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<正> 目前饲料粗蛋白的测定,国内普遍使用的仍是将样品置于凯氏瓶中在普通电炉上加热消化,然后用半微量凯氏定氮仪蒸馏测定。电炉加热消化样品耗电量大,时间长,放样少,控温不便,受热不均;用半微量凯氏定氮仪蒸馏测定,需转移样液,手续繁琐,蒸馏测定时间长,所以均有缺点。辽宁省农科院根据饲料粗蛋白国标测定法的基本要求,结合本单位多年使用LNK801、804远红外消煮炉的经验,并参照日本快速分解装置及瑞典Tecator蛋白质自动测定系统,研制了LNK882饲料用多功能快速消化器和LNK871凯式定氮快速蒸馏器,并进行了与普通电炉消化饲料及半微量凯氏定氮仪蒸馏测定的比较试验。试验材料选用鸡饲料、虾饵料、鱼粉、骨肉粉、豆粕。消化及蒸馏测定方法执行国标法GB6432—86。  相似文献   

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《饲料工业》2017,(12):55-58
粗蛋白质是饲料的重要指标,也是饲料产品的必检指标。本试验选择采用传统的半微量定氮法和两种不同型号的全自动凯氏定氮仪法对10种蛋白饲料原料中的粗蛋白质含量进行检测,分析不同方法的准确度,为饲料质量检测分析检测技术提供参考。试验结果表明,全自动凯氏定氮仪更适合大批量样品的检测,而且检测精度更高。  相似文献   

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饲料中硝态氮对燃烧法与凯氏法总氮含量测定结果的影响   总被引:1,自引:1,他引:0  
为了确定硝态氮对饲料含氮量的杜马斯燃烧法测定值(Cn)和凯氏法测定值(Kn)的影响,对14种硝态氮含量较高的饲料原料,采用杜马斯燃烧法和凯氏法测定各样本中的含氮量,并以化学法测定硝态氮含量为对照进行分析。结果表明:14种样本含氮量的燃烧法测定值显著高于凯氏法测定值(P<0.01),虽然2种方法测定结果间高度相关(r=0.9960),但拟合曲线与Y=X存在显著差异(P<0.01),燃烧法与凯氏法测定值间差值(Cn-Kn)与饲料中硝态氮含量相关性低(R2=0.6036)。由此可得出,当饲料中含有大量硝态氮时,燃烧法测定值显著高于凯氏法测定值,但2种方法测定值差与硝态氮含量相关性低,因此硝态氮是造成饲料含氮量的燃烧法与凯氏法测定值间差异的原因之一,但不是惟一原因。  相似文献   

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吴凡 《江西饲料》2011,(2):31-32
通过国标法(-B6435—86,简称GB法)、国标改进法(简称改进法)和Shl0A水分快速测定仪法(简称仪器法)3种方法测定饲料中水分含量,并对试验数据进行数理统计分析,结果表明:3种方法无显著性差异。  相似文献   

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本文采用化学分析及仪器分析两种测试方式,对饲料样品的粗蛋白质含量进行分析检验,旨在探讨两种分析测试方法的测量误差,经统计分析,两种测试方法的分析结果无显著差异。同化学分析法相比较,FossTecator2300凯氏定氮仪具有自动化程度高、分析速度快、分析数据准确等优势。  相似文献   

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本文采用Foss2300公司全自动定氮仪,应用GB/T6432—94国标凯氏法测定试样中的含氮量方法,对饲料苜蓿中粗蛋白的含量进行测定。即样品中的含氮物质在混合催化剂的作用下用浓硫酸破坏有机物,使含氮物转化成硫酸铵。加入强碱进行蒸馏使氮选出,用硼酸吸收,再用盐酸滴定。测出氮含量乘以换算系数6.25,得出粗蛋白的含量。  相似文献   

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双缩脲法和凯氏定氮法测定饲料中蛋白质含量的比较研究   总被引:3,自引:0,他引:3  
蛋白质含量是饲料质量控制的重要指标之一.本实验用凯氏定氮法和双缩脲法测定饲料中蛋白质含量作对比实验.结果表明这两种方法所得实验结果差异较大,双缩脲法测得结果较凯氏法低约15.1%,且结果不稳定,不适于饲料蛋白质含量的测定.  相似文献   

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三种测定饲料水分含量的方法比较   总被引:1,自引:0,他引:1  
通过国标法(GB6435-86,简称GB法)、国标改进法(简称改进法)和Sh10A水分快速测定仪法(简称仪器法)三种方法测定饲料中水分含量,并对试验数据进行数理统计分析,结果表明:三种方法无显著性差异。  相似文献   

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通过国标法(~B6435—86,简称GB法)、国标改进法(简称改进法)和Shl0A水分快速测定仪法(简称仪器法)三种方法测定饲料中水分含量,并对试验数据进行数理统计分析,结果表明:三种方法无显著性差异。  相似文献   

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快速检测是有效的控制饲料原料和产品质量的重要手段,为此国家“八五”科技攻关项目中确立了“饲料蛋白质快速检测技术研究”子专题。经科技人员刻苦攻关,研究建立了快速测定饲料中粗蛋白质的方法(DirectDistillation法)简称DD法。该方法准确度和精密度与国标法(GB/T6432─94)一致,检测速度比国标法提高10倍。关于DD法快速测定猪、鸡配合饲料粗蛋白质的研究,我们已作了报道(《中国饲料》)1994.9期),本文主要介绍测定几种饲料原料的DD法。l材料与方法1.l检测样品玉米、麸皮、豆粕、菜籽饼1.2仪器设备GC─N蒸馏装置;自动…  相似文献   

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顾问刘中一张德邻宋瑞祥聂振邦张子仪戎易王维四会长白美清国务院原副秘书长、第四届理事会会长常务副会长(8人,以姓氏笔划为序)刘永好新希望集团董事长、第四届理事会副会长刘汉元通威股份有限公司董事长、第四届理事会副会长陈丹广东恒兴集团股份有限公司董事长、第四届理事会副会长张延喜农业部原副部长、第四届理事会副会长吴明夏湖南正虹科技发展股份有限公司董事长、第四届理事会副会长陶一山唐人神集团股份有限公司董事长、第四届理事会副会长温鹏程广东温氏食品集团有限公司董事长、第四届理事会副会长谭竹洲原化学工业部副部长、第…  相似文献   

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Progesterone levels in peripheral blood of dogs were analysed during the cycle in which hysterectomy (n = 5) or sham surgery (n = 3) was performed as well as during the cycle of dogs (n = 5) hysterectomized at least one year prior to this study; the data were compared with the findings in control dogs (n = 3). The averages of the duration of the luteal period observed in the three experimental groups were not significantly different from those of control dogs. Immediately after surgery, the progesterone level decreased from 25 to 50% of the presurgical level, but returned to presurgical level in about four days. Prolactin levels were elevated for about 30 h after surgery. Nevertheless, the averages of the mean prolactin levels for each animal during the luteal period of the experimental groups were not significantly different from those of control dogs. It is concluded that in the dog, the uterus is not involved in the lifespan of the cyclic corpus luteum.  相似文献   

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对症用药就是通过对患病信鸽的症状进行诊断,进而确定病属,选择药物及如何用药的方法。  相似文献   

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嗅源是军犬嗅觉作业训练的依据.军犬鉴别中嗅源能力的培养在整个鉴别训练中占有重要地位,关系到鉴别训练的成败和鉴别能力的提高.所以,军犬在嗅认嗅源时必须按照训犬员的指令充分、细致地感受嗅源气味,并且对嗅源气味产生兴奋反应.如何培养军犬充分嗅认嗅源以及及时解决嗅认过程中出现的问题,成为我们进行鉴别训练的关键.……  相似文献   

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As there is no statistical evidence that saddle fit influences the load exerted on a horse's back, this study was performed to assess the hypothesis that the width of the tree significantly alters the pressure distribution on the back beneath the saddle. Nineteen sound horses were ridden at walk and trot on a treadmill with three saddles differing only in tree width. Kinetic data were recorded by a sensor mat. A minimum of 14 motion cycles were used in each trial. The saddles were classified into four groups depending on fit. For each horse, the saddle with the lowest overall force (LOF) was determined. Saddles were classified as "too-narrow" if they were one size (2 cm) narrower than the LOF saddle, and "too-wide" if they were one size (2 cm) wider than the LOF saddle. Saddles two sizes wider than LOF saddles were classified as "very-wide". In the group of narrow saddles, the pressure in the caudal third (walk 0.63 N/cm(2)+/-0.10; trot 1.08 N/cm(2)+/-0.26) was significantly higher compared to the LOF saddles (walk 0.50 N/cm(2)+/-0.09; trot 0.86 N/cm(2)+/-0.28). In the middle transversal third, the pressure of the wide saddles (walk 0.73 N/cm(2)+/-0.06; trot 1.52 N/cm(2)+/-0.19) and very-wide saddles (walk 0.77 N/cm(2)+/-0.06; trot 1.57 N/cm(2)+/-0.19) was significantly higher compared to LOF saddles (walk 0.65 N/cm(2)+/-0.10/ 0.63 N/cm(2)+/-0.11; trot 1.33 N/cm(2)+/-0.22/1.27 N/cm(2)+/-0.20). This study demonstrates that the load under poorly fitting saddles is distributed over a smaller area than under properly fitting saddles, leading to potentially harmful pressures peaks.  相似文献   

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