| 饮用纯净水中14种卤代烃的顶空气相色谱分析 |
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| 引用本文： | 陈艳彬,周围.饮用纯净水中14种卤代烃的顶空气相色谱分析[J].甘肃农业大学学报,2010,45(1). |
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| 作者姓名： | 陈艳彬 周围 |
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| 作者单位： | 1. 甘肃农业大学食品科学与工程学院,甘肃,兰州,730070
2. 甘肃出入境检验检疫局中心实验室,甘肃,兰州,730020 |
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| 摘 要： | 基于顶空气相色谱分析,采用ECD检测器测定,建立了饮用纯净水中14种卤代烃的检测方法,并对色谱柱、色谱检测器、平衡温度、平衡时间及样品基体进行了研究和条件优化.结果表明:在所建立的最佳实验条件下14种卤代烃的回收率在88.2%～99.6%之间,相对标准偏差为1.68%～6.29%,检测限为0.1～120μg.L-1;所建立的分析方法快速、简便,适合饮用纯净水中多种卤代烃的检测分析.
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| 关 键 词： | 饮用纯净水 顶空气相色谱 卤代烃 |
Determination of 14 kinds of halohydrocarbons in purified drink water by head space and gas chromatography |
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| CHEN Yan-bin,ZHOU Wei.Determination of 14 kinds of halohydrocarbons in purified drink water by head space and gas chromatography[J].Journal of Gansu Agricultural University,2010,45(1). |
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| Authors: | CHEN Yan-bin ZHOU Wei |
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| Institution: | 1.College of Food Science and Engineering;Gansu Agricultural University;Lanzhou 730070;China;2.Central Laboratory;Entry and Exit Inspection and Quarantine Bureau of Gansu;Lanzhou 730020;China |
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| Abstract: | A method was developed for quick-determination of 14 kinds of halohydrocarbons in purified drink water by head space and gas chromatography with electron capture detector (HS-GC-ECD). Some conditions and parameters were optimized as column, detector, equilibrium time and temperature, and sample matrix. Under the optimal conditions, the recoveries of the fourteen halohydrocarbons were in the range of 88.2 % ～99.6 %. The relative standard deviations were from 1.68 % to 6.29 %. The determination limit was between 0.1～120 μg·L~(-1). It is suggested that this method is rapid, simple and suitable for determination of halohydrocarbons in purified drink water. |
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| Keywords: | purified drink water head space gas chromatography halohydrocarbon |
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