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| 薄膜样品的制作与均匀度测定 | |
| 引用本文： | 池济宏,李寒辉,赵素英.薄膜样品的制作与均匀度测定[J].河北北方学院学报(自然科学版),2006,22(3):21-24. |
| 作者姓名： | 池济宏 李寒辉 赵素英 |
| 作者单位： | 1. 河北北方学院基础农学部,河北,张家口,075000 2. 北京邮电大学,北京,100876 3. 万全中学,河北,万全,076250 |
| 摘 要： | 液滴法1]是制作薄膜样品的最简单方法,本文介绍了使用该方法制作薄膜样品的具体步骤.由于样品在自然蒸发过程中具有结晶效应,使得最终形成的样品极不均匀.如果使用这种样品刻度系统的灵敏度曲线,样品的不均匀性会引起严重的实验误差.利用使用X光会聚透镜的XRF系统2]形成的小束斑,可对样品的均匀度进行分析.另外文中给出了在使用此种样品刻度系统灵敏度曲线时,消除样品不均匀性引起误差的方法. |
| 关 键 词： | 液滴法 X光会聚透镜 均匀度 XRF分析 |
| 文章编号： | 1673-1492(2006)03-0021-04 |
| 收稿时间： | 04 20 2006 12:00AM |
| 修稿时间： | 2006年4月20日 |
Making Film Sample and Measement of Its Uniformity |
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| CHI Ji-hong,LI han-hui,ZHAO Su-ying.Making Film Sample and Measement of Its Uniformity[J].Journa of Hebei North University:Natural Science Edition,2006,22(3):21-24. | |
| Authors: | CHI Ji-hong LI han-hui ZHAO Su-ying |
| Institution: | 1. Department of Base Course, Hebei North University, Zhangjiakou, Hebei 075000, China; 2. Beijing University of Posts and Telecommunications, Beijing 100876, China; 3. Wanquan Middle School, Wanquan, Hebei 076250, China |
| Abstract: | A means to make film sample is described in detail in this paper. But the final sample is quite non-uniform because of crystallization. When the sample is used to perform sensitivity calibration of the instrument, serious error will arise. However, the micro-beam of the monolithic X-ray focusing lens can be used to analyze distribution of the elements on the sample. And a method is also put forward to eliminate the influence of crystallization when the samples are used to perform sensitivity calibration. |
| Keywords: | liquidtitration method X-ray focusing lens uniformity X-ray fluorescence analysis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |