唑螨酯原药高效液相色谱分析方法研究 |
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引用本文: | 杨 晶,曹立冬,李凤敏,等.唑螨酯原药高效液相色谱分析方法研究[J].农药科学与管理,2014(1):38-41. |
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作者姓名: | 杨 晶 曹立冬 李凤敏 等 |
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作者单位: | 中国农业科学院植物保护研究所,北京100193 |
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摘 要: | 本文采用高效液相色谱法,以乙腈+水为流动相,使用Eclipse XDB-C18、5μm为填料的不锈钢柱和二极管阵列检测器,在260nm波长下对唑螨酯原药进行分离和定量分析。结果表明,该分析方法的线性相关系数为1.000 0;标准偏差为0.53;变异系数为0.56%;平均回收率为100.59%。
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关 键 词: | 唑螨酯 原药 高效液相色谱 分析 |
Analytical Method for Determination of Fenpyroximate TC by HPLC |
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Institution: | Yang ring, Cao Lidong, Li Fengmin, Huang Qiliang ( Institute of Plant Protection, Chinese Academy of Agricultural Sciences, Beijing 100193, China) |
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Abstract: | A method for separation and quantitative analysis of fenpyroximate TC by HPLC with acetonitrile and water solution as mobile phase, Eclipse XDB-C18 column and DAD at 260nm wavelength was described. The results showed that the linear correlation coefficient was 1.000 0, the standard deviation was 0.53, the variation coefficient was 0.56%, the average recovery was 100.59%. |
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Keywords: | fenpyroximate TC HPLC analysis |
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