| 农药中间体3，5，6-三氯吡啶-2-醇钠的合成 |
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| 引用本文： | 王同涛,张瑞生,刘自友,齐慧芹,李少华.农药中间体3，5，6-三氯吡啶-2-醇钠的合成[J].农药科学与管理,2009,30(7):31-34. |
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| 作者姓名： | 王同涛 张瑞生 刘自友 齐慧芹 李少华 |
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| 作者单位： | 山东华阳科技股份有限公司,山东,泰安,271411 |
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| 摘 要： | 本文介绍了3，5，6-三氯吡啶-2-醇钠的合成方法，以三氯乙酰氯为起始原料，经过加成、环化、芳构化制备，产品含量可达93．8％，总收率为71．2％（以三氯乙酰氯计）。
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| 关 键 词： | 3 5 6一三氯吡啶-2-醇钠 三氯乙酰氯 丙烯腈 合成 |
Synthesis of 3,5,6-trichloropyridin-2-ol sodium |
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| Wang Tongtao,Zhang Ruisheng,Liu Ziyou,Qi Huiqin,Li Shaohua.Synthesis of 3,5,6-trichloropyridin-2-ol sodium[J].Pesticide Science and Administration,2009,30(7):31-34. |
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| Authors: | Wang Tongtao Zhang Ruisheng Liu Ziyou Qi Huiqin Li Shaohua |
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| Institution: | Shandong Huayang Technology Co.;Ltd;Taian 271411;China |
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| Abstract: | The article introduced synthetic methods for 3,5,6-trichloropyridin-2-ol sodium,The trichloroacetyl chloride was used as starting material,followed by addition,cyclization and aromatization. The content of 3,5,6-trichloropyridin-2-ol sodium in final product was up to 93.8% with a total yield of 71.2%(calculated by trichloroacetyl chloride) . |
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| Keywords: | 3 5 6-trichloropyridin-2-ol sodium trichloroacetyl chloride acrylonitrile synthesis |
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