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白兰叶挥发油提取方法及工艺条件研究
引用本文:张霞,刘敦菊,徐立,眭顺照,李名扬.白兰叶挥发油提取方法及工艺条件研究[J].安徽农学通报,2011,17(3):41-43,76.
作者姓名:张霞  刘敦菊  徐立  眭顺照  李名扬
作者单位:西南大学园艺园林学院,重庆,400715;西南大学花卉研究所,重庆,400716
摘    要:采用2种不同方法,即超声辅助提取法、微波辅助一水蒸气蒸馏法,对白兰叶的挥发油进行了提取。以白兰叶挥发油提取量为指标,通过正交实验设计优选提取工艺。研究表明,白兰叶挥发油的最佳提取工艺为微波辅助一水蒸气蒸馏法,其提取工艺条件为:微波功率480W、微波时间7min、提取时间5h、料液比1:10(g/mL),此条件下挥发油提取率可达到0.81%。

关 键 词:白兰  挥发油  超声助提  微波辅助-水蒸气蒸馏法  正交实验设计

Study on the Extraction Methods and Technological Conditions for Volatile Oil in the Leaves of Michelia alba DC.
Institution:Zhang Xia et al. ( College of Horticulture and Landscape, Southwest University, Chongqing 400715, China ; Institute of Ornamental Research, Southwest University, Chongqing 400716, China)
Abstract:The volatile oil in the leaves of Michelia alba DC. was extracted by two different methods, including ultrasonically assisted extraction and microwave - assisted hydrodistillatin. With the yield rate of volatile oil as the index, the optimum ex- tracting technology and the optimum conditions of extraction for volatile oil from the leaves of Michelia alba DC. were deter- mined by orthogonal experimental design. The results suggested that the optimum extracting technology was microwave -as- sisted hydrodistillatin and the optimum conditions for extracting were the microwave power of 480W, microwave time of 7rain, extraction time of 5h and the ratio of feed and liqiud of 1/10(g/mL) . Under such conditions,the yield of volatile oil was 0. 81%.
Keywords:Michelia alba DC    Volatile oil  Ultrasonically assisted extraction  Microwave - assisted hydrodiotillation  Orthogonal experimental design
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