镍钴硫化物的制备及其反应温度对形貌和超级电容器性能的影响

采用一步溶剂热合成法制备了镍钴硫化物纳米微球,利用X射线衍射光谱（XRD）、扫描电子显微镜（SEM）和X光电子能谱（XPS）对制备的材料进行了表征。采用循环伏安和恒电流充放电等电化学方法考察了镍钴硫化物用作超级电容器的电极材料的性能。160℃制备的材料在2 mA/cm²的电流密度下,测得的质量比电容和面积比电容分别为1 298 F/g和1.13 F/cm²。在电流密度为10 mA/cm²下,经过10 000圈的循环稳定性测试后,比电容保持了原来的70.8%。此外,通过对反应温度的控制,研究了反应温度对其超级电容器性能的影响。结果表明,反应温度对生成物的形貌几乎没有什么影响,对其电化学性能有一定的影响。     

灰褐链霉菌对淀粉糖工业副产物糖渣发酵利用的研究

将淀粉糖工业中的副产物糖渣作为营养物质加入到灰褐链霉菌发酵生产ε-聚赖氨酸的培养基中。结果表明,①糖渣中的葡萄糖、蛋白质和脂肪能够作为碳源和氮源被微生物利用,说明该处理糖渣的思路可行;②糖渣中的硅藻土在发酵过程中能够有效减小灰褐链霉菌的菌球直径,提高了产物ε-聚赖氨酸的产量,当添加糖渣质量浓度为15 g/L时,ε-聚赖氨酸质量浓度达到最高值2.46 g/L,提高幅度为59.7%;③剩余的硅藻土可作为助滤剂加快后续的板框过滤速率,能够节省新助滤剂的添加量。综上,实现了将糖渣变废为宝、降低了生产成本,具有重要的经济效益和社会效益。     

过滤介质对大豆浓缩磷脂透明度的影响

以大豆原油为原料,分别选择硅藻土、活性炭、活性白土、豆粕、珍珠岩、木质纤维素、凹凸棒土和膨润土作为过滤介质,对大豆原油过滤除杂,制备大豆浓缩磷脂,研究各种过滤介质对大豆浓缩磷脂透明度的影响,结果表明木质纤维素可以有效去除大豆原油中的杂质,制备得到的大豆浓缩磷脂透明度甚至比食品级大豆浓缩磷脂高。     

壳聚糖与硅藻土调理市政污泥

以污泥比阻为评价指标,综合考虑脱水率、泥饼含水率及过滤时间因素,研究使用壳聚糖与硅藻土对污泥单独调理的最佳条件及联合调理改善污泥脱水性能的效果,并与聚丙烯酰胺调理污泥的效果进行了对比。结果表明,先投加0.5 g/g硅藻土调理污泥,再投加5 mg/g壳聚糖以30 r/min搅拌反应150 s,污泥比阻下降了95.43%,脱水率上升至91.02%,泥饼含水率降至83.13%,过滤时间降至29.5 s。壳聚糖与硅藻土联合调理的效果明显优于壳聚糖或硅藻土单独调理的效果,且其联合调理改善污泥脱水综合性能的效果优于聚丙烯酰胺调理污泥的效果。     

WO3/g-C3N4复合催化剂的制备及其可见光 光催化性能分析

在盐酸质子化条件下,采用超声微波协助法成功制备了可见光型复合催化剂WO₃/g-C₃N₄。利用X射线多晶粉末衍射仪(XRD)、扫描电镜(SEM)、透射电镜(TEM)、紫外可见漫反射(UV-Vis)和BET比表面测试仪对样品进行了表征,并以罗丹明B(RhB)为目标降解物对其光催化性能进行研究。结果表明:复合催化剂样品是由片状的WO₃纳米片负载在g-C₃N₄表面组成的。当WO₃负载的质量分数为40%时,前驱物在500℃条件下煅烧2 h后所得样品的光催化性能明显好于同条件下制得的单一相WO₃和g-C₃N₄,在可见光(波长大于420 nm)照射下,5 h内对100 mL浓度为10^-5 mol/L罗丹明B橙溶液的降解高达98%。     

秸秆还田对土壤养分及土壤微生物数量的影响

为探明秸秆还田后土壤养分及土壤微生物数量的变化情况,通过田间试验,研究了秸秆还田对小麦-玉米轮作体系中土壤养分及土壤微生物数量的影响。结果表明：秸秆还田可以增加土壤有机质含量,提高土壤养分库容,增加土壤中细菌、真菌及放线菌数量。50%秸秆还田、100%秸秆还田、150%秸秆还田条件下,土壤有机质增幅为0.02~0.04个百分点,土壤碱解氮、有效磷、速效钾分别增加6.64~9.00、3.37~4.07、10.33~19.00 mg/kg。不同秸秆还田量增加土壤微生物丰富度,细菌、真菌、放线菌增幅分别为2.2×10⁸个/g~3.1×10⁸个/g、0.5×10⁶个/g ~3.5×10⁶个/g、1.3×10⁷个/g ~1.9×10⁷个/g。但过量秸秆还田不利于农田生产力。     

大丽轮枝菌拮抗细菌B.subtilis LZ2-70产芽孢条件优化

 为了提高大丽轮枝菌（Verticillium dahilae Kleb.）拮抗细菌枯草芽孢杆菌 Bacillus subtilis LZ2-70菌株的芽孢形成率及芽孢数量,在摇瓶发酵基础上对影响该菌芽孢形成的主要因素进行了考察。通过单因素试验确定了最佳的碳源、氮源和无机盐等,通过正交试验研究了培养基最佳浓度和组合,以及种龄、接种量、培养液初始pH和培养时间等发酵条件。摇瓶发酵生产芽孢的最佳条件为:0.5% 麦芽糖、2% 黄豆饼粉、0.05% KH₂PO₄和0.1% MnSO₄·H₂O、培养液初始pH值8.0、种龄24 h、装瓶量30 mL/ 250 mL 、接种量10%、发酵时间48 h、培养温度为30 ℃、摇床转速为200 r·min^-1。在此优化条件下,发酵液中LZ2-70菌株的芽孢数量达到6.6×10⁹ 个·mL^-1,芽孢形成率为98.94%。     

氮肥水平和种植密度对冬小麦茎秆抗倒性能的影响

以中穗型小麦品种山农15为材料,在2个氮肥水平(180 kg hm^-2和240 kg hm^-2)和2个密度(150×10⁴ hm^-2和225×10⁴ hm^-2)下,研究了抗倒性能相关的形态学特征、茎基部节间化学组分、抗倒指数（茎秆机械强度/茎秆重心高度）、木质素合成相关酶活性和籽粒产量的变化特点,以及抗倒指数与形态学和生化指标的相关性。结果表明,施氮水平和种植密度间存在显著的互作效应,当施氮水平由180 kg hm^-2增至240 kg hm^-2或种植密度由150×10⁴ hm^-2增加到225×10⁴ hm^-2时,茎秆重心高度、基部节间长度显著提高,基部节间直径、厚度、充实度、机械强度和抗倒指数显著降低,同时茎秆基部节间纤维素含量、木质素含量显著减少,含氮量显著升高,碳氮比(C/N比)以及木质素合成相关酶活性显著降低。逐步回归分析表明,氮肥水平对小麦抗倒性的影响大于种植密度。本试验条件下,氮肥水平180 kg hm^-2和种植密度为150×10⁴ hm^-2的处理穗数较低,但穗粒数和千粒重显著高于其它处理,因而籽粒产量最高。建议在降低氮肥用量至180 kg hm^-2的同时降低种植密度至150×10⁴ hm^-2,可在增强植株抗倒伏能力的同时获得高产。     

基于滤食鱼类天然产力的安康库区生态负荷量测定

为厘清汉江水体鱼类集约养殖与生态负荷量的关系,测定安康库区滤食性鱼类天然鱼产力,测算Ⅱ类水质限定条件下的安康库区生态负荷量,并与以水体磷含量为标准的计算结果比较。结果表明,设定网箱深度3 m,单位水体生态负荷量为193.44 g/m³,总产量控制为10.47×10⁴ t。库区网养单产为100 kg/m³时,网箱养殖面积控制为1.93‰,网箱生态养殖面积与单位面积产量呈反比。     

微波辅助NaOH-H2O2水解氧化法制备稻根纤维素

为了探讨农业废弃物提取纤维素的新途径,以稻根为原料,采用微波辅助Na OH-H2O2水解氧化法制备稻根纤维素,利用FT-IR、XRD、SEM等对稻根纤维素进行初步表征与分析。从而研究了微波功率、加热时间、Na OH浓度、固液比等因素对稻根纤维素提取率的影响。结果表明：在Na OH浓度6%、微波功率450 W、时间3.0 min、液料比1：25的条件下提取出粗稻根纤维;微波辅助条件下,以H2O2和12.5 g/L硅酸钠混合氧化漂白液处理粗稻根纤维素得到稻根纤维素提取率为89.3%。因此,采用微波辅助Na OH-H2O2水解氧化法制备稻根纤维素去除木质素效率高、对纤维素的结构损伤小,具有节能、高效、污染小等特点。     

Switched-Capacitor Complex Filter and Its Application

The realization of cascade connection and its application in negative-pass filtering of Switched-Capacitor Complex Filter(SCCF) are studied in this paper,in which a SC complex negative-pass filter is designed and its attenuation characteristics obtained by computer simulation are also presented.     

Digital Filtering with Zero Phase Error

Aiming at the problem of phase error caused by normal filters in signal processing , summarizes the important meaning of digital filtering with zero phase error. Puts forward RRF Filtering which is a new way to realize digital filtering with zero phase error through reversing the time serials of the signal. Another way to realize digital filtering with zero phase error is suggested through reversing the time serials of normal filter. Testifies the way to realize digital filtering with zero phase error. Points out how to design the digital filter with zero phase frequency peculiarity. Solves the problem of phase error in DSP.     

Dynamic Characteristic of Micromachined Arrayed Microphone

Several kinds of microphone developed via silicon Micro Electro Mechanical System (MEMS) processes in recent years are investigated in this paper. The analysis and research of the merits and demerits of them show that: these conventional microphones mainly function as acoustic electric converters; the filtering against noise is implemented by a special filter circuit or a digital filter. Therefore, a design method for silicon micro array filter microphone is presented, where the filtering is achieved while converting signals. The effects of damping, silicon reed number and sensor element pair on dynamic characteristic are discussed; it follows that: Increasing damping can reduce microphone's sensitivity, while increasing silicon reed number can improve the sensitivity curve, furthermore, the implementation of the filter function is simultaneous with acquiring of the noise signal.     

The Filtering Character of Hilbert-Huang Transform and Its Application

Hilbert-Huang transform(HHT) is a new two-step time-frequency analytic method to analyze the nonlinear and non-stationary signal. The key step of this method is empirical mode decomposition(EMD) method with which any complicated data set can be decompose into a finite and often small number of intrinsic mode functions(IMF). Using Hilbert transform to those IMF components can yield instantaneous frequency, the final presentation of this results is a energy frequency-time distribution, designated as the Hilbert spectrum. Examples from the numerical results of signal de-noising are given to demonstrate the power of this new method, those results can clarity the advance and efficient of this method.     

Research on Applying Mallat's Pyramid Algorithm to Process One Dimensional Signal

Discuss the problem resulting from applying Mallat 's pyramid algorithm to process one dimensional signal . A formula for constructing scaling function and wavelet function according to second sampling interval and the corresponding formula for computing continuous approximation and detail are given .     

KT系列内燃机空气粉尘滤清器及其净化效率试验计算公式的变更

KT系列内燃机空气粉尘滤清器是国家最新专利产品,是阻隔式纸制滤清器的更新换代产品,是纸制滤清器的一次革命。在恶劣的空气环境下,KT系列内燃机空气粉尘滤清器的使用效果尤其明显,也可与原纸制滤清器匹配使用。该产品在使用过程中,不需要更换滤芯,仅需添加一定量的溶液即可。针对国家标准中净化效率试验计算公式不适用的问题对该公式变更,经上海内燃机研究所测试使用,认为变更公式正确。     

Implementation of FIR Filter Using High Density Programmable Logic Device

In order to accelerate the working speed of a FIR filter, the structure-optimized FIR filter, which includes a vector-multiplication that can efficiently reduce the numbers of multiplication and addition of tradition structure, has been deduced .The vector-multiplication can be realized easily by means of the LUT in HDPLD FLEX10K. Using development software of MAX+PLUS II, both parallel and serial parameteized FIR filter have been designed.