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2,5-二苯乙炔噻吩β-环糊精微胶囊的研制与性能研究
引用本文:吴仁海,王恒亮,张永超,孙建伟,杨东亚.2,5-二苯乙炔噻吩β-环糊精微胶囊的研制与性能研究[J].河南农业科学,2011,40(1):90-93.
作者姓名:吴仁海  王恒亮  张永超  孙建伟  杨东亚
作者单位:河南省农业科学院,植物保护研究所,河南省农作物病虫害防治重点实验室,河南,郑州,450002
基金项目:郑州市金水区技术研究与开发经费支持项目,河南省农科院植保所青年基金项目
摘    要:以分子包埋法制备2,5-二苯乙炔噻吩(DPET)β-环糊精微胶囊剂,通过正交试验考察囊芯与囊壁比例、反应温度、反应时间等参数对微胶囊包埋率的影响,结果表明,囊芯与囊壁比例为1:40、反应温度40~60℃、反应时间0.5~2h时,包埋率在60%以上.在紫外光照射下,DPET β-环糊精微胶囊剂半衰期为4.63h,而未包埋...

关 键 词:2  5-二苯乙炔噻吩  β-环糊精  微胶囊  光活化农药

Preparation and Properties of the Inclusion Compound of 2,5-Diphenylethynylthiophene with β-Cyclodextrin
WU Ren-hai,WANG Heng-liang,ZHANG Yong-chao,SUN Jian-wei,YANG Dong-ya.Preparation and Properties of the Inclusion Compound of 2,5-Diphenylethynylthiophene with β-Cyclodextrin[J].Journal of Henan Agricultural Sciences,2011,40(1):90-93.
Authors:WU Ren-hai  WANG Heng-liang  ZHANG Yong-chao  SUN Jian-wei  YANG Dong-ya
Institution:(Institute of Plant Protection,Henan Academy of Agricultural Sciences,Henan Key Laboratory of Crop Pest Control,Zhengzhou 450002,China)
Abstract:The 2,5-diphenylethynylthiophene(DPET) with β-cyclodextrin was prepared in inclusion compound.The ratio of DPET to cyclodetrin,the temperature and the time of reaction as the dominating factors were optimized by orthogonal experiment.The results showed that the yield of DPET inclusion compound with β-cyclodextrin was more than 60% when the mass ratio of DPET to cyclodextirn was 1∶40 and the reaction was under 40-60℃ for 0.5-2 hours.The half life of DPET was 11.08 min under ultraviolet while it extended to 4.63h for DPET β-cyclodextrin inclusion compound.The bioactivity of the compound was evaluated with the third-instar larvae of Plutella xylostella L.Pretreated with ultraviolet,DPET β-cyclodextrin inclusion compound showed higher activity than DPET,which indicated that the inclusion compound with β-cyclodextrin could retard the DPET's decompositon under light.
Keywords:2  5-Diphenylethynylthiophene  β-cyclodextrin  Inclusion compound  Light-activated insecticide
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