| HPLC测定调经祛斑片中芍药苷的含量 |
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| 引用本文： | 马春娟,孙怀娟.HPLC测定调经祛斑片中芍药苷的含量[J].人参研究,2009,21(4):26-27. |
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| 作者姓名： | 马春娟 孙怀娟 |
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| 作者单位： | 通化师范学院制药与食品科学系,吉林通化,134002 |
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| 摘 要： | 目的：建立调经祛斑片中芍药苷的HPLC测定方法。方法：色谱柱：Shim-pack柱;流动相：乙腈-0.1%磷酸溶液（14∶86）;梯度洗脱;流速1.0mL·min^-1;检测波长：230nm。结果：芍药苷线性范围为0.1～2.0μg,r=0.9999;平均回收率为99.12%,RSD=0.63%。结论：该方法准确,简便,易行,重复性好,可用于该制剂的质量控制。
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| 关 键 词： | 调经祛斑片 芍药苷 高效液相色谱法 |
The Method of Determining paeoniflor in in Tiaojing Quban tabletsby HPLC |
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| Authors: | Ma Chun juan Sun Huai juan |
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| Institution: | (Thonghua Teachers CollegeJilin Province , Tonghua134002 ) |
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| Abstract: | Objective：To develop an HPLC method for determination of paeoniflorin in Tiaojing Quban tablets.Methods：ODS-C18 column was adopted;The mobile phasa consisted of Acetonitrile-0.1% phosphoric acid（14：86） acid solution with gradieal elution at a flow rate of 1.0mL·min^-1;The detection wavelength was 230nm.Results：A good linear was obtained in the range of 0.1-2.0ug,r=0.9999;The average recovery was 99.12﹪（RSD=0.63﹪）.Conclusions：The results show that the method is accurate,reproducible,simple,and can be used for the quality control of Tiaojing Quban tablets. |
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| Keywords: | Tiaojing Quban tablets paeoniflorin HPLC |
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