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| 虫酰肼和呋喃虫酰肼在土壤中的检测方法及残留动态 | |
| 引用本文： | 周航,王京文,汪万山,杨文叶,钱鸣蓉.虫酰肼和呋喃虫酰肼在土壤中的检测方法及残留动态[J].浙江农业学报,2011,23(6). |
| 作者姓名： | 周航 王京文 汪万山 杨文叶 钱鸣蓉 |
| 作者单位： | 1. 杭州市植保土肥总站,浙江杭州,310020 2. 浙江省建德市洋溪街道办事处,浙江建德,311607 3. 浙江省农业科学院农产品质量标准研究所,浙江杭州,310021 |
| 基金项目： | 杭州市科技发展计划(20080632B08) |
| 摘 要： | 本研究运用液相色谱法分析,采用乙腈匀浆提取,氨基柱净化,经有机膜过滤进样检测,虫酰肼和呋喃虫酰肼回收率分别为83.0％～100.5％和87.0％～ 109.5％.相对标准偏差(RSD)在1.9％ ～ 10.2％,均符合农药检测要求.试验表明:虫酰肼和呋喃虫酰肼施药后1h土壤中的残留量最大,随着间隔时间延长残留量逐渐减少；砂质壤土中农药降解速度明显快于砂土.砂质壤土中农药残留消解方程:虫酰肼Ct=0.847e-0.1848t,T1/2=3.75 d,R2=0.9554；呋喃虫酰肼Ct=0.875e-o2895t,T1/2=2.39 d,R2 =0.929;在砂土中降解方程:虫酰肼Ct=0.816e-0.1241t,T/2 =5.53 d,R2 =0.9418;呋喃虫酰肼Ct=0.8657e-1462t,T/2=4.74 d,R2=0.9399. |
| 关 键 词： | 砂质壤土 砂土 虫酰肼 呋喃虫酰肼 液相色谱法 残留动态 |
Detection method and residue dynamic of tebufenozide and furan tebufenozide in soil |
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| ZHOU Hang , WANG Jing-wen , WANG Wan-shan , YANG Wen-ye , QIAN Ming-rong.Detection method and residue dynamic of tebufenozide and furan tebufenozide in soil[J].Acta Agriculturae Zhejiangensis,2011,23(6). | |
| Authors: | ZHOU Hang WANG Jing-wen WANG Wan-shan YANG Wen-ye QIAN Ming-rong |
| Institution: | ZHOU Hang1,WANG Jing-wen1,*,WANG Wan-shan2,YANG Wen-ye1,QIAN Ming-rong3(1Hangzhou General Station of Plant Protection & Soil and Fertilizer in Zhejiang Province,Hangzhou 310020,China,2Yangxi Sub-district Office of Jiande,Jiande 311607,3Institute of Quality and Standard for Agro-products,Zhejiang Academy of Agricultural Sciences,Hangzhou 310021,China) |
| Abstract: | A method for determining residue of tebufenozide and furan tebufenozide pesticides in soil by means of liquid chromatograph was developed.The samples were extracted by acetomintrile,purified using amino column and filtered by the organic membrane.The results showed that the recoveries were in the range of 83% and 100.5%,and furan tebufenozide were 87% to 109.5%,with RSD less than 10.2%,which indicated that the method could meet the requires for the analysis of the pesticide residue in soil.Comparing the deg... |
| Keywords: | sandy loam sand tebufenozide furan tebufenozide liquid chromatography analysis dynamic of residue |
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