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超声波-微波协同提取香樟木质部提取物的响应面优化
引用本文:李权,林金国,王晓娴. 超声波-微波协同提取香樟木质部提取物的响应面优化[J]. 福建农业大学学报(自然科学版), 2013, 0(6): 665-670
作者姓名:李权  林金国  王晓娴
作者单位:福建农林大学材料工程学院,福建福州350002
基金项目:国家级星火计划重大资助项目(2012GA720001);国家林业局林业公益性行业科研专项资助项目(200704010);福建省自然科学基金资助项目(B0110024).
摘    要:
采用响应面优化方法,在单因素试验的基础上,用Design-Expt软件Box-Behnken Design建立数学模型,并对各因素及其相互间的交互作用进行分析.结果表明:回归得到的二次多项式模型极显著,模型的预测值与试验真实值之间的相关性达98.83%.优化后的最佳工艺参数:液料比60 mL·g-1,提取时间30 min,粒径大小40-50目.在该条件下香樟木质部提取物得率为4.65%,与理论预测值基本一致.

关 键 词:超声波-微波协同提取  得率  工艺优化

Optimization of microwave-ultrasound assisted extraction of extractives from Cinnamomum camphora wood using response surface methodology
LI Quan,LIN Jin-guo,WANG Xiao-xian. Optimization of microwave-ultrasound assisted extraction of extractives from Cinnamomum camphora wood using response surface methodology[J]. Journal of Fujian Agricultural University, 2013, 0(6): 665-670
Authors:LI Quan  LIN Jin-guo  WANG Xiao-xian
Affiliation:(College of Material Engineering, Fujian Agriculture and Forestry University, Fuzhou, Fujian 350002, China)
Abstract:
The mathematical model was established using Box-Behnken Design of Design-Expert software and effect of various factors and their interactions were analyzed as we ll.The results showed that the second order polynomial was the best model,the correlation between model prediction and test real value was 98.83%.The optimum extraction condition was as follows:liquid-solid ratio of 60 mL · g-1,extraction time of 30 min,particle size of 40-50 mesh.Under above optimum condition,the extraction yield was 4.65%,which was basically equal to theoretical prediction value.
Keywords:microwave-ultrasound assisted extraction  yield  process optimization
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