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离子液体微波辅助萃取金银花中绿原酸的研究
引用本文:李庆龙,曲有乐,欧阳小琨.离子液体微波辅助萃取金银花中绿原酸的研究[J].浙江水产学院学报,2010(1):30-33,43.
作者姓名:李庆龙  曲有乐  欧阳小琨
作者单位:[1]浙江海洋学院食品与药学学院、医学院,浙江舟山316004 [2]佳木斯大学药学院,黑龙江佳木斯154007
基金项目:国家自然科学基金(20976166);浙江省教育厅高校青年教师资助专项(11134100309)
摘    要:以离子液体Bmim]BF4和水的混合溶剂为萃取溶剂,采用微波辅助技术萃取金银花中的绿原酸,并对微波辅助条件进行了优化。结果表明,萃取溶剂Bmim]BF4/V水为4/11;萃取时间9min;微波功率600W条件下微波辅助萃取绿原酸,绿原酸的萃取得率为1.475%。与传统的溶剂萃取方法进行比较,离子液体萃取法快速、高效。

关 键 词:离子液体  微波辅助萃取  金银花  绿原酸

Application of Ionic Liquids in Microwave-Assisted Extraction of Chlorogenic
Institution:LI Qing-long, Qu You-le, OU YANG Xiao-kun (1. Food and Pharmacy & Medical School of Zhejiang Ocean University, Zhoushan 316004; 2. College of Chemical and Pharmacy, Jiamusi University, Jiamusi 154007, China)
Abstract:The application of hydrophilic imidazole ionic liquid Bmim]BF4 mixed with water for solvent extraction, and microwave-assisted extraction of chlorogenic acid from honeysuckle were investigated. The effects of microwave power, extraction time and solvent were discussed, respectively. The optimal conditions were that the solvent was VBmim]BF4 /V ,(4/11 ), the extraction time was 9 min; the microwave power was 600 W, the yield of ehlorogenic acid was 4.75%. The proposed method was rapid and efficient to extract chlorogenic acid from honeysuckle compared with traditional solvent extraction.
Keywords:ionic liquid  microwave-assisted extraction  honeysuckle  chlorogenic acid
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