| 薄层色谱法鉴别加味三黄片的有效成分及薄层扫描法测定加味三黄片中小檗碱的含量 |
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| 引用本文： | 杨建明,李立恒,王志勇,曹亮,薛贵平,黄红娜.薄层色谱法鉴别加味三黄片的有效成分及薄层扫描法测定加味三黄片中小檗碱的含量[J].河北北方学院学报(自然科学版),2011,27(2):31-34,39. |
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| 作者姓名： | 杨建明 李立恒 王志勇 曹亮 薛贵平 黄红娜 |
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| 作者单位： | 1. 河北北方学院基础医学院药学系,河北张家口,075000
2. 河北北方学院附属第一医院,河北张家口,075000 |
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| 摘 要： | 目的 建立薄层色谱法鉴别加味三黄片中主要有效成分的方法 及薄层扫描法测定三黄片中小檗碱的含量的方法.方法 采用甲醇回流提取法制备供试品,用薄层色谱法鉴定三黄片中的小檗碱,黄芩苷,大黄素及大黄酚等成分,利用薄层扫描法测定加味三黄片中小檗碱的含量,扫描条件为:检测波长λ=345 nm.结果 加味三黄片供试品与对照品色谱在相...
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| 关 键 词： | 加味三黄片 成分鉴定 薄层色谱法 含量测定 薄层扫描法 |
Identification of Chief Effective Component of Jiawei Sanhuang Tablet with Thin-Layer Chromatography (TLC) and Determination of Content of Berberine in Jiawei Sanhuang Tablet with TLC Scanning |
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| YANG Jian-ming,LI Li-heng,WANG Zhi-yong,CAO Liang,XUE Gui-ping,HUANG Hong-na.Identification of Chief Effective Component of Jiawei Sanhuang Tablet with Thin-Layer Chromatography (TLC) and Determination of Content of Berberine in Jiawei Sanhuang Tablet with TLC Scanning[J].Journa of Hebei North University:Natural Science Edition,2011,27(2):31-34,39. |
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| Authors: | YANG Jian-ming LI Li-heng WANG Zhi-yong CAO Liang XUE Gui-ping HUANG Hong-na |
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| Institution: | YANG Jian-ming1,LI Li-heng2,WANG Zhi-yong1,CAO Liang2,XUE Gui-ping1,HUANG Hong-na1(1.College of Basic Medicine,Hebei North University,Zhangjiakou 075000,Hebei,China,2.The First Affiliated Hospital,China) |
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| Abstract: | Objective To develop the methods of TLC to identify the chief effective components of Sanhuang tablet and the methods of TLC scanning to determine the content of Berberine in Sanhuang tablet.Methods The testing solution was prepared by refluxing in methanol.The Berberine,Emodin,Chrysophanol and Baicalin in Jiawei Sanhuang tablet were identified by the motheds of TLC,and the content of Berberine in Jiawei Sanhuang tablet was determined by the mothed of TLC scanning.The detection wavelength was 345 nm.Results... |
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| Keywords: | Jiawei Sanhuang tablet components identification TLC determination of content TLC scanning |
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