INVESTIGATION ON THE DITERMINATION OF METAL IRON IN SLAG CONTAINING VANADIUM TITANIUM ( IODIN-ALCOHOL FOR SEPARATION EDTA FOR DITERMINATION)

Great accuracy can be obtained when metal iron is determined with bromine for dissolution K2Cr2O7 for titration. Unfortunately, harmful substances such as Br2, CH3OH, HgCl2, K2Cr2O7 etc. must be used when this method. But these harmful substances can be avoided when I2-C2H5OH is used for dissolution and EDTA for titration as discussed in this paper. As this method is simple with good reapetability, it is suitable for the diterminat ion of metal iron slag containing V.Ti, in slag containing high Ti, and in common slags.     

INVESTIGATION ON THE DITERMINATION OF LOW-VALENCE TITANIUM(II,III) IN SLAG CONTAINING A HIGH TITANIUM CONTENT

In this article a method is investigated for the determination of low-valence titanium in slag containing a high titanium content. The residue is dissolved using H2SO4-HF-H3PO4 after tMFe, Fe2O3 and the part of FeO are separated from sample with FeCl3-HCl, and NH4 Fe(SO4)2 is added to oxidate low titanium. Then the standard solution of K2Cr2O7 is used to tit-rat Fe2+ in sample solution. The method possesed with a advantage of simple rapid and good repeatability so that it can be used in the roution determination.     

PHASE ANALYSLS OF LOW-VALENCE TITANIUM IN SLAG CONTAINING HIGH TITANIUM

Hcl is used to remove MF4, Fe2O3 and part of FeO. The residue is dissolved by H2SO4-HF-H3PO4. Then, NH4Fe(SO4)2 is added to oxidate low-valence titanium and the standard solution of K2Cr2O7 is used to titrate Fe2+. The amount of total iron minus the amount of iron which has been removed, so that the amount of residue Fe2+ can be adjusted. This method has many advantages such as simplicity, rapidity repeatability.     

DETERMINATION OF METALLIC IRON IN HIGH TITANIUM SLAG BY HEADSPACE GAS CHROMATNGRALHY

The following details are discussed in the present paper, after high titanium slag and H3PO4 is put in the closed system,the .reaction takes place under controlled temperature conditions, and the gas produced is collected. The two phases of gas liquid attain kinetic equilibrium, ihe gas above the liquid is used to make GC analysis with the aid of chromatographic column of 5A molecular sieve, TCD and N2 30ml/min. Satisfactory quantitative results can be achieved with simple instruments and uncomplicated operation technique.     

中国粮食仓储行业淘汰甲基溴行动

为切实履行我国政府对国际社会<关于消耗臭氧层物质的蒙特利尔议定书>的<哥本哈根修正案>所作出的承诺,中国粮食仓储行业在保障我国粮食安全储备的前提下,在"淘汰甲基溴,保护臭氧层"方面采取了一系列行动(包括调研、确定替代技术、培训、制定规程、建设示范库、研究替代技术等),以达到替代甲基溴的目的.淘汰甲基溴的实际行动,研究新的淘汰甲基溴替代技术,对增强人们保护臭氧层的意识,推广和应用替代技术和确保人类共同家园的可持续发展都具有重要的意义.     

氮素营养与甘蓝型油菜角果的发育

本研究运用田间和盆钵试验,观察了甘蓝型油菜(B.napus)角果生长的基本特点,探讨了不同氮水平与角果发育的关系。结果表明,角果生长发育进程呈“S”型曲线,即含明显的生长缓慢期、生长优势期、物质积累优势期和衰老期;氮水平间角果面积增长速率的差异达极显著的正相关(r=0.9091~(**)),单株角果面积与籽粒产量亦呈极显著的正相     

玉米C型胞质雄性不育系花粉败育的细胞学研究

利用光学和电子显微镜对玉米C型胞质雄性不育系和保持系的花药与小孢子发育过程进行对比观察.结果表明,不育系小孢子初始败育发生在幼龄小孢子时期,单核中期基本上完全败育,绒毡层到开花前崩溃.在小孢子初始发育时期,不育系绒毡层细胞的质体呈“杯状”变态.导致雄性不育主要的细胞学原因是绒毡层细胞结构、功能的失常.     

ICP-MS测定小麦中的铅、镉、汞、砷

重金属污染及其测量方法一直以来都是粮食检测部门关注的重点.本文探索采用微波消解结合ICP-MS的方法同时测定小麦中铅、镉、砷、汞含量,并根据此法测量结果评价了江苏小麦重金属污染情况.结果表明,该方法测试铅、镉、砷、汞含量的相关系数(r2,)分别为0.9991、0.9999、0.9999、0.9997;检测限分别为0.05μg/kg、0.01 μg/kg、0.02μg/kg、0.06 μg/kg;精密度分别为3.7％士2.8％、3.8％士2.8％、2.8％士1.9％、3.7％士3.5％;加标回收率分别为99.5％±4.4％、98.2％±4.6％、100.6％±7.1％、97.9％±10.8％;2014年江苏小麦铅、镉、砷、汞含量未见超标.结果认为,微波消解结合ICP-MS是一种高效、准确的小麦铅、镉、汞、砷含量测定方法.     

[云南狗尾草×谷子(四倍体)]F_1组织培养中的植株再生

为了谷子三系选育研究的需要,我们进行了〔Setaria yunnanensis×S.italica(4n)〕F_1(不育材料)的幼穗培养研究。在 N_6+2,4-D 0.5～2.0毫克/升+KT 2.0毫克/升的培养基上由小穗轴切口处诱导出淡黄色质地紧密的愈伤组织,此愈伤组织在 N_6+2,4-D 1.0+KT 1.0的培养基上长大,并在表面产生了一些颗粒状结构,后者在转移到 N_6+KT 1.     

玉米优良自交系埃1278C、埃1278C—2与海7—1的选育及其抗病性鉴定

本研究自1969年开始,应用一环系和二环系选育方法选育玉米自交系.到1973年先后育成了两个白粒马齿型和一个黄色硬粒型优良自交系.这三个自交系产量高,配合力好,综合性状优良.根据在室内和田间抗病性鉴定的结果,它们的抗大小斑病性类似或优于抗病系330,525,C103,MO17;埃1278C—2的抗小斑病性表现尤为突出.本文还就选育抗病系的方法和早代测定配合力的效果进行了讨论.     

棉花根系的生长特性及其与栽培措施和产量关系的研究 Ⅱ栽培措施对棉花根系生长的影响及其与地上部和产量的关系

本文研究了灌溉、施肥量与播种期对露地棉与地膜棉根系的生长特性及其与地上部的相互作用和产量形成的影响。结果表明,生长期灌水处理棉株根系入土浅,总长度减少,未灌水处理根量在深土层明显增加;重肥处理根系入土深,深土层根量增加。灌水及重肥处理根系新根量均增加,根系伤流量增大,生理活力增强。早播棉株主根深度增加,根重增大,尤在生育前期增长明显,同时.根系建成提前,根系分布范围广。灌水、重肥与早播处理棉株根重、地上部重及籽棉产量等均增加。棉株根量与产量间存在显著相关关系,蕾期根量对产量的效应最大。