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Titanium dioxide nanofibers prepared by using electrospinning method
Authors:Bin?Ding  Chul?Ki?Kim  Email author" target="_blank">Hak?Yong?KimEmail author  Min?Kang?Seo  Soo?Jin?Park
Institution:(1) Department of Textile Engineering, Chonbuk National University, 561-756 Jeonju, Korea;(2) Department of Advanced Organic Materials Engineering, Chonbuk National University, 561-756 Jeonju, Korea;(3) Advanced Materials Division, Korea Research Institute of Chemical Technology, 305-600 Uysong, Daejeon, Korea
Abstract:The synthesis of titanium dioxide nanofibers with 200–300 nm diameter was presented. The new inorganic-organic hybrid nanofibers were prepared by sol-gel processing and electrospinning technique using a viscous solution of titanium isopropoxide (TiP)/poly(vinyl acetate) (PVAc). Pure titanium dioxide nanofibers were obtained by high temperature calcination of the inorganic-organic composite fibers. SEM, FT-IR, and WAXD techniques were employed to characterize these nanofibers. The titanium dioxide nanostructured fibers have rougher surface and smaller diameter compare with PVAc/TiP composite nanofibers. The anatase to rutile phase transformation occurred when the calcination temperature was increased from 600 °C to 1000 °C.
Keywords:Hybrid nanofibers  Titanium isopropoxide/Poly(vinyl acetate)  Titanium dioxide  Calcination
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