| 调环酸钙5%泡腾片剂高效液相色谱分析 |
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| 引用本文： | 李岩,王胜翔,史娜,郑杨.调环酸钙5%泡腾片剂高效液相色谱分析[J].农药科学与管理,2012,33(9):40-42. |
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| 作者姓名： | 李岩 王胜翔 史娜 郑杨 |
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| 作者单位： | 1. 黑龙江省农药管理检定站,哈尔滨,150090
2. 农业部农药检定所,北京,100125 |
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| 摘 要： | 本文采用高效液相色谱法,以乙腈＋0.1%磷酸水溶液为流动相,使用ZORBAX SB-C18不锈钢柱和二极管阵列检测器,在275nm波长下对试样中的调环酸钙进行分离和定量分析。结果表明,该方法测得调环酸钙的线性相关系数为0.999 9;标准偏差为0.07;变异系数为1.40%;平均回收率为100.0%。
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| 关 键 词： | 调环酸钙 高效液相色谱 |
Analytical Method of Prohexadione Calcium 5 % Effervescent Tablet by HPLC |
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| Li Yan,Shi Na,Zheng Yang.Analytical Method of Prohexadione Calcium 5 % Effervescent Tablet by HPLC[J].Pesticide Science and Administration,2012,33(9):40-42. |
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| Authors: | Li Yan Shi Na Zheng Yang |
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| Institution: | (Pesticide Management and Test Station of Heilongjiang Province,Harbin 150090,China) Wang Shengxiang(Institute for the Control of Agrochemicals,Ministry of Agriculture,Beijing 100125,China) |
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| Abstract: | A method for the separation and the quantitative analysis of Prohexadione calcium by HPLC with acetonitrile and 0.1% aqueous phosphoric as mobile phase,using ZORBAX SB-C18 column and DAD at 275nm wavelength was described.The result showed that the linear relative coefficient was 0.999 9,the standard deviation was 0.07,the variation coefficient was 1.40%,the average recovery was 100.0%. |
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| Keywords: | prohexadione calcium HPLC |
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