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芦笋老茎中多糖提取工艺的优化
引用本文:郑学芳,黄云祥,廉琪,宋士涛,张建平,彭友舜.芦笋老茎中多糖提取工艺的优化[J].安徽农业科学,2011,39(4):2089-2090.
作者姓名:郑学芳  黄云祥  廉琪  宋士涛  张建平  彭友舜
作者单位:郑学芳,廉琪,宋士涛,张建平,彭友舜(河北科技师范学院理化学院,河北秦皇岛,066600);黄云祥(河北秦皇岛长胜农业科技发展有限公司,河北秦皇岛,066600)
摘    要:目的]优化微波直提法和微波-索氏提取法提取芦笋老茎中多糖的工艺。方法]以多糖提取率为考察指标,通过正交试验优化2种提取方法的提取工艺。结果]微波直提法的最佳工艺条件为:料液比为1∶30,提取时间为20 min,提取温度为60℃,微波功率为600 W,在此条件下多糖的提取率为4.35%;微波-索氏提取法的最佳工艺条件为:料液比为1∶33,微波时间为10 min,微波功率为600W,提取温度为70℃,在此条件下多糖的提取率为2.29%。结论]微波直提法具有提取效率高,提取温度低,能量消耗小等特点,可用于实际生产中。

关 键 词:芦笋  多糖  微波直提法  微波-索氏提取法  正交试验

Optimization of Extraction Process for Polysaccharide from Old Stem of Asparagus
ZHENG Xue-fang et al.Optimization of Extraction Process for Polysaccharide from Old Stem of Asparagus[J].Journal of Anhui Agricultural Sciences,2011,39(4):2089-2090.
Authors:ZHENG Xue-fang
Institution:ZHENG Xue-fang et al(School of Physics and Chemistry,Hebei Normal University of Science and Technology,Qinghuangdao,Hebei 066600)
Abstract:Objective] To optimize the extraction conditions of microwave extraction and microwave-soxhlet extraction for polysaccharide from old stems of Asparagus.Method] By employing yield of polysaccharide as investigation index,the extraction processes of the two methods were optimized by orthogonal test.Result] The optimal extraction conditions of microwave extraction were determined to be solid to liquid ratio of 1∶ 30,extraction duration of 20 min,extraction temperature of 60 ℃ and extraction power of 600 W,under which,the yield of polysaccharide reached as high as 4.35%.The optimum extraction process of microwave-soxhlet extraction were as follows:solid to liquid ratio of 1∶ 30,extraction duration of 10 min,extraction power of 600 W and extraction temperature of 70℃,and the yield of polysaccharide reached 2.29% under the optimal extraction conditions.Conclusion] High in extraction efficiency,low in extraction temperature and save in consumption,the microwave extraction is favorable for the extraction of polysaccharide from old stem of Asparagus in practical production.
Keywords:Asparagus  Polysaccharide  Microwave extraction  Microwave-soxhlet extraction  Orthogonal test  
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