “void-filler” arrangement within the fabrics. For the betterment of serviceability and practicability of the coated fabric, the water tolerance and contact angle studies were conducted. The relatively high contact angle than pure cotton fabric, and excellent water resistance after coating ensure improved endurance for external or industrial uses. Therefore, this proof-of-construct manifests commercialization of the developed fabric for multipurpose applications in a facile, less-hazardous and economical way.     

The modification of Kevlar fibers in coupling agents by <Emphasis Type="Italic">γ</Emphasis>-ray co-irradiation

Kevlar fibers were treated in three kinds of coupling agents’ solutions by Co⁶⁰ γ-ray co-irradiation. After the treatment, the interlaminar shear strength (ILSS) values of Kevlar fibers/epoxy composites were all improved. Surface elements of the fibers were determined by energy dispersive X-ray microanalysis (EDX). X-ray photoelectron spectroscopy (XPS) indicated that the oxygen/carbon ratio of the treated fibers was increased and Fourier transform infrared (FT-IR) spectrum confirmed the increase in the polar groups at the fiber surface. The tensile strength of the fibers was evaluated by statistical analysis using the Weibull distribution. The wettability of the fiber surface was also enhanced by the treatment. The possible mechanisms of γ-ray co-irradiation treatment are proposed by the radical reactions. The results indicated that γ-ray co-irradiation technique modified the physicochemical properties of Kevlar fibers and improved the interfacial adhesion of its composites.     

Comparative Performance of Copper and Silver Coated Stretchable Fabrics

The present work described the development of multifunctional, electrically conductive and durable fabrics by coating of silver and copper particles using a dipping-drying method. The particles were directly grown on fabric structure to form electrically conductive fibers. Particles were found to fill the spaces between the microfibers, and were stacked together to form networks with high electrical conductivity. The electrically conductive fabrics showed low resistance with high stretch ability. The utility of conductive fabrics was analyzed for electromagnetic shielding ability over frequency range of 30 MHz to 1.5 GHz. The EMI shielding was found to increase with increase in concentration of copper and silver particles. Furthermore, the heating performance of the copper and silver coated fabric was studied through measuring the change in temperature at the surface of the fabric while applying a voltage difference across the fabric. The maximum temperature (119°C for silver and 112°C for copper) were obtained when the applied voltage was 10 V. Moreover, the role of deposited particles on antibacterial properties was examined against pathogenic bacteria such as Staphylococcus aureus and Escherichia coli. At the end, the durability of coated fabrics was examined against several washing cycles. The fabrics showed good retention of the particles, proved by small loss in the conductivity of the material after washing.     

Polypropylene/high-density polyethylene/carbon fiber composites: Manufacturing techniques,mechanical properties,and electromagnetic interference shielding effectiveness

This study uses polypropylene (PP)/high-density polyethylene (HDPE) polyblends (80/20 wt.%) as matrices, which are then melt-blended with inorganic carbon fibers (CF) as reinforcement to form electrically conductive PP/HDPE composites. Tensile test, flexural test, Izod impact test, scanning electron microscopy (SEM), differential scanning calorimetry (DSC), and X-ray diffraction (XRD) are performed to evaluate different physical properties of samples. A surface resistance and electromagnetic interference shielding effectiveness (EMI SE) measurements are used to evaluate the electrical properties of the PP/HDPE/CF composites. Test results show that an increasing content of carbon fibers results in an 18 %, 23 %, and 60 % higher tensile strength, flexural strength, and impact strength, respectively. SEM results show that carbon fibers break as a result of applied force, thereby bearing the force and increasing the mechanical properties of composites. DSC and XRD results show that the addition of carbon fibers causes heterogeneous nucleation in PP/HDPE polyblends, thereby increasing crystallization temperature. However, the crystalline structure of PP/HDPE composites is not affected. Surface resistivity results show that 5 wt.% of carbon fibers can form a conductive network in PP/HDPE polyblends and reduce the surface resistivity from 12×10¹² ohm/sq to 4×10³ ohm/sq. EMI SE results show that, with a 20 wt.% CF and a frequency of 2-3 GHz, the average EMI SE of PP/HDPE/CF composites is between -48 and -52 dB, qualifying their use for EMI SE, which is required for standard electronic devices.     

An experimental investigation on the response of woven natural silk fiber/epoxy sandwich composite panels under low velocity impact

This paper presents results of dynamic deformation behavior of woven natural silk/epoxy sandwich composite panels. The specimens were prepared in configurations of reinforced woven natural silk fiber (RWNSF)/Epoxy/Foam, RWNSF/Epoxy/Coremat; RWNSF/Epoxy/Honeycomb and reinforced RWNSF/Epoxy (control material) using hand-lay-up method. Each of the three core material was sandwiched between reinforced woven natural silk fiber/Epoxy composite facesheet. Drop weight impact test was carried out under 32 J impact energy. Degree of damages inflicted on the contact surface, through thickness and rear surface were analyzed, sandwich composites performed better than the reinforced (control material). Failure mechanism involved interlaminar matrix cracking, layer debonding, delamination and fibre breakage.     

Process technology and performance evaluation of functional knee pad

In this study, Polylactic Acid (PLA) nonwoven fabric and thermoplastic polyurethane (TPU) honeycomb air cushion (TPU-HAC) were employed to form an impact resistant layer for functional knee pads. PLA nonwoven fabric has low manufacture cost and flexibility of the honeycomb air cushion improved the quality of functional knee pad sold in the market. This study focused on the strength of PLA nonwovens and the impact resistance of TPU honeycomb air pads. The PLA fibers and low-melting-point (low-Tm) PLA fibers are used as raw materials to fabricate PLA nonwoven fabric. The PLA fibers and low-melting-point PLA fibers were mixed at weight ratios of 10, 20, 30, 40, and 50 %. PLA nonwoven fabric and TPU-HAC materials were combined in a sandwich structure to protect against impact. Impact resistance was evaluated using a falling-weight impact-resistance machine. Experimental findings indicate that changing various layers can improve the impact resistance of the sandwich structure of the TPU-HAC materials. A TPU-HAC layer with a thickness of 2/8/10 mm optimized the impact resistance. In 25 J falling-weight impact test, the TPU-HAC layer 2/8/10 mm provides an impact resistance of 2932 N; the PLA/TPU-HAC composite had the best impact resistance; 2516 N. PLA nonwoven fabric had the best mechanical properties with low-Tm PLA fibers at 30 % weight. The impact resistance achieved using above combination of materials met the level 2, range 3 impact values mentioned in EN 14120 standards.     

Sound absorbent,flame retardant warp knitting spacer fabrics: Manufacturing techniques and characterization evaluations

This study proposes a combination for reciprocal reinforcement between warp knitting spacer fabrics and PU foams. PET/Kevlar nonwoven fabrics are made with an 80:20 ratio and an incorporation of various needle-punching speed of 100, 150, 200, 250, and 300 needles/min. Ascribing to having an optimal bursting strength, sound absorption coefficient, and limited oxygen index (LOI), the PET/Kevlar nonwoven fabric that is made by 200 needles/min are selected to be combined with a glass-fiber fabric by applying needle punch in order to form a surface layer. Next, warp knitting spacer fabrics and the nonwoven fabrics are laminated, followed by being combined with polyurethane (PU) foam that are featured with different densities of 200, 210, 220, 230, and 240 kg/m³ in order to form spacer fabric/PU foam composites with multiple functions. The composites are then tested with a drop-weight test, a compression test, a bursting strength test, a sound absorption test, and a horizontal burning test. The test results indicate that all spacer fabric/PU foam composites reach a horizontal burning level of HF1, and their sound absorption coefficients at 2500-4000 Hz also suggest a satisfactory sound absorption. In particular, the optimal residual stress and compressive strength are present when the composites contain 210 kg/m³ PU foam. Similarly, the optimal bursting strength of the composites occurs when they are composed of 230 kg/m³ PU foam. The spacer fabric/PU foam composites are proven to have high strengths, sound absorption, and fire retardant, and thus have promising potentials for use as construction materials and light weight composite planks.     

Matrix modification with silane coupling agent for carbon fiber reinforced epoxy composites

To improve interfacial adhesion between carbon fiber and epoxy resin, the epoxy matrix is modified with N-(2-aminoethyl)-3-aminopropylmethyldimethoxysilane (YDH602) and N-(2-aminoethyl)-3-aminopropyltrimethoxysilane (YDH792), respectively. And the effect of matrix modification on the mechanical performance of carbon/epoxy composites is investigated in terms of tensile, flexural and interlaminar properties. The flexural properties indicate that the optimum concentration of silane coupling agents YDH602 and YDH792 for the matrix modification is approximately 0.5 wt% of the epoxy resin system, and the mechanical properties of the YDH792-modified epoxy composites is better than that of the YDH602-modified epoxy composites at the same concentration. Compared to unmodified epoxy composite, the incorporation of 0.5 wt% YDH792 results in an increase of 4, 44 and 42 % in tensile, flexural and interlaminar shear strength (ILSS) values of the carbon/epoxy composite, respectively, while the corresponding enhancement of tensile and flexural modulus is 3 and 15 %. These improvements in mechanical properties can be considered to be an indication of better fiber/matrix interfacial adhesion as confirmed by SEM micrographs of the fracture surface after interlaminar shear testing. The viscosity of the modified epoxy resin system can be reduced by incorporation of silane coupling agent YDH792, which is beneficial for fiber impregnation or wetting during liquid composite molding process.     

Manufacturing technique and acoustic evaluation of sandwich laminates reinforced high-resilience inter/intra-ply hybrid composites

This study focused on the fabrication and acoustic property evaluation of sandwich cover-ply-reinforced highresilience thermal-bonding nonwoven hybrid composites. P-phenyleneterephthalamides and bicomponent high-resilience bonding polyester intra-ply hybrid nonwoven fabrics were compounded with glass plain fabric to produce the high strength sandwich structural cover ply by means of needle punching and thermal bonding to reinforce the whole composites and dissipate energy when being impacted. Then, the acoustic absorption properties of the homogenous intra-ply hybrid meshwork layer were investigated before and after being reinforced with the aforementioned cover ply. The influencing factors, including areal density, fiber blending ratio, needle punching depth, and air cavity thickness between back plate of the impedance tube and composites, were comparatively investigated. Results revealed that hybrid composites exhibited exceedingly high acoustic absorption properties. Acoustic absorption coefficients were promoted with increases in areal densities and fiber blending ratio of 3D crimped hollow polyester, particularly at low-mid frequency range. In addition, needle punching depths and back air cavity thicknesses considerably affected the average absorption coefficients. The meshwork center layer reinforced with sandwich structural cover-ply perform high resilience properties.     

Mechanical properties of uniaxial natural fabric Grewia tilifolia reinforced epoxy based composites: Effects of chemical treatment

The effects of chemical treatment on the mechanical, morphological, and chemical resistance properties of uniaxial natural fabrics, Grewia tilifolia/epoxy composites, were studied. In order to enhance the interfacial bonding between the epoxy matrix and the Grewia tilifolia fabrics, two different types of treatment: alkali treatment (5 % NaOH) and (3-aminopropyl)-triethoxysilane coupling agent (CA), were used. The epoxy composites containing 0–15 wt% of Grewia tilifolia fabric were prepared by hand lay-up technique, at room temperature. The tensile and flexural properties of the untreated, alkali-treated and coupling agent treated Grewia tilifolia reinforced epoxy composites were determined as a function of fabric loading. The 9 % wt Grewia tilifolia fabric reinforced epoxy composites showed improved tensile and flexural modulii when compared to the neat epoxy matrix. Significant improvement in the mechanical properties was obtained when both alkali and coupling agent treated fabrics were used as reinforcement. Morphological studies demonstrated that better adhesion between the fabrics and the matrix was achieved especially when the alkali-treated and coupling agent treated Grewia tilifolia fabrics were used in the composites. For the water absorption and chemical resistance studies, various solvents, acids and alkalis were used on the epoxy composites. This study has shown that Grewia tilifolia fabric/epoxy composites are promising candidates for structural applications, where high strength and stiffness are required.     

Ballistic-resistant stainless steel mesh compound nonwoven fabric

The energy of impact must decay and be transmitted after a bullet is shot through a ballistic-resistant cloth with a laminate structure. A rigid net structure transmits the impact stress to reduce the breakage of the material in the direction perpendicular to the fabric after the impacting of a projectile. This work combines the rigid net structure of stainless steel mesh with two layers a needle-punched polyamide nonwoven fabric to create a sandwich-like laminate structure. A compound fabric that is composed of a stainless steel mesh and polyamide nonwoven fabrics is placed in multi-layer Kevlar fabrics, and the buffer effect is measured by performing a dropping weight impact test and a bullet-shooting test. The specifications of the stainless steel mesh and the order of placement of the compound fabrics are varied to show the effect of these parameters on the energy of fracture propagation and the buffer effect of the multi-layered Kevlar compound fabric that includes a layer of compound fabric that is made of stainless steel mesh and polyamide nonwoven fabrics. In this study, the compound fabric replaces several layers of Kevlar unidirectional fabric, to be used to reduce the cost of bulletproof vests without reducing ballistic resistance.     

Enhanced Electromagnetic Interference Shielding Effects of Cobalt-Nickel Polyalloy Coated Fabrics with Assistance of Rare Earth Elements

Co-Ni-P coatings were prepared on ramie fabric by electroless plating with addition of rare earth (RE: Ce, Pr, and Nd). The proposed ultra-low-cost and easy-operated electroless plating method involved successive steps, namely, alkali mercerization, malic acid modification, Co nanoparticles activation, and Co-Ni-P deposition. FT-IR and XPS measurements were utilized to verify the functions of modification and activation procedures. Refined effects of Ce, Pr, and Nd on the structures and morphologies of resulting Co-Ni-P coatings were demonstrated by XRD and FE-SEM measurements. Moreover, by adding tiny dose of RE into the one-pot plating solution, electroless deposition rates were substantially accelerated in all cases. With regard to the resulting fabric-based Co-Ni-P coatings obtained in the presence of RE, not only mechanical durability but also chemical stability were improved. All Co-Ni-P coated fabrics displayed admirable electromagnetic properties and high electromagnetic interference (EMI) shielding effectiveness (SE). Owing to the benefits from RE, EMI SE values of Co-Ni-P shielding fabrics were enhanced with increment of 3-11 dB ranging from 30 to 6000 MHz. Significantly, Co-Ni-P-Nd coated fabric with uniform surface morphology and outstanding corrosion resistance possessed the highest EMI SE of 42.27-66.76 dB.     

Basalt nanoparticle reinforced hybrid woven composites: Mechanical and thermo-mechanical performance

Nanoparticles are gaining wider importance and increasing utility in many areas of engineering and technology. This investigative work is conducted to study the effect of incorporating basalt nano particles in composites with basalt/basalt and basalt/jute woven structures as reinforcement. The nanoparticles were developed from basalt, they were characterized and used for reinforcing composites of basalt and jute hybrid fabrics. The mechanical and thermo-mechanical properties of hybrid woven basalt reinforced epoxy composites were evaluated. Microscopic examination was carried out in order to analyze the internal structure and fractured surfaces. Interfacial characteristics, material morphology and failure was studied by use of Scanning Electron Microscope (SEM) and optical microscopy. Thermal stability was characterized by TGA. The results elaborated that the incorporation of basalt nanoparticles exhibited superior properties compared to the pure epoxy resin impregnated basalt fabric reinforced composites in terms of mechanical and thermal stability.     

Investigating ballistic impact properties of woven kenaf-aramid hybrid composites

In this study, the ballistic impact performance of woven kenaf-Kevlar hybrid and non-hybrid composites against fragment simulating projectiles (FSPs) was investigated. All the composites were prepared using the hand lay-up technique, method, followed by static load compression. The hybrid composites consist of Kevlar fabric and woven kenaf layers. The results obtained indicate that the energy absorption, ballistic limit velocity (V ₅₀) and failure behaviour of the composites during the impact event were affected by the woven kenaf hybridisation. The additional kenaf layers in hybrid composites resulted in the increase in composites thickness and areal density, thus increased the energy absorption (14.46 % to 41.30 %) and V ₅₀ (5.5 % to 8.44 %). It was observed that the hybrid composites failed through a combination of fibre shear, delamination and fibre fracture in the impacted surface, woven kenaf-Kevlar interface and rear surface respectively. Although the specific energy absorption was lower for the hybrid composites, further investigations need to be carried out to utilise the great potential natural fibres.