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马尾松土贡种源松针挥发油化学成分GC/MS分析
引用本文:李军集,周丽珠,聂永雄,舒文波,梁忠云,谷瑶.马尾松土贡种源松针挥发油化学成分GC/MS分析[J].云南林业科技,2014(3):27-30.
作者姓名:李军集  周丽珠  聂永雄  舒文波  梁忠云  谷瑶
作者单位:[1]广西林业科学研究院,广西南宁530002 [2]国家林业局中南速生材繁育实验室,广西南宁530002 [3]广西苍梧县国营天洪岭林场,广西苍梧543100
基金项目:广西财政专项基本科研业务费(林科201407)资助.
摘    要:用挥发油提取器提取马尾松土贡种源松针中挥发油,利用气相色谱-质谱(GC-MS)分析其中的化学成分,采用GC峰面积归一化法定量,并与马尾松普通种源松针油做对比。结果表明,土贡种源和普通种源挥发油得油率分别为0.52%、0.60%,各分出69、75个成分,鉴定其中23个,分别占挥发油总量的92.65%、94.56%,其挥发油主要成分为α-蒎烯(37.673%、46.715%)、莰烯(3.724%、3.015%)、β-蒎烯(14.969%、12.978%)、石竹烯(8.242%、10.212%),除α-蒎烯含量相差9.042%以外,其他成分含量相差不大。

关 键 词:马尾松  土贡种源  松针油

GC/MS Analysis of Chemical Composition of Pine Needle Oil from Pinus massoniana Tugong Provenance
LI Jun-ji,ZHOU Li-zhu,NIE Yong-xiong,SHU Wen-bo,LIANG Zhong-yun,GU Yao.GC/MS Analysis of Chemical Composition of Pine Needle Oil from Pinus massoniana Tugong Provenance[J].Yunnan Forestry Science and Technology,2014(3):27-30.
Authors:LI Jun-ji  ZHOU Li-zhu  NIE Yong-xiong  SHU Wen-bo  LIANG Zhong-yun  GU Yao
Institution:1. Guangxi Academy of Forestry, Nanning Guangxi 530002, P. R. China; 2. Key Laboratory of Central South Fast-growing Timber Cultivation of Forestry Ministry, Nanning Guangxi 530002, P. R. China; 3. Tianhongling State-owned Forest Farm, Cangwu Guangxi 543100, P. R. China)
Abstract:The essential oil of Tugong Provenance and ordinary type Pinus massoniana was extracted by the volatile oil extractor , and the chemical composition of essential oil was analyzed and compared by gas chromatography -mass spectrometry ( GC-MS) by using the peak area normalization method .The results showed that the yield of essential oil of these two provenances were 0.52 % and 0.60 % respectively .23 constituents were identified from 69 and 75 chromatographic peaks respectively , and the relative content up to 92.65%, 94.56% respectively .The major constituents were α-pinene ( 37.673 %, 46.715 %) , camphene ( 3.724 %, 3.015 %) , β-pinene (14.969 %, 12.978 %), caryophyllene (8.242 %, 10.212 %).The major constituents were similar except theα-pinene content difference with 9.042 %.
Keywords:GC-MS  Pinus massoniana  Tugong Provenance  pine needle oil  GC-MS
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