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盐穗木总生物碱不同提取方法的比较
引用本文:贾琦珍,詹艳,陶大勇.盐穗木总生物碱不同提取方法的比较[J].塔里木农垦大学学报,2010,22(1):33-36.
作者姓名:贾琦珍  詹艳  陶大勇
作者单位:1. 塔里木畜牧科技兵团重点实验室,新疆,阿拉尔,843300;塔里木大学动物科学学院,新疆,阿拉尔,843300
2. 塔里木大学动物科学学院,新疆,阿拉尔,843300
基金项目:塔里木盆地生物资源保护利用兵团重点实验室开放课题 
摘    要:为确定盐穗木总生物碱最佳提取工艺,采用超声波提取法、索氏提取法、乙醇加热提取法、酸水提取法四种方法提取盐穗木总碱,考察粗提物的提取率,确定最佳的提取方法。结果显示:超声波提取法提取率最高,总碱含量为0.993mg/100mg,总碱质量百分数为0.23%;酸水提取法提取率其次,总碱含量为0.520mg/100mg,总碱质量百分数为0.22%;索氏提取法,总碱含量为0.477mg/100mg,总碱质量百分数为0.04%;乙醇加热提取法,总碱含量为0.404mg/100mg,总碱质量百分数为0.04%。研究表明:以氯仿为溶剂,用超声波提取法提取盐穗木总碱,提取率最高。

关 键 词:盐穗木  总生物碱  提取方法

Comparision of the Different Extract Methods of Tota Alkaloids from Halostachyscaspica
Jia Qizhen,Zhan Yan,Tao Dayong.Comparision of the Different Extract Methods of Tota Alkaloids from Halostachyscaspica[J].Journal of Tarim University of Agricultural Reclamation,2010,22(1):33-36.
Authors:Jia Qizhen  Zhan Yan  Tao Dayong
Institution:Jia Qizhen1,2 Zhan Yan2 Tao Dayong1,2(1 Key Laboratory of Tarim Animal Husb,ry Science , Technology,XinJiang Production & Construction Group,Alar,Xinjiang 843300)(2 College of Animal Science,Tarim University,Xinjiang 843300)
Abstract:In order to determine the extraction percentage of total alkaloids from Halostachyscaspica,the methods of total alkaloids'extraction were used ultrasonic extraction,Soxhlet extraction,ethanol heated backstreaming extraction and acid extraction respectively to determine the optimal extraction method with extraction rate of total alkaloids.The results showed: the best method was ultrasonic extraction by which the content of total alkaloids was 0.993 mg/100mg and the qualitative percentage of content in total ...
Keywords:Halostachyscaspica  total alkaloids  extracted methods  
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