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石油储罐罐底油三相分离工艺研究
引用本文:王艳红,葛文中,蔡亚平,张华,杨元凤,杨德武.石油储罐罐底油三相分离工艺研究[J].黑龙江八一农垦大学学报,2009,21(1):79-82.
作者姓名:王艳红  葛文中  蔡亚平  张华  杨元凤  杨德武
作者单位:1. 黑龙江八一农垦大学生命科学技术学院,大庆,163319
2. 沈阳化工学院机械工程学院
摘    要:罐底油具有油水乳化严重、油渣相互附着力强、渣颗粒相对比重小等特点,直接进行油水渣三相分离获得原油非常困难。为解决罐底油三相分离的技术问题,本文采用Tween-80破乳剂打破“W/O”状态,再辅以超声振荡和适当微波加热措施,使原油与水、无机固形物之间解吸附而分离。单因素与正交试验结果显示:以3%质量浓度破乳剂与罐底油体积比为1:1、温度50℃、超声处理12min后,原油回收率可达到98.4%。

关 键 词:罐底油  油渣  破乳剂  三相分离

Study On The Triple-phase Separation Technology of Oil-water Sludge from Oil Storage
Wang Yanhong,Ge Wenzhong,Cai Yaping,Zhang Hua,Yang Yuanfeng,Yang Dewu.Study On The Triple-phase Separation Technology of Oil-water Sludge from Oil Storage[J].Journal of Heilongjiang August First Land Reclamation University,2009,21(1):79-82.
Authors:Wang Yanhong  Ge Wenzhong  Cai Yaping  Zhang Hua  Yang Yuanfeng  Yang Dewu
Institution:Wang Yanhong, Ge Wenzhong, Cai Yaping, Zhang Hua, Yang Yuanfeng, Yang Dewu (1.College of Life Science and Technology, Heilongjiang August First Land Reclamation University, Daqing 163319; 2.Shen Yang Institute of Chemical Technology)
Abstract:Oil-water sludge had the characteristics of good emulsification oil-water, strong adhesion of oily sludge and small relative gravity in oil-water sludge which was difficult to directly separate crude oil from oil-water sludge. In order to solve the triple-phase separation technology of oil-water sludge, Tween-80 was selected to destroy emulsification of "W/O", followed by ultrasonic oscillating and microwave heating, which made the inorganic solids disintegrate and the crude oil from oil-water sludge were reclaimed. According to single-factor-analysis and orthogonal experiment design, the optimal process was confirmed that separation temperature was 50℃, 3% emulsification reagent, ultrasonic oscillating was 12 minutes, volume rate of emulsification reagent and oil-water sludge was 1:1. The rate of reclaiming crude oil could arrive at 98.4%.
Keywords:oil-water sludge  oily sludge  emulsification reagent  triple phase separation
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