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氯丙嘧啶酸原药及其杂质的高效液相色谱-质谱联用法分析
引用本文:胡礼,王胜翔,薄瑞. 氯丙嘧啶酸原药及其杂质的高效液相色谱-质谱联用法分析[J]. 农药科学与管理, 2011, 0(2): 45-47
作者姓名:胡礼  王胜翔  薄瑞
作者单位:湖南化工研究院;农业部农药检定所;
摘    要:采用高效液相色谱-质谱联用法对氯丙嘧啶酸原药中的有效成分及其杂质进行分离分析。得到氯丙嘧啶酸及其2个杂质的质谱图,并根据质谱图推断出各杂质可能的结构。

关 键 词:氯丙嘧啶酸  杂质  高效液相色谱-质谱联用

Identification of Aminocyclopyrachlor and Relative Impurities in TC by HPLC-MS
Hu Li,Wang Shengxiang,Bo Rui(Institute for the Control of Agrochemicals,Ministry of Agriculture,Beijing. Identification of Aminocyclopyrachlor and Relative Impurities in TC by HPLC-MS[J]. Pesticide Science and Administration, 2011, 0(2): 45-47
Authors:Hu Li  Wang Shengxiang  Bo Rui(Institute for the Control of Agrochemicals  Ministry of Agriculture  Beijing
Affiliation:Hu Li(Hunan Reserch Institute of Chemical Industry,Changsha 410014,China),Wang Shengxiang,Bo Rui(Institute for the Control of Agrochemicals,Ministry of Agriculture,Beijing 100125
Abstract:A method for separation and identification of aminocyclopyrachlor technical material was developed.The aminocyclopyrachlor and 2 relative impurities in aminocyclopyrachlor technical material were separated and identified.The chemical structures of these compounds were confirmed.
Keywords:Aminocyclopyrachlor  impurities  HPLC-MS  
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