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“土法”提取杉木屑精油化学成份GC/MS分析及探讨
引用本文:李军集,何春茂,梁忠云,周丽珠,谷瑶.“土法”提取杉木屑精油化学成份GC/MS分析及探讨[J].热带农业科学,2013(11):70-74.
作者姓名:李军集  何春茂  梁忠云  周丽珠  谷瑶
作者单位:[1]广西林业科学研究院广西南宁530002 [2]国家林业局中南速生材繁育实验室广西南宁530002
摘    要:“土法”提取精油因其设备简单、拆装方便、容易运输、易操作、成本低等特点,在偏远农村广泛使用,本试验对“土法”水蒸汽蒸馏方法提取精油进行化学成份的GC/MS分析.共分出71个色谱峰.采用GC峰面积归一化法进行定量,其中鉴定出47个化合物,占该精油总量的91.8%。其主要成分为α-柏木烯(22.4%)、柏木醇(20.07%)、α-松油醇(4.29%)、α-蒎烯(2.26%)等.本试验为更好的利用“土法”提取杉木屑精油提供参考,为改进“土法”提取设备提供可靠依据。

关 键 词:气质联用  精油  杉木  柏木醇  α-柏木烯

GC/MS Analysis of the Chemical Composition of the Essential Oil Extracted by Indigenous Extraction Method from the Powder of Cunninghamia lanceolata
LI Junji,HE Chunmao,LIANG Zhongyun,ZHOU Lizhu,GU Yao.GC/MS Analysis of the Chemical Composition of the Essential Oil Extracted by Indigenous Extraction Method from the Powder of Cunninghamia lanceolata[J].Chinese Journal of Tropical Agriculture,2013(11):70-74.
Authors:LI Junji  HE Chunmao  LIANG Zhongyun  ZHOU Lizhu  GU Yao
Institution:1 Guangxi Academy of Forestry, Nanning, Guangxi 530002; 2 Key Laboratory of Central South Fast-growing Timber Cultivation of Forestry Ministry of China, Nanning, Guangxi 530002, China)
Abstract:The indigenous extraction method of essential oil was widely used in the remote countryside due to its superiority such as simple devices, convenient to disassemble, transport and manipulate. The chemical compositions of the essential oil extracted by the indigenous method was analyzed by GC/MS,47 constituents were identified from 71 chromatographic peaks, and the relative content up to 91.8%. The major constituents were α-cedrene(22.4%), cedrol(20.07%), α-terpineol(4.29%)and α-pinene(2.26%). This result provided reference for the further usage of the Cunninghamia lanceolata essential oil and improving the extraction equipment.
Keywords:GC-MS  Essential oil  Cunninghamia lanceolata  cedrol  α-cedrene
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