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棉酚快速测定适宜条件的筛选
引用本文:敖维平,曲明悦.棉酚快速测定适宜条件的筛选[J].畜牧兽医杂志,2007,26(6):23-25.
作者姓名:敖维平  曲明悦
作者单位:1. 兵团塔里木畜牧科技重点实验室,新疆,阿拉尔,843300
2. 塔里木大学动物科技学院
基金项目:新疆建设兵团塔里木畜牧科技重点实验室基金
摘    要:采用间苯三酚法和高效液相色谱法测定棉籽粕中游离棉酚含量,通过对提取方法和样品称量等测定条件筛选,并分析比较测定结果及回收率。结果表明:采用超声波滤取,间苯三酚法测定游离棉酚,具有操作简便、条件要求低、回收率高等优点,可作为企业内控质量检测推广应用方法。

关 键 词:间苯三酚  高效液相色谱  棉酚  方法
文章编号:1004-6704(2007)06-0023-03
修稿时间:2007-05-14

Election Appropriate Conditions of Rapid Measurement for Free Gossypol
AO Wei-ping,QU Ming-yue.Election Appropriate Conditions of Rapid Measurement for Free Gossypol[J].Journal of Animal Science and Veterinary Medicine,2007,26(6):23-25.
Authors:AO Wei-ping  QU Ming-yue
Abstract:Free gossypol content is mensurated in cottonseed meal by phloroglucinol dihydrate and high performance liquid chromatography.Then,filtrating sample extraction methods and the weighing of conditions is to analyze the results and rates of reclamation.The results show that the method by Ultrasonic Filtering in phloroglucinol dihydrate is easy to fulfill and gains higher rates of reclamation,which can be widely used in internal enterprises mensurating content of gossypol of cottonseed meal.
Keywords:phloroglucinol dihydrate  high performance liquid chromatography(HPLC)  free gossypol  method
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