| 微波灰化-原子荧光光谱法测定卷烟纸中As含量 |
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| 引用本文： | 贺兵,王璐,苏钟璧,金永灿,张群芳,杨光宇.微波灰化-原子荧光光谱法测定卷烟纸中As含量[J].安徽农业科学,2011(11):6507-6508. |
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| 作者姓名： | 贺兵 王璐 苏钟璧 金永灿 张群芳 杨光宇 |
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| 作者单位： | 云南烟草科学研究院云南省烟草化学重点实验室;云南民族大学化学与生物技术学院; |
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| 基金项目： | 云南省自然科学基金(2009YC022)资助项目 |
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| 摘 要： | 目的]建立一种用于测定卷烟纸中砷含量的微波灰化-原子荧光方法。方法]采用微波灰化法处理卷烟纸样品,然后用原子荧光光谱法测定卷烟纸中砷含量。结果]砷在0.2～20μg/L范围内和荧光强度有良好的线性关系,其回归方程为If=286 C（μg/L）＋2.68（r=0.999 5）。该方法的回收率为95.4%～97.0%,检出限为0.04μg/L。结论]采用原子荧光光谱法测定卷烟纸中的砷含量,灵敏度高,检出限低,精密度好,回收率高,可满足卷烟纸中痕量砷测定的要求。
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| 关 键 词： | 微波灰化 卷烟纸 砷 原子荧光光谱法 |
Determination of Arsenic Content in Cigarette Paper by Atomic Fluorescence Spectrometry with Microwave Ashing |
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| HE Bing et al.Determination of Arsenic Content in Cigarette Paper by Atomic Fluorescence Spectrometry with Microwave Ashing[J].Journal of Anhui Agricultural Sciences,2011(11):6507-6508. |
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| Authors: | HE Bing |
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| Institution: | HE Bing et al(Key Laboratory of Tobacco Chemistry of Yunnan Province,Yunnan Academy of Tobacco Science,Kunming,Yunnan 650106) |
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| Abstract: | Objective] The research' aimed to establish a new method for the determination of arsenic content in cigarette paper by atomic fluorescence spectrometry with microwave ashing.Method] The samples of cigarette paper were treated by microwave ashing.And then arsenic content was determined by using atomic fluorescence spectrometry.Result] Arsenic in the range of 0.2-20 μg/L had a good linear relationship with the fluorescence intensity.Its regression equation was If=286 C(μg/L)+ 2.68(r=0.999 5).The recovery rate of this method was 95.4%-97.0% and the detection limit was 0.04 μg/L.Conclusion] The determination of arsenic content in cigarette paper by atomic fluorescence spectrometry with microwave ashing had high sensitivity,low detection limit,good precision and high recovery rate and the method can meet the determination demands of trace arsenic in cigarette paper. |
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| Keywords: | Microwave ashing Cigarette paper Arsenic Atomice fluorescence spectrometry |
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