显脉金花茶叶的化学成分研究 |
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引用本文: | 黄艳,刘鹏,莫建光.显脉金花茶叶的化学成分研究[J].安徽农业科学,2013(28):11336-11336,11379. |
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作者姓名: | 黄艳 刘鹏 莫建光 |
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作者单位: | 广西分析测试研究中心,广西南宁,530022;广西分析测试研究中心,广西南宁,530022;广西分析测试研究中心,广西南宁,530022 |
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基金项目: | 广西科技攻关项目(桂科攻0815005-1-20) |
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摘 要: | 目的]利用现代化学技术分析显脉金花茶叶的化学成分。方法]用石油醚、氯仿、乙酸乙酯萃取经乙醇浸提得到的显脉金花荼总浸膏,通过薄层硅胶柱分离、薄层色谱(TLC)鉴别,重结晶得到7种单体化合物,利用各种光谱技术和理化性质进行结构鉴定。结果]鉴定出其中7个化合物的结构,包括甾醇类2个,三萜类化合物3个,脂肪醇类1个,黄酮类化合物1个,分别为β-谷甾醇、α-菠菜甾醇、伊香树素、齐墩果酸、olibanumol—L、正三十四醇和山奈酚。结论]α-菠菜甾醇、正三十四醇和olibanumol—L均为首次从该种植物中鉴定出来,β-香树素和山奈酚为首次从该属植物中分离鉴定出来。
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关 键 词: | 金花茶 成分 质谱 薄层色谱 |
Analysis of Chemical Components of Camellia euphlebia Merr. ex Sealy in Guangxi |
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Institution: | HUANG Yan et al ( Guangxi Center of Analysis and Test Research, Nanning, Guangxi 530022) |
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Abstract: | Objective ] To analyze the chemical components of Camellia euphlebia Merr. ex Sealy in Guangxi by modern chemical technology. Method ] The ethanol extracts of C. euphlebia was extracted with petroleum ether, chloroform, ethyl acetate according to the different polarity of solvent, the extracts of petroleum-ether phase, chloroform phase, ethyl-acetate phase were obtained respectively. The compounds were iso- lated and purified by silica ge! column and thin layer chromatography ( TLC ). Various spectroscopic techniques and the physieochemical prop- erties of the structures were used to identify seven kinds of compounds. Result] fl-sitosterol, α-spinasterol, oleanie acid, olibanumol-L, n- tetratriacontanol, kaempfero] were isolated and purified from C. euphlebia in Guangxi. Conclusion ] β-spinasterol, n-tetratriaeontanol, olibanumol-L were the first time identified from the plant, and β-amyrin, kaempferol were firstly isolated from the genus. |
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Keywords: | Camellia euphlebia Merr ex Sealy Components MS TLC |
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