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| 微波消解-原子荧光法测定城市污水中的砷 | |
| 引用本文： | 龙庆华,姚珍,邓海燕,胡伟.微波消解-原子荧光法测定城市污水中的砷[J].安徽农业科学,2010,38(8):4226-4227. |
| 作者姓名： | 龙庆华 姚珍 邓海燕 胡伟 |
| 作者单位： | 1. 北京经济技术开发区环境保护监测站,北京,100176 2. 南昌工程学院,江西南昌,330099 3. 北京开拓热力中心,北京,100176 4. 南京理工大学化工学院,江苏南京,210094 |
| 摘 要： | 目的]测定城市污水中的总砷。方法]应用微波消解进行前处理,再采用氢化物发生原子荧光光谱法测定城市污水中的砷。结果]在最佳试验条件下,砷的检出限为0.049μg/L,相关系数r〉0.999,加标回收率为96.9%～105.4%,相对标准偏差为2.67%～5.14%。结论]微波消解-氢化物发生原子荧光光谱法测定城市污水中的砷简便、快速、高效、安全,灵敏度高,精确度好,检出限低。 |
| 关 键 词： | 微波消解 原子荧光法 城市污水 砷 |
Test of the Arsenic in Municipal Sewage with the Method of Microwave Digestion-atomic Fluorescence Spectrometry |
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| LONG Qing-hua et al.Test of the Arsenic in Municipal Sewage with the Method of Microwave Digestion-atomic Fluorescence Spectrometry[J].Journal of Anhui Agricultural Sciences,2010,38(8):4226-4227. | |
| Authors: | LONG Qing-hua |
| Institution: | Station of Environmental Protection Monitoring;Beijing Economic and Technological Development Zone;Beijing 100176 |
| Abstract: | Objective]The content of total arsenic in urban sewage was determined.Method]The municipal sewage was firstly treated with the method of microwave digestion and then the content of total arsenic was determined with the hydride generation atomic fluorescence spectrometry.Results]In the best experimental condition,the detection limitation of arsenic was 0.049 μg/L;the correlation coefficient r was > 0.999,the recovery was 96.9%-105.4% and the relative standard deviation was 2.67%-5.14%.Conclusion]The method of microwave digestion-hydride generation atomic fluorescence spectrometry in the determination of arsenic in municipal sewage was simple,fast,efficient,safe,high sensitivity,good accuracy and low detection limitation. |
| Keywords: | Microwave digestion Tomic fluorescence spectrometry Urban sewage Arsenic |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |