Corn yield variation as related to soil water fluctuation and nitrogen fertilizer. I. Soil water‐yield relationships

Abstract

The objective of this work was to study the effect of plant available soil water (PAW) in different soil layers before and during the growing season on corn yields (Zea mays L.) and to determine if the soil water may be a reliable index in forecasting the grain yield. The experiments were carried out for 10 years at the same site on a deep‐permeable well‐drained chernozem with good physico‐chemical and biological properties situated in a temperate‐continental dry climate with annual precipitation of about 500 mm and wide seasonal and annual fluctuation.

The results show that the maximum yields (MY) were highly correlated to water stored in the soil as well at the beginning as during the growing season. In most cases the yields were better correlated to PAW at the beginning of June (r = 0.96**) than at the beginning of March (r = 0.87**) or July (r = 0.91**). Nevertheless, the July PAW was more efficient in terms of yield per unit of PAW. Thus, 1 mm of PAW within 0–150 cm in March, June and July 1^st increases the MY by 16, 21 and 30 kg/ha of grain, respectively. The MY was more related to March and especially to June 1^st PAW (0–150 cm) than to June‐July precipitation.

The PAW from deeper soil layers was in almost all cases better correlated with MY and more efficient. Thus, for the PAW within 0–70 cm on March, June and July 1^st the simple correlation coefficients with yields were 0.69, 0.87** and 0.76* respectively while for the PAW within 0–150 cm the correlation coefficients were 0.87**, 0.96** and 0.91** respectively. Also, 1 mm of PAW within 0–100 cm on March, June and July 1st increases the yields by 23, 34 and 39 kg/ha while the PAW within 100–150 cm increases the yields by 40, 56 and 78 kg/ha respectively.

The results suggest that in this dry area the amount of yield is highly related to PAW at the beginning as well as during the growing season and that soil water may be a good index for forecasting yields as early as three month prior to harvest, except for years with weather accidents in late summer. They also show that PAW from deeper soil layers has a paramount effect on maximum corn yield.     

Dryland corn response to tillage and nitrogen fertilization. I. Growth‐yield‐N relationships

Abstract

Crop response to fertilizer nitrogen (N) is dependent upon tillage management. This study was conducted to determine how tillage rotation influences non‐irrigated crop growth, N uptake and yield. The effects of tillage rotation, N rate and N timing schedule on early season dry matter production and N uptake, ear leaf N concentration at silking, and yield of corn [Zea mays (L.) Pioneer 3378] were investigated at Painter, VA, on an Altavista loam (fine‐loamy, mixed, thermic Aquic Hapludult). In 1986, maximum yields achieved in the 6‐year continuous no till (NT) [5.82 Mg/ha] and first year no till (AT) [5.64 Mg/ha] were significantly greater than that of the 6‐year continuous conventional till (CT) [3.67 Mg/ha], but no yield differences were obtained in the drier 1987 season. A higher rate of N fertilizer was required to obtain maximum yield in the first year no till (168 kg N/ha) than in the NT (112 kg N/ha) during 1986. Early 1986 N uptake and growth response with and without N at planting increased in the order CT < AT = NT and AT < CT < NT, respectively, indicating greatest immobilization of soil N occurred in the newly established no till soil. Lack of differences in critical ear leaf N values developed for NT and CT in each year imply that plant norms developed for one tillage system may accurately assess N status of corn grown under different tillage practices.     

Relationship between soil‐test P and K and yield response of runner peanuts to fertilizer

Abstract

Direct fertilization of peanuts (Arachis hypogaeaL.) with P and K has generally shown few yield responses, resulting in only limited information concerning critical soil‐test levels of P and K. The purpose of the experiments in this report was to determine the critical soil‐test levels of P and K for runner peanuts using the double‐acid extraction procedure. Fertilizer experiments were conducted on farmers’ fields from 1973 to 1986. Site selection was based on soil test data that indicated “medium”; or “low”; levels of available P or K but “high”; in Ca and Mg. Phosphorus and potassium were applied together at all sites at rates of 20 and 74 kg/ha, respectively, as concentrated superphosphate and potassium chloride.

There were yield increases to fertilizer in 6 of the 39 experiments. Soil‐test P for these six ranged between 4 and 53 kg/ha; soil‐test K ranged between 10 and 31 kg/ha. Delineating the yield effect into their P and K components with the aid of multiple regressions of yield on soil test values showed that yield increases were due to the K component of the fertilizer. The critical soil‐test K value was calculated to be 37 kg/ha. Sound mature kernels (SMK) were generally unaffected by fertilizer.     

Cover crop nitrogen availability to conventional and no‐till corn: Soil mineral nitrogen,corn nitrogen status,and corn yield

Abstract

Understanding seasonal soil nitrogen (N) availability patterns is necessary to assess corn (Zea mays L.) N needs following winter cover cropping. Therefore, a field study was initiated to track N availability for corn in conventional and no‐till systems and to determine the accuracy of several methods for assessing and predicting N availability for corn grown in cover crop systems. The experimental design was a systematic split‐split plot with fallow, hairy vetch (Vicia villosa Roth), rye (Secale cereale L.), wheat (Triticum aestivum L.), rye+hairy vetch, and wheat+hairy vetch established as main plots and managed for conventional till and no‐till corn (split plots) to provide a range of soil N availability. The split‐split plot treatment was sidedressed with fertilizer N to give five N rates ranging from 0–300 kg N ha^‐1 in 75 kg N ha^‐1 increments. Soil and corn were sampled throughout the growing season in the 0 kg N ha^‐1 check plots and corn grain yields were determined in all plots. Plant‐available N was greater following cover crops that contained hairy vetch, but tillage had no consistent affect on N availability. Corn grain yields were higher following hairy vetch with or without supplemental fertilizer N and averaged 11.6 Mg ha^‐1 and 9.9 Mg ha^‐1 following cover crops with and without hairy vetch, respectively. All cover crop by tillage treatment combinations responded to fertilizer N rate both years, but the presence of hairy vetch seldom reduced predicted fertilizer N need. Instead, hairy vetch in monoculture or biculture seemed to add to corn yield potential by an average of about 1.7 Mg ha^‐1 (averaged over fertilizer N rates). Cover crop N contributions to corn varied considerably, likely due to cover crop N content and C:N ratio, residue management, climate, soil type, and the method used to assess and assign an N credit. The pre‐sidedress soil nitrate test (PSNT) accurately predicted fertilizer N responsive and N nonresponsive cover crop‐corn systems, but inorganic soil N concentrations within the PSNT critical inorganic soil N concentration range were not detected in this study.     

Rice yield and water use as affected by soil management practices

A field experiment was conducted at the Shenyang Experimental Station of Ecology, Chinese Academy of Sciences,to study the effects of soil management practices on water use and rice (Oryza sativa L.) yield in an axtuic brown soil during 2001 and 2002. A completely random experimental design with three replications was employed, having four soil management practices as treatments, namely: an undisturbed plow layer (CK), a thin plastic film (TN), a thick plastic film (TI) and subsoil compacting (CP). Results indicated no significant differences among all treatments for rice biomass and grain yields. Also, water consumption was about the same for treatments TN and CK, however the treatments TI and CP were much lower with more than 45% and 40% of the irrigation water in the treatments TI and CP, respectively,saved each year compared to CK. Therefore, water use efficiency was higher in the treatments TI and CP. These results will provide a scientific basis for the water-saving rice cultivation.     

Crop yield—nitrate‐n and total n and k concentration relationships: Corn and fescuegrass

Abstract

Six greenhouse pot experiments were conducted in which yield and nutrient uptake responses of corn (Zea mays L.) or tall fescue (Festuca arundinacea Shreb) to N, P, K, lime, or temperature variables were measured. This paper describes yield—NO₃‐N and total N concentration trends in these experiments. Crop concentrations of total N and NO₃‐N during early growth increased consistently with amount of applied N. These concentrations usually decreased (by dilution and assimilation) with time of growth and yield response to other growth‐limiting nutrients and other factors. Concentrations of K also increased in corn with amount of applied K, and high K was associated with higher concentrations of NO₃‐N during early growth in some experiments. This was usually true only for early crop growth periods during which rates of nutrient uptake exceeded growth rate. High K concentrations may have retarded growth and NO₃‐N reduction and assimilation.     

Relationships between nitrogen rate,plant nitrogen concentration,yield and residual soil nitrate‐nitrogen in silage corn

Abstract

Nitrogen (N) fertilizer is a key factor of yield increase but also an environmental pollution hazard. The sustainable agriculture system should have an acceptable level of productivity and profitability and an adequate environmental protection. The objectives of this study were to determine the relationships between N rate, DM yield, plant N concentration (NC) and residual soil nitrate‐nitrogen in order to improve the predicted N rate in corn (Zea mays L.) silage. The experiment was conducted over a period of three years in the province of Quebec on three soil series in a continuous corn crop sequence. Treatments consisted of six rates of N: O, 40, 80, 120, 160, and 200 kg N ha^‐1 as ammonium nitrate applied at planting: broadcast and side banded. Four optimum N rates were calculated using different models: (i) economic rate base on fertilizer and corn price using the quadratic model (E); (ii) economic rate based on fertilizer and corn price using the quadratic‐plus‐plateau model (QP); (iii) critical rate based on linear‐plus‐plateau model (P); (iv) lower than maximum rate (L) corresponding to 95% of maximum yield. The optimum plant NC at all growing stages and the N uptake at harvest were calculated depending on these N rates and yields.

The NC of whole plant at 8‐leaf stage (25–30 cm plant height) of ear leaf at tasselling and of whole plant at harvest stage, the N rate, the N uptake at harvest and the DM yield were all significantly intercorrelated and affected by soils and years, but not affected by N fertilizer application method. The DM yield was linearly and significantly related to NC of whole plant at 8‐leaf stage (rv = 0.932**). At this stage, the average NC corresponding to the optimum N rate and yield was of 3.71, 3.68, and 3.66% as calculated with E, L, and P model, respectively. Our data suggest that the NC of whole plant at 8‐leaf stage may be used to evaluate the N nutrition status of plant and the required optimum N fertilizer rate. The NC of ear leaf at tassel stage was also significantly correlated to corn yield (r = 0.994**). It may be used as an indicator to evaluate the near‐optimum N rate in the subsequent years.

The N uptake by whole above‐ground plant at harvest was quadratically related to corn yield. Data show that at high fertilizer N rate, the N uptake still increased without significantly increasing yield. The N uptake was of 176.5, 163.0, and 155.0 kg N ha^‐1 using the E, L and P rates of 146, 126, and 115 kg N applied ha^‐1, respectively. The optimum N rate and yield were affected by soil type and year, but not by the method of N fertilizer application. The yield increased rapidly up to a N rate of about 120 kg N ha^‐1 and then quite slightly to a maximum N rate of 192 kg N ha^‐1. The optimum N rate was of 115 and 126 kg N ha^‐1 using the P and L model respectively and as high as 146.8 kg N ha^‐1 using the E model. The L model, using a much smaller N rate, gave a reasonably high yield compared to E rate (12.2 and 12.5 Mg ha^‐1, respectively). The data show that a relatively much lower N rate than maximum did not proportionally diminish the yield. Thus, for a difference of 40.4% between maximum N rate and P rate a difference of only 7.4% in yield was observed. Using the L model the differences in rate and yield were of 34.4% and 4.7%, respectively. The QP model gave no significant difference compared to E model.

At harvest the residual soil NO₃‐N increased significantly with increasing N fertilizer rate in whole of the 100 cm soil profile, but mainly in the top 40 cm soil layer. The total NO₃‐N found in 0–100 cm profile at rate of 0, 120 and 200 kg applied N ha^‐1 at planting was as high as 33.7, 60.5, and 74.5 kg N ha^‐1 respectively in a light soil and 37.5, 97.5, and 145.5 kg N ha^‐1 in a heavy clay soil. The difference in NO₃‐N content in the 60–100 cm layer between different applied N rate suggests that at harvest, part of fertilizer N applied at planting was already leached below the 100 cm soil layer. Results, thus, show that reasonably high corn yields can be obtained using more adequate N fertilizer rates which avoid the overfertilization and are likely to reduce the air and ground water pollution.     

Pressurized Hot Water and DTPA‐Sorbitol as Viable Alternatives for Soil Boron Extraction. II. Correlation of Soil Extraction to Responses of Boron‐Fertilized Alfalfa

Abstract

Pressurized hot water and DTPA‐Sorbitol are two relatively new, proposed alternative soil boron (B) extraction methods for which no data on yield or plant nutrient uptake have been reported for validation. Both methods initially have shown significant correlation with the hot water extraction method in untreated soils as well as soils incubated with various levels of B. The objective of the research was to extract samples of B‐treated soils by using all three extraction methods and correlate the B values obtained to yield, B tissue concentration, and total B removal of alfalfa (Medicago sativa). Greenhouse and field experiments on alkaline and limed acid soils naturally low in hot water‐extractable B were conducted to test alfalfa response to B fertilizer. In the greenhouse, highly significant relationships exist between plant uptake and extractable B with all three methods at varying levels of applied B, but no alfalfa yield response was observed. All three methods result in accurate predictions of plant B tissue concentrations and total B removal. The field experiment exhibited a significant positive relationship between total alfalfa yield and extractable B using hot water and pressurized hot water extractions. Extractable B using DTPA‐Sorbitol was not related to total alfalfa yield in the field experiment. This work, coupled with the earlier incubation studies, supports the pressurized hot water extraction method as an improvement over hot water in diverse soil types. The lack of relationship in the acid soil supports DTPA‐Sorbitol as an improvement over hot water in alkaline soils.     

Response of wheat cultivars to different soil nitrogen and moisture regimes: II. Nitrogen up‐take,partitioning and influx 1

Nitrogen (N) is one of the major mineral nutrients required for growth and development of plants. Soil water availability, N concentration at the root surface and the ability of plants to absorb N are the most important factors that affect N uptake and partitioning. The objective of this study was to use greenhouse and growth chamber environments to investigate how two contrasting water regimes (stress and nonstress) and different soil N concentrations affect the uptake and distribution of N among different plant parts of three cultivars of wheat (Triticum aestivum L.) at different stages of development Results showed that at the beginning of stem elongation and under non N limiting conditions, there was a high and positive correlation between shoot dry matter production and shoot N content. Under N deficient soils that received different N rates, shoot N content was more related to shoot N concentration than to dry matter. Root growth and N content of the ‘Saada’ cultivar were negatively affected by high soil N concentration. Under mild water stress or nonstressed conditions, N uptake by the shoot increased with increased soil N in all cultivars. Overall, severe water stress masked the effect of N supply, and decreased N uptake in the case of ‘Merchouch 8’ and ‘Saada’. Root N content was not affected by water stress but increased when N was supplied. At anthesis and after rewatering plants from boot stage to anthesis, the plants fully recovered, and those that were water stressed, increased their N absorption to a rate much higher than those that were stressed. Nitrogen influx (NI) decreased with water stress, but increased more with increased soil N under well watered conditions than under stress. “Merchouch 8’ had higher NI than ‘Saada’. From this study we can conclude that the effect of N supply on N content was masked by severe water stress, and ‘Nesma’ was less sensitive to this stress. At anthesis, plants that were previously water stressed increased their rate of N uptake during the recovery. Root N was not affected by water stress but increased when soil N was increased.     

No‐tillage corn response to placement of fertilizer nitrogen,phosphorus, and potassium

Abstract

Fertilizer placement for corn (Zea mays L.) has been a major concern for no‐tillage production systems. This 3‐yr study (1994 to 1996) evaluated fertilizer phosphorus (P) or potassium (K) rates and placement for no‐tillage corn on farmers’ fields. There were two sites for each experiment involving fertilizer P or K. Treatments consisted ofthe following fertilizer rates: 0,19,and 39 kg P ha^‐1 or 0, 51, and 102 kg K ha^‐I. The fertilizer was broadcast or added as a subsurface band 5 cm beside and 5 cm below the seed at planting. Early plant growth, nutrient concentrations, and grain yields were measured. At the initiation of the study, soil test levels for P and K at the 0–1 5 cm depths ranged from optimum (medium) to very high across sites. Effects of added fertilizer and placement on early plant growth and nutrient concentrations were inconsistent. Added fertilizer had a significant effect on grain yields in two of twelve site‐years. Therefore, on no‐tillage soils with high fertility, nutrient addition, and placement affected early plant growth and nutrient utilization, but had limited effect on grain yield. Consequently, crop responses to the additions of single element P or K fertilizers under no‐tillage practices and high testing soils may not result in grain yield advantages for corn producers in the Northern cornbelt regardless of placement method.     

Sulphur fertilizer effect on cotton: I. Nitrogen and sulphur status and petiole nitrate‐nitrogen

Abstract

The effect of S fertilization on S and N status and petiole NO₃ ^?‐N in cotton was observed during the growing seasons of 1980 and 1981. Four sites representing 2 soil subgroups were studied using a randomized complete block design with 4 replications. Leaf and petiole sampling began one week prior to bloom initiation and continued weekly for eight weeks. Leaf samples were analyzed for S and N and the petioles for NO₃ ^?‐N. Levels of leaf‐S varied directly with amounts of applied S. Leaf‐N and petiole NO₃ ^?‐N varied directly with amounts of applied N. Though not always significant, petiole NO₃ ^?‐N and leaf‐N showed negative correlations with leaf‐S. These results suggest that knowledge of the cotton plant S status may be necessary to interpret petiole NO₃ ^?‐N for N fertilization of cotton.     

Response of summer‐planted potatoes to level of applied nitrogen and water

The irrigation and nitrogen (N) requirements of potatoes (cv. Delaware) were determined using sprinklers in a line‐source design on a Spearwood sand. Irrigation water was applied at 73 to 244% of the daily pan evaporation (Epan) and N at 0 to 800 kg N ha^‐1 (total applied) as NH₄NO₃ in 10 applications post‐planting. There was a significant yield (total and marketable) response to irrigation, at all levels of applied N, and N at all levels of applied water (P<0.001). The interaction between irrigation and N was also significant (P<0.001). There was no significant yield response to irrigation from 149% Epan (i.e., W3 treatment) to 244% Epan (i.e., W6 treatment). Irrigation at 125 and 150% of Epan was required for 95 and 99% of maximum yield, respectively, as determined from fitted Mitscherlich relationships. Critical levels of N required for 95 (417 kg ha^‐1) and 99% (703 kg ha^‐1) of maximum yield were also determined from a Mitschlerlich relationship fitted to the average of the W3 to W6 treatments. The percent total N and nitrate‐N in petioles of youngest fully expanded leaves required for 95 and 99% of maximum yield was 1.78 and 2.11, respectively, at the 10 mm tuber stage, and 0.25 and 0.80% at the 10mm plus 14 day stage (from quadratic regressions). There was a significant (P≤0.001) increase in N uptake by tubers with level of applied N from 57 kg ha^‐1 at 0 kg applied N ha^‐1 to 190 kg ha^‐1 at 800 kg applied N ha^‐1 (from a Mitscherlich relationship fitted to the average of W3 to W6 treatments). After accounting for N uptake from soil reserves (57 kg N ha^‐1), apparent recovery efficiency (RE) of fertilizer N by tubers [RE=(Up‐Uo/Np) where Up=uptake of N by the crop, Uo=uptake in absence of applied N and Np is the level of applied N, expressed as a fraction] declined from 0.28 at 100 kg applied N ha^‐1 to 0.17 at 800 kg applied N ha^‐1. There was a linear increase in ‘after cooking darkening’ (i.e., greying) of tubers with increasing level of applied N. Conversely, ‘sloughing’ (i.e., disintegration) of tubers decreased (inverse polynomial) with increasing level of applied N. Rate of irrigation had no effect on these cooking qualities. Reducing applied irrigation and N from levels required for 99% of maximum yield to levels required for 95% of maximum yield would not lead to a significant reduction in profit. This would increase apparent recovery efficiency of applied N by plants, maintain tuber quality, and reduce the impact of potato production on the water systems of the Swan coastal plain.     

Forage yield and crude protein of interseeded legume‐bermudagrass mixtures as affected by phosphorus fertilizer 1

Bermudagrass (Cynodon dactylon L.) is a warm season perennial that is well adapted in the southern Great Plains. It is one of the region's most important forage crops used for livestock production, and is commonly grown without legume interseeding. Recent research has investigated ways of improving the quality and quantity of this forage. The objectives of this study were to determine the effect of interseeded legumes and phosphorus (P) fertilizer on bermudagrass pasture forage yield and crude protein content. One experiment was initiated in 1993 in eastern Oklahoma in an established bermudagrass pasture. Red clover (Trifolium pratense L.), ladino clover (Trifolium repens L.), and two varieties of alfalfa (Medicago sativah), ’alfagraze’ and'common’, were interseeded by hand into an established stand of bermudagrass. The effect of P on forage yield and crude protein was evaluated using a 30‐kg P ha^‐1 rate applied at establishment versus no applied P. Forage yield was collected three times throughout the growing season each year from 1994 through 1997. When both alfalfa varieties were interseeded into a bermudagrass pasture without applying additional P fertilizer, forage yields for the legume‐grass mixtures decreased below those obtained from the monoculture bermudagrass in the first year of the stand. The alfalfa variety ‘alfagraze’ interseeded into established bermudagrass decreased total forage yield over the entire 4‐yr study. Interseeded red clover and ladino clover increased crude protein of the forage compared with monoculture bermudagrass the first two years of the study, with red clover continuing to increase crude protein in the fourth year. However, when 30 kg P ha^‐1 was applied to the bermudagrass prior to establishment of the legumes, no change in yield or protein was observed for both alfalfa varieties’ interseeding treatments versus the unfertilized mixtures. Although forage yield may not be increased, interseeding legumes into established bermudagrass could provide an efficient way to improve pasture crude protein without the use of inorganic fertilizers. However, if alfalfa ('common’ or ‘alfagraze') is interseeded, additional P may need to be applied at legume establishment to prevent possible yield decreases.     

Dry matter yield and nitrogen recovery from bromegrass in south‐central Alberta as affected by rate of long‐term nitrogen applications

Abstract

A field experiment was conducted on a Thin Black Chemozemic soil at Crossfield in south‐central Alberta to determine the effect of long‐term application of ammonium nitrate on dry matter yield (DMY), protein yield (PY), protein concentration, N use efficiency and recovery of N applied to bromegrass (Bromus inermis Leyss.) grown for hay. The N fertilizer was applied at 0, 56, 112, 168, 224, 280, and 336 kg N/ha in early spring of every year from 1968 to 1986. The DMY increased with applied N achieving a maximum at 224 kg N/ha, though the rate of increase in DMY from N fertilization was greatest with the first two increments applied (i.e. 56 and 112 kg N/ha). Protein yield and protein concentration maximized at 336 kg N/ha. The DMY was greater with a single‐cut system than with a double‐cut system. The DMY varied from year to year, but it was not closely related to precipitation received during the April to August period (R² = 0.37). However, in some years low DMYs were associated with low precipitation, or a lack of timeliness of rainfall, or a combination of both. The N use efficiency and % N recovery in bromegrass decreased with increasing N rate. The maximum DMY calculated from quadratic regressions ranged from 3.16 t/ha to 7.91 t/ha, and maximum N rate ranged from 205 to 258 kg N/ha. In summary, DMY, PY, and protein concentration increased, and N use efficiency and % N recovery decreased with increasing N rate in this 19‐year study.     

Monthly variation of forage and soil minerals in central Florida. I. macro‐minerals

Abstract

A two‐year study was conducted to determine the macromineral status of cattle grazed forages, mostly bahiagrass, and soils in central Florida. Soil and forage samples were collected every month for two years. Month differences (P < 0.01) were observed in all forage macrominerals and in crude protein (CP) for both years. No month effect (P > 0.05) was observed in IVOMD level during year 1. Year effects (P < 0.05) were observed in calcium (Ca), sodium (Na) and CP. Concentrations below the critical level were observed in all macrominerals studied. Higher forage macro‐mineral concentrations were found during spring‐summer months. In general, higher (P < 0.05) soil aluminum (Al), Ca, magnesium (Mg), phosphorus (P), and organic matter (OM) were observed during fall‐winter months, while Na was higher in winter. Soil Ca and Mg were adequate and potassium (K), Na and P were deficient. Year 2 showed higher (P < 0.05) soil macromineral concentrations. Correlation coefficients (r >|0.5|, P < 0.05) were present between forage K and forage CP (r = 0.557) and between forage P and forage CP (r = 0.554). Low correlations were found between soil and forage macrominerals. Percentages of total forage samples with macromineral and CP concentrations below critical levels (in parentheses) and suggestive of deficiency were as follow: in forage, Ca (0.30 ppm), 21%; Mg (0.18 ppm), 34%; K (0.60 ppm), 47%; Na (0.06 ppm), 89%; P (0.25 ppm), 85%; and CP (7%), 18%.     

Comparing tests for soil fertility. II. The hydrogen peroxide/sulfuric acid treatment as an alternative to the copper/selenium catalyzed digestion process for routine determination of soil nitrogen‐kjeldahl

Abstract

A two‐step digestion with hydrogen peroxide (H₂O₂)/boiling sulfuric acid (H₂SO₄) ("peroxy treatment") in the absence of heavy metals catalysts is proposed as an alternative to the copper (Cu)/selenium (Se) catalyzed digestion process for the routine determination of soil Kjeldahl‐nitrogen (N). Sixty‐eight samples from pedotypes representative of the Mediterranean environment, with contrasting features and use, were chosen in order to ensure the largest variability of total N and organic carbon (C) contents. The average soil N content was 0.223 g/100g for the H₂O₂ treatment, and 0.196 g/100g for the Cu/Se one, with significant difference between the means and with limits ranging from 0.042 to 0.678 and from 0.025 to 0.696 g/100g for H₂O₂‐N and Cu/Se‐N, respectively. The amounts of soil N determined by the contrasted procedures were strictly dependent on the respective organic C contents, and they correlated each other by the highly significant linear regression: Cu/Se‐N = ‐0.017 + 0.955/H₂O₂‐N, R² = 0.910***. The goodness of fit of this equation was not significantly improved when the organic C and the Al‐Oxa contents were introduced as accessory explanatory variables in multiple regression models. This should allow an easy and quick data conversion with no need of additional laboratory analyses. Altogether, the achieved results clearly show that the tested methods work with homogeneous performance under a range of soil properties, providing evidence that the current digestion procedure by heavy metals catalysts could be conveniently replaced by the less hazardous “peroxy”; treatment. This really represents an attractive innovative procedure for routine determination of soil Kjeldahl‐N with reference to the environment safety concerns.     

Pressurized Hot Water and DTPA‐Sorbitol as Viable Alternatives for Soil Boron Extraction. I. Boron‐Treated Soil Incubation and Efficiency of Extraction

Abstract

Serious challenges associated with hot water extraction, the standard extraction method for water‐soluble boron (B), limit its use in commercial soil‐testing laboratories. Several alternatives to make B testing more practical have been proposed and studied; none of the alternatives have readily replaced the hot water method. Two relatively new, promising B extraction methods are pressurized hot water and DTPA‐Sorbitol. Very little reported work compares B extraction values obtained from the standard hot water extraction method and these two alternative methods. This study was conducted to complete an initial step in validating new procedures—extracting the designated nutrient from fertilized, incubated soils by using standard and alternative extraction methods and comparing the resulting values. The three extraction methods were used to extract B from samples of calcareous sand and silt loam soils and limed, loamy fine sand, all which had been treated with 10 levels of B (0–8 mg kg^?1) and incubated for 7 and 28 days. The amount of B extracted increased as the rate of B application increased with all three soil‐extraction methods. High correlations (r 0.977–0.999) were observed between extractable B and rate of B application with all three procedures. Correlations between the amount of extractable B using hot water extraction and the value obtained with an alternative extraction method were similar for both methods (r=0.89). Hot water generally extracted the least and pressurized hot water the most B regardless of soil type, rate of application, or duration of incubation. This study suggests the more easily used methods of pressurized hot water and DTPA‐Sorbitol could be recommended as replacements to the cumbersome hot water extraction.     

Effect of addition of organic residues,farmyard manure and fertilizer nitrogen on soil fertility in rice‐wheat cropping system

A field experiment was conducted for 3 crop years (July‐June) at the Indian Agricultural Research Institute, New Delhi to study the effects of Sesbania and cowpea green manuring (GM) and incorporation of mungbean residues after harvesting grain, Leucaena loppings, FYM and wheat straw incorporation before planting rice and application of 0,40,80 and 120 kg N ha^?1 to rice on the soil organic carbon (SOC), alkaline permanganate oxidizable N (APO‐N), 0.5 M sodium bicarbonate extractable P (SBC‐P) and 1N ammonium acetate exchangeable K (AAE‐K) in surface 0–15 cm soil after the harvest of rice and wheat grown in sequence. Green manuring and addition of organic residues prevented the decline in SOC. On the other hand addition of N fertilizer tended to decrease SOC after rice harvest. On the contrary application of green manures, organic residues, FYM and fertilizer N increased APO‐N, which indicates the benefit of these treatments to a more labile soil organic N pool. Also application of green manures, organic residues, FYM and fertilizer N increased SBC‐P. Not much change was observed in AAE‐K by the treatments applied.     

Effect of no‐tillage vs. conventional tillage on soil organic matter and nitrogen contents

Abstract

Four treatments (no‐tillage plus subsoiling, no‐tillage, conventional tillage plus subsoiling, and conventional tillage) were continuously in place for 6 yr and a second set of no‐tillage plus subsoiling and conventional plus subsoiling treatments were continuously in place for 3 yr to study the long‐term effects of conventional and no‐tillage corn on soil organic matter (OM) and N contents. Soil samples were taken at random between the rows and in the rows to a depth of 60 cm, in 5‐cm increments to a depth of 30 cm, and then in 15‐cm increments from the 30 to 60‐cm depth for OM and N determination. No‐tillage resulted in A3 and 20% more Kjeldahl N than conventional tillage in the 0 to 5‐cm soil depth after 6 and 3 yr, respectively. after 6 yr, the 0 to 5‐cm depth had 36% more OM in no‐tillage treatments than in conventional tillage treatments, and soil from no‐tillage treatments averaged 27% more OM than the conventional tillage plus subsoiling treatment at the 0 to 15‐cm soil depth.