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| 水稻中乙酰甲胺磷及其代谢产物甲胺磷农药残留分析方法 | |
| 引用本文： | 郑杨. 水稻中乙酰甲胺磷及其代谢产物甲胺磷农药残留分析方法[J]. 农药科学与管理, 2010, 31(8): 37-39 |
| 作者姓名： | 郑杨 |
| 作者单位： | 黑龙江省农药管理检定站,黑龙江,哈尔滨,150090 |
| 摘 要： | 采用乙腈和水（70：5，V／V）为溶剂提取水稻中乙酰甲胺磷、甲胺磷，其他采用NY/T761—2008方法，气相色谱法（FPD检测器）进行测定2种农药在糙米中的残留，其添加回收率为78．7％-91．8％，变异系数为5．72％-14．1％，乙酰甲胺磷的最低检出限为0．005mg/kg，甲胺磷的最低检出限为0．01mg／kg。 |
| 关 键 词： | 乙酰甲胺磷 甲胺磷 残留分析 气相色谱 |
Determination of Residues of Acephate and Its Metabolite in Rice by GC |
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| Zheng Yang. Determination of Residues of Acephate and Its Metabolite in Rice by GC[J]. Pesticide Science and Administration, 2010, 31(8): 37-39 | |
| Authors: | Zheng Yang |
| Affiliation: | Zheng Yang(Institute for the Control of Agrochemicals of Heilongjiang Province,Harbin 150090,China) |
| Abstract: | A method for the determination of acephate and methamidophos residues in rice was developed.The samples were extracted with acetonitrile+water(70+5).Acephate and methamido-phos were quantitated by GC with a FPD detector.The average recoveries ranged from 78.7% to 91.8% and the relative standard deviations were from 5.7% to 14.1%.The limit of detection of acephate and methamidophos were 0.005mg/kg and 0.01mg/kg. |
| Keywords: | acephate methamidophos residue analysis GC |
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